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Optical Characterization of Thin Films by Means of Imaging Spectroscopic Reflectometry

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Optical Characterization of Thin Solid Films

Part of the book series: Springer Series in Surface Sciences ((SSSUR,volume 64))

Abstract

This chapter focuses on optical characterization of thin films by means of non-microscopic imaging spectroscopic reflectometry. This technique is primarily intended for characterization of thin films with an area non-uniformity in their optical properties. An advantage of the technique is the possibility to measure along a relatively large area of the measured films. The motivation for development and exploitation of this technique is also discussed. Essential features and implementation of the technique are given, as well as the basic experimental set-up of imaging spectroscopic reflectometers and the way the experimental data are obtained. The data processing methods are classified based on the purpose of the thin film measurement. Furthermore, this chapter presents examples of results of imaging spectroscopic reflectometry in the field of thin films. At the end of the chapter, potential applications of imaging spectroscopic reflectometry in other tasks are also briefly mentioned.

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Notes

  1. 1.

    When the gradient of thickness non-uniformity is so high (e.g. edges of thin films) that the film cannot be considered uniform within those areas, it is possible to perform correction leading to the correct results.

References

  1. H.G. Tompkins, W.A. McGahan, Spectroscopic Ellipsometry and Reflectometry: A User’s Guide (Wiley, 1999). Google-Books-ID: W35tQgAACAAJ

    Google Scholar 

  2. H.G. Tompkins, E.A. Irene, Handbook Of Ellipsometry (William Andrew Publisher; Springer, Norwich, NY; Heidelberg, Germany, 2005). http://www.books24x7.com/marc.asp?bookid=32277. OCLC: 310147997

  3. M. Quinten, A Practical Guide to Optical Metrology for Thin Films (Wiley-VCH Verlag GmbH & Co, KGaA, 2012)

    Google Scholar 

  4. M.I. Török, Optica Acta: Int. J. Opt. 32(4), 479 (1985). https://doi.org/10.1080/713821745

  5. T. Pisarkiewicz, T. Stapinski, H. Czternastek, P. Rava, J. Non-Cryst. Solids 137, 619 (1991). https://doi.org/10.1016/S0022-3093(05)80194-2, http://www.sciencedirect.com/science/article/pii/S0022309305801942

  6. T. Pisarkiewicz, J. Phys. D: Appl. Phys. 27(1), 160 (1994). https://doi.org/10.1088/0022-3727/27/1/025, http://stacks.iop.org/0022-3727/27/i=1/a=025

  7. E. Márquez, J.M. González-Leal, R. Jiménez-Garay, S.R. Lukic, D.M. Petrovic, J. Phys. D: Appl. Phys. 30(4), 690 (1997). https://doi.org/10.1088/0022-3727/30/4/026, http://stacks.iop.org/0022-3727/30/i=4/a=026

  8. E. Márquez, P. Nagels, J.M. González-Leal, A.M. Bernal-Oliva, E. Sleeckx, R. Callaerts, Vacuum 52(1–2), 55 (1999). https://doi.org/10.1016/S0042-207X(98)00233-4, http://www.sciencedirect.com/science/article/pii/S0042207X98002334

  9. D. Nečas, I. Ohlídal, D. Franta, J. Opt. A: Pure Appl. Opt. 11(4), 045202 (2009). https://doi.org/10.1088/1464-4258/11/4/045202, http://iopscience.iop.org/1464-4258/11/4/045202

  10. L. Abel-Tiberini, F. Lemarquis, M. Lequime, Appl. Opt. 45(7), 1386 (2006). https://doi.org/10.1364/AO.45.001386

  11. D. Nečas, I. Ohlídal, D. Franta, V. Čudek, M. Ohlídal, J. Vodák, L. Sládková, L. Zajíčková, M. Eliáš, F. Vižd’a, Thin Solid Films 571, Part 3, 573 (2014). https://doi.org/10.1016/j.tsf.2013.12.036

  12. J. Spousta, M. Urbánek, R. Chmelík, J. Jiruše, J. Zlámal, K. Navrátil, A. Nebojsa, T. Šikola, Surf. Interface Anal. 34(1), 664 (2002). https://doi.org/10.1002/sia.1383, http://onlinelibrary.wiley.com/doi/10.1002/sia.1383/abstract

