Abstract
A thermal expansion coefficient (αp) is an essential thermophysical quantity for high pressure research. The thermal expansion coefficient is the volume change over temperature in an isobaric heating process. Although isobaric heating processes for diamond anvil cell (DAC) have been conducted by keeping the pressure constant during heating, pressure determination at high temperature high pressure is debatable for decades long. In this paper, a revertible heating/cooling approach is presented, while its pressure determination at high temperature high pressure is not required. A pressure-dependent thermal expansion coefficient of MgO at 9.5 GPa by revertible heating/cooling was determined by a DAC and its result matches with the one collected by large volume press, whose isobaric heating was conducted by manually adjusting its load/pressure.
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Acknowledgements
J. Yan thanks Q. Williams, M. Kunz, A. Doran, A. MacDowell, and B. Kalkan for their discussion and support to this project. J. Yan was supported by COMPRES, the Consortium for Materials Properties Research in Earth Sciences under NSF Cooperative Agreement EAR 1606856. The X-ray diffraction research used resources of the Advanced Light Source, which is a DOE Office of Science User Facility under contract no. DE-AC02-05CH11231. We acknowledge partial support from NSF CIMM project under Award No. 1541079, CIMM LINK project, DOE/NNSA Award No. DE-NA0003979, and DoD support under Contract No. W911NF1910005, NSF LAMDA Project Award # 1946231 under SEED Track 1B support.
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Yan, J., Yang, S. Pressure-Dependent Thermal Expansion Coefficient by a Diamond Anvil Cell. Int J Thermophys 43, 17 (2022). https://doi.org/10.1007/s10765-021-02945-3
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DOI: https://doi.org/10.1007/s10765-021-02945-3