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Fabrication and mechanical properties of triply period minimal surface porous alumina ceramics based on Digital Light Processing 3D printing technology

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Abstract

Digital Light Processing (DLP) was used to prepare porous alumina ceramics. By comparing rheological and curing properties of slurries with different solid content, alumina slurries with high solid content were proposed. The green bodies were sintered in an air atmosphere after a nitrogen-air double-step debinding, and the relative density of alumina ceramics prepared by a slurry of 72.5 wt.% solid content reached 96%. In addition, three kinds (Gyroid, Diamond, and F-RD) of triply period minimal surface (TPMS) structural models with different volume fractions were established through implicit functions and simulated in Comsol. The simulation results showed that the Gyroid structure has a higher compression property than the other two structures under the same ceramic volume fraction. The TPMS structural alumina green bodies were sintered after DLP printing. The maximum compressive strength of the Gyroid structure with 60% ceramic volume fraction reached 27.42 MPa.

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Commercial software COMSOL Multiphysics®

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Acknowledgements

The authors would like to acknowledge the support of the Advanced Ceramics Institute of Zibo, the National Key Research and Development Plan.

Funding

This work was supported by the National Key Research and Development Plan (2021YFB3703100), the Hubei High Value Patent Cultivation Project (2021pm0012), the National Natural Science Foundation of China (U1806221, 51672198), the Innovation and Development Project of Zibo City (2017CX01A022), the Instruction & Development Project for National Funding Innovation Demonstration Zone of Shandong Province (2017-41-1, 2017-41-3, 2018ZCQZB01, 2019ZCQZB03), the Central Guiding Local Science and Technology Development Special Funds (2060503), and the Key Research & Design Program of Shandong Province (2019GGX102011).

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All authors contributed to the study conception and design. Z. Zhang conducted experiments with the guidance of K. Liu; The manuscript was written by Z. Zhang, K. Liu, and Y. Du. All authors evaluated the conclusions of the manuscript and approved it.

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Correspondence to Yanying Du.

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Liu, K., Zhang, Z., Sun, H. et al. Fabrication and mechanical properties of triply period minimal surface porous alumina ceramics based on Digital Light Processing 3D printing technology. Int J Adv Manuf Technol (2023). https://doi.org/10.1007/s00170-023-11164-z

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