  13. M. Urbánek, J. Spousta, K. Navrátil, R. Szotkowski, R. Chmelík, M. Buček, T. Šikola, Surf. Interface Anal. 36(8), 1102 (2004). https://doi.org/10.1002/sia.1850, http://onlinelibrary.wiley.com/doi/10.1002/sia.1850/abstract

  14. I. Ohlídal, D. Nečas, D. Franta, V. Buršíková, Diam. Relat. Mater. 18(2–3), 364 (2009). https://doi.org/10.1016/j.diamond.2008.09.003, http://www.sciencedirect.com/science/article/pii/S0925963508004342

  15. D. Nečas, D. Franta, V. Buršíková, I. Ohlídal, Thin Solid Films 519(9), 2715 (2011). https://doi.org/10.1016/j.tsf.2010.12.065

  16. D. Nečas, I. Ohlídal, D. Franta, J. Opt. 13(8), 085705 (2011). https://doi.org/10.1088/2040-8978/13/8/085705, http://stacks.iop.org/2040-8986/13/i=8/a=085705

  17. L. Stiblert, T. Sandström, Le J. de Phys. Colloq. 44(C10) (1983). https://doi.org/10.1051/jphyscol:19831016

  18. D. Beaglehole, Review of Scientific Instruments 59(12), 2557 (1989). https://doi.org/10.1063/1.1139897

  19. G. Jin, P. Tengvall, I. Lundström, H. Arwin, Analytical Biochemistry (1995), p. 69. https://doi.org/10.1006/abio.1995.9959

  20. H. Arwin, Thin Solid Films 313–314, 764 (1998). https://doi.org/10.1016/S0040-6090(97)00993-0, http://www.sciencedirect.com/science/article/pii/S0040609097009930

  21. L. Asinovski, D. Beaglehole, M.T. Clarkson, phys. status solidi (a) 205(4), 764 (2008). https://doi.org/10.1002/pssa.200777855, http://onlinelibrary.wiley.com/doi/10.1002/pssa.200777855/abstract

  22. U. Wurstbauer, C. Röling, U. Wurstbauer, W. Wegscheider, M. Vaupel, P.H. Thiesen, D. Weiss, Appl. Phys. Lett. 97(23), 231901 (2010). https://doi.org/10.1063/1.3524226, http://scitation.aip.org/content/aip/journal/apl/97/23/10.1063/1.3524226

  23. M. Fried, G. Juhász, C. Major, P. Petrik, O. Polgár, Z. Horváth, A. Nutsch, Thin Solid Films 519(9), 2730 (2011). https://doi.org/10.1016/j.tsf.2010.12.067, http://www.sciencedirect.com/science/article/pii/S0040609010016974

  24. G. Jin, Y.H. Meng, L. Liu, Y. Niu, S. Chen, Q. Cai, T.J. Jiang, Thin Solid Films 519(9), 2750 (2011). https://doi.org/10.1016/j.tsf.2010.12.175, http://www.sciencedirect.com/science/article/pii/S0040609010018249

  25. P.G. Ellingsen, M.B. Lilledahl, L.M.S. Aas, C.d.L. Davies, M. Kildemo, J. Biomed. Opt. 16(11), 116002 (2011). https://doi.org/10.1117/1.3643721

  26. K. Mahmoud, S. Park, S.N. Park, D.H. Lee, Metrologia 51(6), S293 (2014). https://doi.org/10.1088/0026-1394/51/6/S293. WOS:000345426000008

  27. K. Mahmoud, S. Park, S.N. Park, D.H. Lee, in Fifth Asia-Pacific Optical Sensors Conference, vol. 9655, ed. by B. Lee, S.B. Lee, Y. Rao (Spie-Int Soc Optical Engineering, Bellingham, 2015), vol. 9655, p. 965503. WOS:000358602400002

    Google Scholar 

  28. K. Kim, S. Kim, S. Kwon, H.J. Pahk, Int. J. Precis. Eng. Manuf. 15(9), 1817 (2014). https://doi.org/10.1007/s12541-014-0534-3

