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Effects of Ultralow Temperature and Water Saturation on the Mechanical Properties of Sandstone

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Abstract

The surrounding rocks are subjected to ultralow temperatures in applications like liquid nitrogen fracturing, underground storage of liquefied natural gas and polar constructions etc. The mechanical properties of sandstone with different saturations under freezing temperature and after one ultralow temperature freeze–thaw cycle test conditions were investigated in this study. The uniaxial compressive strength (UCS) of both dry and saturated samples increases with the decrease in temperature except at − 90 °C under freezing temperature test conditions, while the UCS of saturated samples is lower than that of dry samples after one ultralow temperature freeze–thaw cycle due to the water softening effects and the damage induced during the water–ice phase transition. The failure patterns of dry samples are more complex than those of saturated samples under freezing temperature, which is also indicated in the lower brittleness index for the saturated samples. The ice cohesion effect and its creep deformation increase the plastic deformation, while decreasing the Young’s modulus of saturated samples under freezing temperature. In addition, the ice net formed in the connected pores significantly increases the sample tensile strength and makes its failure less severe. The UCS, Young’s modulus and brittleness index decrease with saturation under − 120 °C, while the tensile strength increases with saturation. Porosity reduction measured by computerized tomography for the saturated samples after one freeze–thaw cycle is largest at − 120 °C compared with those at − 60 °C and − 180 °C, which is certified by the pore filling shown in scanning electron microscope images.

Highlights

  • Tensile strength is more sensitive to the variations of subzero temperatures compared with the compression strength.

  • The cohesion and creep deformation of ice increase the plastic deformation while decrease the elastic modulus.

  • Porosity reduces after one freeze-thaw cycle due to pore filling.

  • Compression strength and brittleness index decrease while tensile strength increases with the saturation under − 120℃.

  • Failure patterns of dry samples are more complex than those of saturated samples under low temperatures.

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References

  • Arakawa M, Maeno N (1997) Mechanical strength of polycrystalline ice under uniaxial compression. Cold Reg Sci Technol 26(3):215–229

    Google Scholar 

  • Bai Y, Shan R, Ju Y, Wu Y, Sun P, Wang Z (2020) Study on the mechanical properties and damage constitutive model of frozen weakly cemented red sandstone. Cold Regions Sci Technol 2020:171

    Google Scholar 

  • Cai CZ, Li GS, Huang ZW, Shen ZH, Tian SC, Wei JW (2014a) Experimental study of the effect of liquid nitrogen cooling on rock pore structure. J Nat Gas Sci Eng 21:507–517

    Google Scholar 

  • Cai CZ, Li GS, Huang ZW, Shen ZH, Wang HZ, Tian SC, Wei JW (2014b) Experiment study of rock porous structure damage under cryogenic nitrogen freezing. Rock Soil Mech 35(4):965–971

    Google Scholar 

  • Chen TC, Yeung MR, Mori N (2004) Effect of water saturation on deterioration of welded tuff due to freeze–thaw action. Cold Reg Sci Technol 38(2–3):127–136

    Google Scholar 

  • Chung SK, Han KC, Park ES (2006) Feasibility study of underground LNG storage system in rock cavern. Tunnel Undergr Space 16(4):296–306

    Google Scholar 

  • Feng Q, Jiang BS, Zhang Q, Wang LP (2014) Analytical elasto-plastic solution for stress and deformation of surrounding rock in cold region tunnels. Cold Reg Sci Technol 108:59–68

    Google Scholar 

  • Feng Q, Jin J, Zhang S, Liu W, Yang X, Li W (2022) Study on a damage model and uniaxial compression simulation method of frozen–thawed rock. Rock Mech Rock Eng 55(1):187–211

    Google Scholar 

  • Haynes FD (1980) Temperature effect on the uniaxial strength of ice. In: International conference on port and ocean engineering under arctic conditions. Trondheim, Norway (CONF-790833)

  • He T, Chong ZR, Zheng J, Ju Y, Linga P (2019) LNG cold energy utilization: prospects and challenges. Energy 170(2):557–568

    Google Scholar 

  • Huang S, Ye Y, Cui X, Cheng A, Liu G (2020) Theoretical and experimental study of the frost heaving characteristics of the saturated sandstone under low temperature. Cold Regions Sci Technol 2020:174

    Google Scholar 

  • Inada Y, Yokota K (1984) Some studies of low temperature rock strength. Int J Rock Mech Min Sci Geomech Abstr 21(3):145–153

