Abstract
At the National Metrology Institute of Japan (NMIJ), the triple points of \(^{20}\)Ne and \(^{22}\)Ne were realized using modular sealed cells, manufactured by the Istituto Nazionale di Ricerca Metrologica (INRiM) in Italy to measure the difference of the triple-point temperatures of \(^{20}\)Ne and \(^{22}\)Ne. Standard platinum resistance thermometers (SPRTs) were used that were calibrated by NMIJ on the International Temperature Scale of 1990 (ITS-90). In previous reports, sealed cells of \(^{20}\)Ne and \(^{22}\)Ne were mounted one at a time in a cryostat and their triple points were realized in separate cool-downs (the single-cell measurement). In this study, first, the triple point was realized using the single-cell measurement for \(^{20}\)Ne and \(^{22}\)Ne cells. Second, the \(^{20}\)Ne and \(^{22}\)Ne cells were mounted together on the same copper block and their triple points were realized subsequently one after the other in the same cool-down of the cryostat (the double-cell measurement). The melting curves observed by the single-cell and the double-cell measurements were almost identical for each cell. The difference of the triple-point temperatures between the two cells, \(^{22}T -^{20}\!T\), was estimated, not only using the subrange of SPRTs defined in the ITS-90 from 13.8033 K to 273.16 K (subrange 1) but also that defined from 24.5561 K to 273.16 K (subrange 2). The difference in \((^{22}T-^{20}\!\!T)\) between the subranges 1 and 2 is within 0.06 mK, which is caused by the subrange inconsistency in the ITS-90. The standard uncertainty in \((^{22}T-^{20}\!T)\) due to the subrange inconsistency is estimated to be 0.017 mK. After correction for the effects of impurities and other isotopes in the \(^{20}\)Ne and \(^{22}\)Ne cells, the difference in the triple-point temperatures between pure \(^{20}\)Ne and pure \(^{22}\)Ne is estimated to be 0.146 64 (5) K on subrange 1, which is consistent within the uncertainty with the former studies. When \(^{22}T-^{20}\!T\) for pure \(^{20}\)Ne and pure \(^{22}\)Ne is estimated on subrange 2, \(^{22}T-^{20}\!\!T\) becomes 0.146 60 (5), which agrees very well with the former reports of INRiM evaluating \(^{22}T-^{20}\!T\) on subrange 2.
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The authors thank Dr. Shimazaki and Dr. Nakagawa for their valuable discussions.
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Nakano, T., Tamura, O., Steur, P.P.M. et al. Study on the Difference Between the Triple-Point Temperatures of \(^{20}\)Ne and \(^{22}\)Ne Using Sealed Cells. Int J Thermophys 35, 1032–1043 (2014). https://doi.org/10.1007/s10765-014-1697-y
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DOI: https://doi.org/10.1007/s10765-014-1697-y