  29. M. Ohlídal, I. Ohlídal, D. Franta, T. Králík, M. Jákl, M. Eliáš, Surf. Interface Anal. 34(1), 660 (2002). https://doi.org/10.1002/sia.1382, http://onlinelibrary.wiley.com/doi/10.1002/sia.1382/abstract

  30. M. Ohlídal, I. Ohlídal, P. Klapetek, M. Jákl, V. Čudek, M. Eliáš, Jpn. J. Appl. Phys. 42(7S), 4760 (2003). https://doi.org/10.1143/JJAP.42.4760, http://iopscience.iop.org/1347-4065/42/7S/4760

  31. I. Ohlídal, M. Ohlídal, P. Klapetek, V. Čudek, M. Jákl, in Wave-Optical Systems Engineering II (2004), pp. 260–271. https://doi.org/10.1117/12.509628, http://dx.doi.org/10.1117/12.509628

  32. M. Ohlídal, V. Čudek, I. Ohlídal, P. Klapetek, in Proceedings of SPIE, ed. by C. Amra, N. Kaiser, H.A. Macleod (2005), vol. 5963, pp. 596, 329–596, 329–9. https://doi.org/10.1117/12.625380, http://proceedings.spiedigitallibrary.org/proceeding.aspx?articleid=876920

  33. M. Ohlídal, I. Ohlídal, P. Klapetek, D. Nečas, V. Buršíková, Diam. Relat. Mater. 18(2–3), 384 (2009). https://doi.org/10.1016/j.diamond.2008.10.012

  34. M. Ohlídal, I. Ohlídal, E-J. Surf. Sci. Nanotechnol. 7, 409 (2009). https://doi.org/10.1380/ejssnt.2009.409

  35. I. Ohlídal, M. Ohlídal, D. Nečas, D. Franta, V. Buršíková, Thin Solid Films 519(9), 2874 (2011). https://doi.org/10.1016/j.tsf.2010.12.069, http://ww.sciencedirect.com/science/article/pii/S0040609010016998

  36. M. Ohlídal, I. Ohlídal, P. Klapetek, D. Nečas, A. Majumdar, Meas. Sci. Technol. 22(8), 085104 (2011). https://doi.org/10.1088/0957-0233/22/8/085104, http://iopscience.iop.org/0957-0233/22/8/085104

  37. D. Nečas, V. Čudek, J. Vodák, M. Ohlídal, P. Klapetek, J. Benedikt, K. Rügner, L. Zajíčková, Meas. Sci. Technol. 25(11), 115201 (2014). https://doi.org/10.1088/0957-0233/25/11/115201

  38. D. Nečas, I. Ohlídal, D. Franta, M. Ohlídal, V. Čudek, J. Vodák, Appl. Opt. 53(25), 5606 (2014). https://doi.org/10.1364/AO.53.005606

  39. J. Schaefer, J. Hnilica, J. Sperka, A. Quade, V. Kudrle, R. Foest, J. Vodak, L. Zajickova, Surf. Coat. Technol. 295, 112 (2016). https://doi.org/10.1016/j.surfcoat.2015.09.047. WOS:000376834700017

  40. D. Nečas, I. Ohlídal, D. Franta, M. Ohlídal, J. Vodák, J. Opt. 18(1), 015401 (2016). https://doi.org/10.1088/2040-8978/18/1/015401, http://stacks.iop.org/2040-8986/18/i=1/a=015401

  41. J. Vodák, D. Nečas, M. Ohlídal, I. Ohlídal, Measurement Science and Technology 28(2), 025205 (2017). https://doi.org/10.1088/1361-6501/aa5534, http://stacks.iop.org/0957-0233/28/i=2/a=025205

  42. P. Hariharan, Optical Interferometry (Academic Press, 2003). Google-Books-ID: EGdMO3rfVj4C

    Google Scholar 

  43. D. Franta, I. Ohlídal, Acta Phys. Slovaca 50(4), 411 (2000)

    Google Scholar 

  44. A. Majumdar, J. Schäfer, P. Mishra, D. Ghose, J. Meichsner, R. Hippler, Surf. Coat. Technol. 201(14), 6437 (2007). https://doi.org/10.1016/j.surfcoat.2006.12.011, http://www.sciencedirect.com/science/article/pii/S0257897206014800

