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Pulsed laser deposition of functionalized Mg–Al layered double hydroxide thin films

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Abstract

In this paper, magnesium–aluminium layered double hydroxide (LDH) has been functionalized with sodium dodecyl sulfate (DS) and deposited as thin film by pulsed laser deposition (PLD). Mg, Al-LDH powders were prepared by co-precipitation and used as reference material. Intercalation of DS as an anionic surfactant into the LDHs host layers has been prepared in two ways: co-precipitation (P) and reconstruction (R). DS intercalation occurred in LDH powder via both preparation methods. The films deposited via PLD, in particular at 532 and 1064 nm, preserve the organic intercalated layered structure of the targets prepared from these powders. The results reveal the ability of proposed deposition technique to produce functional composite organo-modified LDHs thin films.

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Acknowledgements

Financial support from Romanian National NUCLEU Program LAPLAS4-code 16 47, Projects PN-II-RU-TE-2014-4-1550 and Projects PN-II-RU-TE-2014-4-0976 is gratefully acknowledged. C.C.M. and A.W.H. gratefully acknowledge the financial support by the Austrian Federal Ministry of Science, Research and Economy and the National Foundation for Research, Technology and Development in the frame of the Christian Doppler Laboratory for Combinatorial Oxide Chemistry (COMBOX).

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Authors and Affiliations

  1. National Institute for Lasers, Plasma and Radiation Physics, Atomistilor 409, Bucharest, Romania

    A. Vlad, R. Birjega, I. Tirca, A. Matei, A. Nedelcea & M. Dinescu

  2. Faculty of Sciences, University of Craiova, 200585, Craiova, Romania

    I. Tirca

  3. Department of Chemical Technology and Catalysis, Faculty of Chemistry, University of Bucharest, 4-12 Regina Elisabeta Bd., 030018, Bucharest, Romania

    R. Zavoianu

  4. Christian Doppler Laboratory for Combinatorial Oxide Chemistry at the Institute for Chemical Technology of Inorganic Materials (ICTAS), Johannes Kepler University Linz, Altenberger Str. 69, 4040, Linz, Austria

    C. C. Mardare & A. W. Hassel

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  1. A. Vlad
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Correspondence to A. Vlad.

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Vlad, A., Birjega, R., Tirca, I. et al. Pulsed laser deposition of functionalized Mg–Al layered double hydroxide thin films. Appl. Phys. A 124, 152 (2018). https://doi.org/10.1007/s00339-018-1583-8

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