    Google Scholar 

  • Ji SY, Wang AL, Su J, Yue QJ (2011) Experimental studies on elastic modulus and flexural strength of sea ice in the Bohai Sea. J Cold Regions Eng 25(4):182–195

    Google Scholar 

  • Jia H, Liu Q, Xiang W, Zhang W, Lang L (2013) Damage evolution model of saturated sandstone under freeze–thaw cycles. Chin J Rock Mech Eng 32(S2):3049–3055

    Google Scholar 

  • Jia H, Xiang W, Tan L, Zhang W, Zeng W, Cao S, Cheng C (2016) Theoretical analysis and experimental verifications of frost damage mechanism of sandstone. Chin J Rock Mech Eng 35(5):879–895

    Google Scholar 

  • Jia HL, Zi F, Yang GS, Li GY, Shen YJ, Sun Q, Yang PY (2019) Influence of pore water (ice) content on the strength and deformability of frozen argillaceous siltstone. Rock Mech Rock Eng 53(2):967–974

    Google Scholar 

  • Jia HL, Ding S, Zi F, Dong YH, Shen YJ (2020) Evolution in sandstone pore structures with freeze–thaw cycling and interpretation of damage mechanisms in saturated porous rocks. CATENA 195:104915

    Google Scholar 

  • Kammoshida N, Okawara M, Abe M, Furuzumi M (2010) Mechanical behavior of Kimachi sandstone under ultralow temperature. J Min Mater Process Inst Jpn 127(1):8–13

    Google Scholar 

  • Kodama J, Goto T, Fujii Y, Hagan P (2013) The effects of water content, temperature and loading rate on strength and failure process of frozen rocks. Int J Rock Mech Min Sci 62:1–13

    Google Scholar 

  • Kurilko A, Novopashin M (2005) Features of low temperature effect upon strength of enclosing rock and kimberlite in the “Udachnaya” pipe. J Min Sci 41(2):119–122

    Google Scholar 

  • Lemaitre J (1985) A continuous damage mechanics model for ductile fracture. J Eng Mater Technol 107(1):83-89

  • Li YP, Wang ZY (2012) Study of parameters and strength of thermal effects for granite under low temperature. Rock Soil Mech 33(2):321–325

    Google Scholar 

  • Li ZF, Xu HF, Zhang CY (2016) Liquid nitrogen gasification fracturing technology for shale gas development. J Petrol Sci Eng 138:253–256

    Google Scholar 

  • Liu M, Bai B, Li X (2014) Experimental studies on the short term effect of CO2 on the tensile failure of sandstone. Energy Proc 63:3357–3363

    Google Scholar 

  • Looney B (2021) Statistical review of world energy globally consistent data on world energy markets and authoritative publications in the field of energy. Rev World Energy Data 70:8–20

    Google Scholar 

  • Ma Z, Zhang G, Gamage RP, Zhang C (2021) Measurement of thermal expansion coefficient of rock minerals using XRD and its implications to thermal damage mechanism. IOP Conf Ser Earth Environ Sci 861(7):1

    Google Scholar 

  • Mardoukhi A, Mardoukhi Y, Hokka M, Kuokkala V-T (2020) Effects of test temperature and low temperature thermal cycling on the dynamic tensile strength of granitic rocks. Rock Mech Rock Eng 54(1):443–454

    Google Scholar 

  • Matsunaga I, Kuriyagawa M, Kinoshita N (1981) Mechanical properties of rock at cryogenic temperature. J Min Mater Process Inst Jpn 97:431–436

    Google Scholar 

  • Memon KR, Mahesar AA, Ali M, Tunio AH, Mohanty US, Akhondzadeh H, Awan FUR, Iglauer S, Keshavarz A (2020) Influence of cryogenic liquid nitrogen on petro-physical characteristics of mancos shale: an experimental investigation. Energy Fuels 34(2):2160–2168

    Google Scholar 

  • Ming F, Zhang S, Niu F, Zhou Z (2021) A study on crack damage stress and the damage constitutive model of frozen sandstone. Bull Eng Geol Env 80(9):6955–6970

    Google Scholar 

  • Ning JG, Wang H, Zhu ZW, Sun YX (2005) Investigation of the constitutive modle of frozen soil based on meso-mechanics. J Beijing Inst Technol 2005:10

