Skip to main content

Microstructural Properties of Polymer-Modified Self-Healing Concrete Using Scanning Electron Microscopy and X-ray Diffraction

  • Conference paper
  • First Online:
Sustainable Construction Materials

Part of the book series: Lecture Notes in Civil Engineering ((LNCE,volume 194))

  • 522 Accesses

Abstract

This study aims to study the microstructural properties of polymer-modified self-healing concrete using scanning electron microscopy (SEM) and X-ray diffraction (XRD) tests. Until recent years, the mechanical properties of concrete have been studied extensively and these properties alone could not help to examine the microstructure of cement paste. Thus, SEM and XRD were employed to study the microstructural changes in polymer-modified concrete (PMC) in the presence of super-absorbent polymer (SAP) and control concrete (CC) before self-healing. The result of this analysis revealed the presence of unhydrated cement particles trapped within the film made by SAP in PMC when compared to CC. The compressive strength of PMC after 28 days of self-healing was slightly more than that of CC, showing that the SAP has speeded the rate of hydration during the self-healing phase. This improvement in the value could be due to the active participation of unhydrated cement particles from PMC.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 299.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 379.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 379.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Manoj Kumaar C, Mageswari M (2021) Incorporation of nanocatalyst and its behaviour in green concrete structures: mechanical and microstructural study. Appl Nanosci (Switzerland), no. 0123456789

    Google Scholar 

  2. de Rooij M, Schlangen E, De Belie N, Van Tittelboom K (2013) Self-healing phenomena in cement-based materials, vol. 11. Springer

    Google Scholar 

  3. Kumaar MC, Mageswari M (2019) Recovery of mechanical properties of self healing concrete using super absorbent polymer (SAP). Int J Civil Eng Technol 10(2):202–210

    Google Scholar 

  4. Iffat S, Manzur T, Noor MA (2015) Super absorbent polymer in concrete as internal curing material. In: UKIERI concrete congress—concrete research driving profit and sustainability, no. November, pp 1632–1643

    Google Scholar 

  5. Ho H-L, Huang R, Lin W-T, Cheng A (Jan. 2018) Pore-structures and durability of concrete containing pre-coated fine recycled mixed aggregates using pozzolan and polyvinyl alcohol materials. Constr Build Mater 160:278–292

    Google Scholar 

  6. Qureshi T, Kanellopoulos A, Al-Tabbaa A (Dec. 2018) Autogenous self-healing of cement with expansive minerals-I: Impact in early age crack healing. Constr Build Mater 192:768–784

    Google Scholar 

  7. Qureshi T, Kanellopoulos A, Al-Tabbaa A (Jan. 2019) Autogenous self-healing of cement with expansive minerals-II: Impact of age and the role of optimised expansive minerals in healing performance. Constr Build Mater 194:266–275

    Google Scholar 

  8. Manoj Kumaar C, Mageswari M (2021) Thermal analysis on self-healing concrete using polyvinyl alcohol. Int J Ambient Energy 42(2):220–226

    Google Scholar 

  9. Wang Z, Yu J, Li G, Zhang M, Leung CKY (Jul. 2019) Corrosion behavior of steel rebar embedded in hybrid CNTs-OH/polyvinyl alcohol modified concrete under accelerated chloride attack. Cement Concr Compos 100:120–129

    Google Scholar 

  10. Paiva H, Silva AS, Velosa A, Cachim P, Ferreira VM (2017) Microstructure and hardened state properties on pozzolan-containing concrete. Constr Build Mater 140:374–384

    Article  Google Scholar 

  11. Chindasiriphan P, Yokota H, Pimpakan P (2020) Effect of fly ash and superabsorbent polymer on concrete self-healing ability. Constr Build Mater 233:116975

    Google Scholar 

  12. Zhou J, Ye G, Van Breugel K (2016) Cement hydration and microstructure in concrete repairs with cementitious repair materials. Constr Build Mater 112:765–772

    Article  Google Scholar 

  13. Blaiszik B (2010) Self-healing polymers and composites. Annual Rev Mater Res, no. October 2015, pp 179–211

    Google Scholar 

  14. Sclofani DAS, Contrafatto L (2013) Experimental behaviour of polyvinyl-alcohol modified concrete. Adv Mater Res 687(July):155–160

    Article  Google Scholar 

  15. Li G, Huang X, Lin J, Jiang X, Zhang X (2019) Activated chemicals of cementitious capillary crystalline waterproofing materials and their self-healing behaviour. Constr Build Mater 200:36–45

    Google Scholar 

  16. Sidiq A, Gravina RJ, Setunge S, Giustozzi F (2019) Microstructural analysis of healing efficiency in highly durable concrete. Constr Build Mater 215:969–983

    Google Scholar 

Download references

Acknowledgements

The authors would like to thank Sathyabama Institute of Science and Technology for providing facilities to carry out the casting, curing and performing compression tests. The authors would also like to thank the Department of Chemistry, Indian Institute of Technology, Madras for helping to carry out the XRD analysis and Nanotechnology Research Centre, SRM Institute of Science and Technology, for carrying out the SEM analysis.

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2022 The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd.

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Manoj Kumaar, C., Mageswari, M. (2022). Microstructural Properties of Polymer-Modified Self-Healing Concrete Using Scanning Electron Microscopy and X-ray Diffraction. In: Satyanarayanan, K.S., Seo, HJ., Gopalakrishnan, N. (eds) Sustainable Construction Materials. Lecture Notes in Civil Engineering, vol 194. Springer, Singapore. https://doi.org/10.1007/978-981-16-6403-8_24

Download citation

  • DOI: https://doi.org/10.1007/978-981-16-6403-8_24

  • Published:

  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-16-6402-1

  • Online ISBN: 978-981-16-6403-8

  • eBook Packages: EngineeringEngineering (R0)

Publish with us

Policies and ethics