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Equipment for Environmental Radioactivity Measurement: Calibration and Traceability

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Abstract

Radiation level and activity concentration of radioisotopes present in the earth’s environment can be detected and measured by specific instruments based on several detection techniques. The environmental radioactivity monitoring and measurement instruments commonly use gaseous ionization chamber (GM Tube), liquid or solid scintillation medium [LSC, NaI(Tl), ZnS(Ag)], semi-conductor (HPGe, PIPS), or their combination as detection methods. These instruments should be capable of measuring trace levels of radionuclides present in the environmental matrices with utmost accuracy. In the last few decades, organizations like ISO, IAEA, and BIPM have taken several measures to bring conformity in measurement through proper certification and QC mechanisms which are recognized worldwide. It is safely assumed (and often demonstrated) by an instrument manufacturer that a new instrument is calibrated as per established norms. It initially behaves according to the specifications; however, its capabilities gradually vary with time due to mechanical deterioration, dust, moisture, chemicals, etc. present in the operating environment. These deviations from standard specifications depend upon the frequency of usage and the severity of the operating conditions and are expected and acceptable within documented limits. A recalibration of the instrument becomes necessary when these limits are breached and the results are no more acceptable. Calibration of environmental radioactivity detection and measurement instruments, using certified standard radioactive sources or certified reference materials, is of paramount importance, as it has a direct impact on the health of humans, environment, and non-human biota. In addition, these sources must be traceable with an unbroken chain of measurements to the SI (BIPM) via international bodies like NIST, ILAC-MRA, or National Metrological Institutes/Laboratories.

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Abbreviations

AFRAC:

African accreditation cooperation

ALARA:

As low as reasonably achievable

ALMERA:

Analytical laboratories for the measurement of environmental radioactivity

APAC:

Asia Pacific accreditation cooperation incorporated

ARAC:

Arab accreditation cooperation

BARC:

Bhabha atomic research centre

BIPM:

International bureau of weights and measures

Bq:

Becquerel

BRIT:

Board of radiation & isotope technology,

CGPM:

General conference on weight and measures

CIPM:

International committee for weights and measures

CMI:

Czech metrology institute, Czech Republic

Cps/cpm:

Counts per second/minute

CRM:

Certified reference material

Dpm:

Disintegration per minute

EA:

European cooperation accreditation

EMR:

Electromagnetic radiation

ESL:

Environmental survey laboratory

eV:

Electron volt

FWHM:

Full-width at half-maximum

GM:

Geiger-Muller

GUM:

Guide to the expression of uncertainty in measurement

HPGe:

High purity germanium (detector)

IAAC:

Inter American accreditation cooperation

IAEA:

International atomic energy agency

IAF:

International accreditation forum

ICRP:

International commission on radiation protection

IEC:

International electrotechnical commission

ILAC:

International laboratory accreditation cooperation

ISO:

International standards organization

keV:

Kilo electron volt

LEA:

The radioactivity standards laboratory - laboratoire d’Etalons d’Activité), France

LSA:

Liquid scintillation analysis

LSC:

Liquid scintillation counting

MDL:

Minimum detectable limit

MeV:

Mega electron volt

MRA:

Mutual recognition arrangement

mSv:

Milli Sievert

NaI:

Sodium iodide

NBR:

Natural background radiation

NCRP:

National commission on radiation protection and measurements

NIST:

National institute of science and technology, USA

NML/NMI:

National metrology laboratory/institute

NPL:

National physical laboratory, United Kingdom

NPP:

Nuclear power plant

PMT:

Photo multiplier tube

PSDL:

Primary standard dosimetry laboratory

PTB:

Physicalish-Technishe- Bundesanstalt, Germany

QC:

Quality control

SI:

International system of units

SRM:

Standard reference material (NIST)

SSDL:

Secondary standard dosimetry laboratory

Sv:

Sievert

TLD:

Thermo-luminescent dosimeter

UKAS:

United Kingdom accreditation service

USNRC:

United States nuclear regulatory commission

WHO:

World Health Organization

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Acknowledgments

Authors would like to thank Dr. D. K. Aswal, Director, Health, Safety, and Environment Group (HS&EG), BARC for taking keen interest on the subject and providing constant help and guidance throughout the preparation of this chapter. We would also like to thank our colleagues from Bhabha Atomic Research Centre (BARC) who provided insight into several topics through discussion and review.

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Correspondence to A. Vinod Kumar .

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© 2023 Springer Nature Singapore Pte Ltd.

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Mishra, M.K., Kumar, A.V. (2023). Equipment for Environmental Radioactivity Measurement: Calibration and Traceability. In: Aswal, D.K., Yadav, S., Takatsuji, T., Rachakonda, P., Kumar, H. (eds) Handbook of Metrology and Applications. Springer, Singapore. https://doi.org/10.1007/978-981-99-2074-7_118

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