    Google Scholar 

  • Sammis C, Biegel R (2004) Mechanics of strengthening in crystalline rock at low temperatures: a preliminary assessment. In: Proceedings of the 26th seismic research review: trends in nuclear explosion monitoring, pp 475–484

  • Song YQ, Liu JC, Shao ZX (2020) Experimental study on physical and mechanical properties of limestone under freezing thawing cycles. Sci Technol Eng 20(2):741–746

    Google Scholar 

  • Tang M, Wang Z, Sun Y, Ba J (2010) Experimental study of mechanical properties of granite under low temperature. Chin J Rock Mech Eng 29(4):787–794

    Google Scholar 

  • Ulusay R (2015) The ISRM suggested methods for rock characterization, testing and monitoring: 2007–2014. Int J Rock Mech Min Sci 46:627–634

    Google Scholar 

  • Wan D, Zhu Z, Zhou C, Li J, Ying P, Wang M (2020) Effect of pre-existing symmetrical cracks on propagation behaviors of a blast-induced crack. Shock Vib 2020:1

    Google Scholar 

  • Wang L, Lu Z, Shao S (2017) A composite power exponential nonlinear model of rock and soil. Chin J Rock Mech Eng 39(9):1724–1730

    Google Scholar 

  • Wang EL, Ren ZF, Han HW (2021) Experimental study on uniaxial compre-ssive strength of ultra-low temperature frozen clay. Chin J Geotech Eng 43(10):1851–1860

    Google Scholar 

  • Weibull W (1951) A statistical distribution function of wide applicability. J Appl Mech 18(3):293–297

    Google Scholar 

  • Xie Q, Zhu Z, Kang G (2014) Dynamic stress–strain behavior of frozen soil: experiments and modeling. Cold Reg Sci Technol 106–107:153–160

    Google Scholar 

  • Xu B, Li N, Li ZK, Yan N (2013) Low-temperature LPG and LNG storage caverns and related research review of rock mechanics. Chin J Rock Mech Eng 32(S2):2977–2993

    Google Scholar 

  • Zhang D, Ranjith PG, Perera MSA (2016) The brittleness indices used in rock mechanics and their application in shale hydraulic fracturing: a review. J Petrol Sci Eng 143:158–170

    Google Scholar 

  • Zhang D, Pathegama Gamage R, Perera M, Zhang C, Wanniarachchi W (2017) Influence of water saturation on the mechanical behaviour of low-permeability reservoir rocks. Energies 10(2):236

    Google Scholar 

  • Zhang HM, Wang H, Zhang JF (2020) Analysis of meso-damage characteristics of freeze–thaw rock on CT scale. J Liaoning Tech Univ (nat Sci) 39(1):51–56

    Google Scholar 

  • Zhao J, Xie M, Yu J, Zhao W (2019) Experimental study on mechanical properties and damage evolution of fractured rock under freezing-thawing action. J Eng Geol 27(6):1199–1207

    Google Scholar 

  • Zheng GH, Xu JY, Wang P, Fang XY, Wen M (2019) Physical characteristics and degradation model of stratified sandstone under freeze–thaw cycling. Rock Soil Mech 40(02):632–641

    Google Scholar 

  • Zhu YL, Zhang JY (1992) Constitutive relations of frozen soil in uniaxial compression. J Glaciol Geocryol 14(3):210–217

    Google Scholar 

Download references

Acknowledgements

The authors would like to acknowledge the financial support from the Natural Science Foundation of Hebei Province (E2020202170), Natural Science Foundation of China (42202325, 42172306) Top Young Talents Program of Department of Education of Hebei Province (BJ2021022) and Hebei Province (No. 2020HBQZYC001).

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Authors and Affiliations

  1. School of Civil and Transportation Engineering, Hebei University of Technology, Tianjin, 300401, China

    Decheng Zhang, Guanju Lu, Jie Wu & Wen Nie

  2. Department of Civil Engineering, Monash University, Building 60, Melbourne, VIC, 3800, Australia

    P. G. Ranjith

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  1. Decheng Zhang
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  2. Guanju Lu
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  3. Jie Wu
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  4. Wen Nie
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  5. P. G. Ranjith
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Correspondence to Jie Wu.

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Zhang, D., Lu, G., Wu, J. et al. Effects of Ultralow Temperature and Water Saturation on the Mechanical Properties of Sandstone. Rock Mech Rock Eng 56, 3377–3397 (2023). https://doi.org/10.1007/s00603-023-03229-y

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  • DOI: https://doi.org/10.1007/s00603-023-03229-y

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