  45. D. Franta, D. Nečas, L. Zajíčková, Opt. Express 15(24), 16230 (2007). https://doi.org/10.1364/OE.15.016230, https://www.osapublishing.org/oe/abstract.cfm?uri=oe-15-24-16230

  46. D. Franta, D. Nečas, L. Zajíčková, I. Ohlídal, Thin Solid Films 571, 490 (2014). https://doi.org/10.1016/j.tsf.2014.03.059

  47. D. Nečas, J. Vodák, I. Ohlídal, M. Ohlídal, A. Majumdar, L. Zajíčková, Appl. Surf. Sci. 350, 149 (2015). https://doi.org/10.1016/j.apsusc.2015.01.093, http://www.sciencedirect.com/science/article/pii/S016943321500118X

  48. V. Holý, K. Wolf, M. Kastner, H. Stanzl, W. Gebhardt, J. Appl. Crystallogr. 27(4), 551 (1994). https://doi.org/10.1107/S0021889894000208, http://scripts.iucr.org/cgi-bin/paper?wi0141

  49. D. Franta, I. Ohlídal, P. Klapetek, A. Montaigne-Ramil, A. Bonanni, D. Stifter, H. Sitter, J. Appl. Phys. 92(4), 1873 (2002). https://doi.org/10.1063/1.1489068, http://aip.scitation.org/doi/10.1063/1.1489068

  50. D. Franta, D. Nečas, L. Zajíčková, Thin Solid Films 534, 432 (2013). https://doi.org/10.1016/j.tsf.2013.01.081

  51. D. Franta, D. Nečas, L. Zajíčková, I. Ohlídal, J. Stuchlík, D. Chvostová, Thin Solid Films 539, 233 (2013). https://doi.org/10.1016/j.tsf.2013.04.012

  52. I. Ohlídal, D. Necas, D. Franta, phys. status solidi (c) 5(5), 1399 (2008). https://doi.org/10.1002/pssc.200777769, http://onlinelibrary.wiley.com/doi/10.1002/pssc.200777769/abstract

  53. J.A. Ogilvy, H.M. Merklinger, J. Acoust. Soc. Am. 90(6), 3382 (1991). https://doi.org/10.1121/1.401410, http://asa.scitation.org/doi/abs/10.1121/1.401410

  54. D. Franta, I. Ohlídal, P. Klapetek, A. Montaigne-Ramil, A. Bonanni, D. Stifter, H. Sitter, Acta Phys. Slovaca 53(2), 95 (2003)

    Google Scholar 

  55. S. Adachi, Optical properties of crystalline and amorphous semiconductors: materials and fundamental principles (Boston: Kluwer Academic Publishers, 1999). http://trove.nla.gov.au/version/39699241

  56. D. Franta, D. Nečas, I. Ohlídal, A. Giglia, in Optical Systems Design 2015: Optical Fabrication, Testing, and Metrology V, vol. 9628 (2015), vol. 9628, pp. 96,281U–96,281U–12. https://doi.org/10.1117/12.2190104

  57. J. Vodák, D. Nečas, D. Pavliňák, J.M. Macak, T. Řičica, R. Jambor, M. Ohlídal, Appl. Surf. Sci. 396, 284 (2017). https://doi.org/10.1016/j.apsusc.2016.10.122

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Acknowledgements

The work on this chapter was supported by the project LO1411 (NPU I) funded by Ministry of Education Youth and Sports of the Czech Republic. Presented reflectometers were realized using the facilities of Institute of Physical Engineering, Brno University of Technology.

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Ohlídal, M., Vodák, J., Nečas, D. (2018). Optical Characterization of Thin Films by Means of Imaging Spectroscopic Reflectometry. In: Stenzel, O., Ohlídal, M. (eds) Optical Characterization of Thin Solid Films. Springer Series in Surface Sciences, vol 64. Springer, Cham. https://doi.org/10.1007/978-3-319-75325-6_5

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