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Nanoarchitectonics of eco-friendly nickel oxide nanoplatelets for energy storage

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Abstract

Nanostructured nickel hydroxide coatings were prepared directly by aqueous electrophoretic deposition (EPD) method without binder or organic solvent. β-Ni(OH)2 nanoplatelets were first synthetized by chemical precipitation from nickel nitrate in ammonia under ultrasound. These particles, stabilized at pH ≈ 8, present an equivalent diameter of 250 nm and an electrophoretic mobility of ≈ + 2.5 × 10–8 m2 V−1 s−1. Cathodic EPD was performed at room temperature for different values of particles concentration, deposition time and applied electric field. An optimal coating was achieved using a 1 g L−1 of β-Ni(OH)2 particles suspension during 30 min deposition time at an electric field of 75 V m−1. In this work, the suspension conductivity was studied showing that a very narrow range of conductivity can leads to efficient deposition in aqueous EPD. The β-Ni(OH)2 coatings were heated at 325 °C in air for 1, 2 and 3 h to form NiO films. The electrochemical properties of the NiO films were evaluated by cyclic voltammetry (CV) and galvanostatic charge/discharge (GCD). Significant differences were observed in term of specific capacitance values as a function of annealing time and film thickness. Finally, the film microstructure was determined by the calculation of the electrochemically active surface area (ECSA) using Randles–Ševčík equation.

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Acknowledgements

The authors would like to acknowledge Marie-Laure LEONARD from ESIREM, Université de Bourgogne for TGA analysis and Virginie MOUTARLIER for XRD analysis and Nicolas ROUGE for SEM analysis from UTINAM Institute platform.

Funding

Funding was provided by Ministère de l'Enseignement supérieur, de la Recherche et de l'Innovation.

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Authors and Affiliations

  1. Institut UTINAM-UMR 6213 CNRS, Université de Bourgogne Franche-Comté, Besançon, France

    Siham Mouhtadi, Cédric C. Buron, Claudine Filiâtre & Isabelle Pochard

  2. Instituto de Cerámica y Vidrio, CSIC, Madrid, Spain

    Oxel Urra & Begoña Ferrari

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  1. Siham Mouhtadi
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  2. Oxel Urra
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Correspondence to Isabelle Pochard.

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Mouhtadi, S., Urra, O., Buron, C.C. et al. Nanoarchitectonics of eco-friendly nickel oxide nanoplatelets for energy storage. Appl. Phys. A 129, 6 (2023). https://doi.org/10.1007/s00339-022-06278-2

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