Abstract
This chapter introduces the basic concepts of electron microscopy, which comprises an extensive toolbox for characterizing the size, three-dimensional shape, composition, and crystal structure of nanoparticles, nanoparticle superstructures and nanostructured materials.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Williams, D.B., Carter, C.B.: Transmission Electron Microscopy—A Textbook for Materials Science, 2nd edn. Springer, USA (2009)
van Tendeloo, G., van Dyck, D., Pennycook, S.J. (eds.): Handbook of Nanoscopy. Wiley-VCH, Weinheim (2012)
Yalcin, A.O., Fan, Z., de Nijs, B., Tichelaar, F.D., van Blaaderen, A., Vanmaekelbergh, D., van Huis, M.A., Zandbergen, H.W.: unpublished results
Velikov, K.P., van Blaaderen, A.: Synthesis and characterization of monodisperse core-shell colloidal spheres of Zinc Sulfide and Silica. Langmuir 17, 4779–4786 (2001)
Bals, S., Casavola, M., van Huis, M.A., van Aert, S., Batenburg, K.J., van Tendeloo, G., Vanmaekelbergh, D.: 3D atomic imaging of colloidal core-shell nanocrystals. Nano Lett. 11, 3420–3424 (2011)
Lenders, J., Dey, A., Friedrich, H., de With, G., Sommerdijk, N.: unpublished results
Friedrich, H., de Jongh, P.E., Verkleij, A.J., de Jong, K.P.: Electron tomography for heterogeneous catalysts and related nanostructured materials. Chem. Rev. 109, 1613–1629 (2009)
Goris, B., van Huis, M.A., Bals, S., Zandbergen, H.W., Manna, L., Van Tendeloo, G.: Thermally induced structural and morphological changes of CdSe/CdS octapods. Small 8, 937–942 (2012)
Friedrich, H., Gommes, C.J., Overgaag, K., Meeldijk, J.D., Evers, W.H., de Nijs, B., Boneschanscher, M.P., de Jongh, P.E., Verkleij, A.J., de Jong, K.P., van Blaaderen, A., Vanmaekelbergh, D.: Quantitative structural analysis of binary nanocrystal superlattices by electron tomography. Nano Lett. 9, 2719–2724 (2009)
Zečević, J., Gommes, C.J., Friedrich, H., de Jongh, P.E., de Jong, K.P.: Mesoporosity of Zeolite Y: quantitative three-dimensional study by image analysis of electron tomograms. Angew. Chem. Int. Ed. 51, 4213–4217 (2012)
Midgley, P.A., Dunin-Borkowski, R.E.: Electron tomography and holography in materials science. Nat. Mater. 8, 271–280 (2009)
Friedrich, H., McCartney, M.R., Buseck, P.R.: Comparison of intensity distributions in tomograms from BF TEM, ADF STEM, HAADF STEM, and calculated tilt series. Ultramicroscopy 106, 18–27 (2005)
Van Tendeloo, G., Bals, S., Van Aert, S., Verbeeck, J., Van Dyck, D.: Advanced electron microscopy for advanced materials. Adv. Mater. 24, 5655–5675 (2012)
van Huis, M.A., Figuerola, A., Fang, C.M., Béché, A., Zandbergen, H.W., Manna, L.: Chemical transformation of Au-tipped CdS nanorods into AuS/Cd core/shell particles by electron beam irradiation. Nano Lett. 11, 4555–4561 (2011)
Miszta, K., Dorfs, D., Genovese, Al, Kim, M.R., Manna, L.: Cation exchange reactions in colloidal branched nanocrystals. ACS Nano 5, 7176–7183 (2011)
Friedrich, H., Frederik, P.M., de With, G., Sommerdijk, N.A.J.M.: Imaging self-assembled structures: the interpretation of TEM and cryo-TEM images. Angew. Chem. Int. Ed. 49, 7850–7858 (2010)
Cui, H., Hodgdon, T.K., Kaler, E.W., Abezgauz, L., Danino, D., Lubovsky, M., Talmon, Y., Pochan, D.J.: Elucidating the assembled structure of amphiphiles in solution via cryogenic transmission electron microscopy. Soft Matter 3, 945–955 (2007)
Simonsen, S.B., Chorkendorff, I., Dahl, S., Skoglundh, M., Sehested, J., Helveg, S.: Direct observations of oxygen-induced platinum nanoparticle ripening studied by in situ TEM. J. Am. Chem. Soc. 132, 7968–7975 (2010)
Young, N.P., van Huis, M.A., Zandbergen, H.W., Xu, H., Kirkland, A.I.: Transformation of gold nanoparticles investigated using variable temperature high-resolution transmission electron microscopy. Ultramicroscopy 110, 506–516 (2010)
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2014 Springer-Verlag Berlin Heidelberg
About this chapter
Cite this chapter
van Huis, M.A., Friedrich, H. (2014). Electron Microscopy Techniques. In: de Mello Donegá, C. (eds) Nanoparticles. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-44823-6_7
Download citation
DOI: https://doi.org/10.1007/978-3-662-44823-6_7
Published:
Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-662-44822-9
Online ISBN: 978-3-662-44823-6
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)