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Introduction to Food Analysis

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Food Analysis

Part of the book series: Food Science Text Series ((FSTS))

Abstract

Food scientists and technologists determine the chemical composition and physical characteristics of foods routinely as part of their quality management, product development, or research activities. Consumer, government, and food industry concern for food quality and safety has increased the importance of analyses that determine composition and critical product characteristics. To successfully base decisions on results of any analysis, one must correctly conduct all three major steps in the analysis: (1) select and prepare samples, (2) perform the assay, and (3) calculate and interpret the results. The choice of analysis method is usually based on the objective of the analysis, characteristics of the method itself, and the food matrix involved.Validation of the method is important, as is the use of standard reference materials to ensure quality results. Rapid methods used for quality assessment in a production facility may be less accurate but much faster than official methods used for nutrition labeling. Endorsed methods for the chemical analyses of foods have been compiled and published by various scientific organizations. Such official methods allow for comparison of results between different laboratories and for evaluation of new or more rapid procedures. This chapter provides introductory information on the topics summarized above that lays the foundation before covering various specific methods of food analysis in other chapters.

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References

  1. McGorrin RJ (2009) One hundred years of progress in food analysis. J. Agric. Food Chem. 57(18):8076–8088

    Article  CAS  PubMed  Google Scholar 

  2. Cifuentes A (2012) Food analysis: Present, future, and foodomics. ISRN Analytical Chemistry. Article ID 801607

    Google Scholar 

  3. Spence JT (2006) Challenges related to the composition of functional foods. J Food Compost Anal 19 Suppl 1: S4–S6

    Article  Google Scholar 

  4. Alli I (2016) Food quality assurance: principles and practices, 2nd edn. CRC, Boca Raton, FL

    Google Scholar 

  5. Vasconcellos JA (2004) Quality assurances for the food industry: a practical approach. CRC, Boca Raton, FL

    Google Scholar 

  6. Pearson D (1973) Introduction – some basic principles of quality control, Ch. 1. In: Laboratory techniques in food analysis. Wiley, New York, pp 1–26

    Google Scholar 

  7. Pomeranz Y, Meloan CE (1994) Food analysis: theory and practice, 3rd edn. Chapman & Hall, New York

    Google Scholar 

  8. Cruz RMS, Khmelinskii I, Vieira M (2014) Methods in food analysis. CRC, Boca Raton, FL

    Google Scholar 

  9. Nollett LML (2004) Handbook of Food Analysis, 2nd edn. vol 1: physical characterization and nutrient analysis, vol 2: residues and other food component analysis. CRC, Boca Raton, FL

    Google Scholar 

  10. Nollett LML, Toldra F (2012) Food analysis by HPLC, 3rd edn. CRC, Boca Raton, FL

    Book  Google Scholar 

  11. Ötleş S (2008) Handbook of food analysis instruments. CRC, Boca Raton, FL

    Google Scholar 

  12. Ötleş S (2011) Methods of analysis of food components and additives, 2nd edn. CRC, Boca Raton, FL

    Book  Google Scholar 

  13. Latimer GW, Jr (1997) Check sample programs keep laboratories in sync. Inside Lab Manage 1(4): 18–20

    Google Scholar 

  14. Ambrus A (2008) Quality assurance, Ch. 5. In: Tadeo JL (ed) Analysis of pesticides in food and environmental samples. CRC, New York, p 145

    Google Scholar 

  15. ISO/IEC (2010) ISO/IEC 17025:2005. General requirements for the competence of testing and calibration laboratories (last review in 2010). http://www.iso.org/iso/home/store/catalogue_tc/catalogue_detail.htm?csnumber=39883

  16. Wetzel DLB, Charalambous G (eds) (1998) Instrumental methods in food and beverage analysis. Elsevier Science, Amsterdam, The Netherlands

    Google Scholar 

  17. Wolf W (1993) In: Methods of analysis for nutrition labeling. AOAC International, Ch 7, pp 115–120, as adapted from W. Ikins, DeVires J, Wolf W, Oles P, Carpenter D, Fraley N, Ngeh-Nwainbi J. The Referee. AOAC International 17(7), pp 1, 6–7

    Google Scholar 

  18. Wolf WR, Andrews KW (1995) A system for defining reference materials applicable to all food matrices. Fresenius J Anal Chem 352:73–76

    Article  CAS  Google Scholar 

  19. Lovett RA (1997) U.S. food label law pushes fringes of analytical chemistry. Inside Lab Manage 1(4): 27–28

    Google Scholar 

  20. Ellis C, Hite D, van Egmond H (1997) Development of methods to test all food matrixes unrealistic, says OMB. Inside Lab Manage 1(8):33–35

    Google Scholar 

  21. DeVries JW, Silvera KR (2001) AACC collaborative study of a method for determining vitamins A and E in foods by HPLC (AACC Method 86–06). Cereal Foods World 46(5):211–215

    CAS  Google Scholar 

  22. Sharpless KE, Greenberg RR, Schantz MM, Welch MJ, Wise SA, Ihnat M (2004) Filling the AOAC triangle with food-matrix standard reference materials. Anal and Bioanal Chem 378:1161–1167

    Article  CAS  Google Scholar 

  23. Wise SA, Sharpless KE, Sander LC, May WE (2004) Standard reference materials to support US regulations for nutrients and contaminants in food and dietary supplements. Accred Qual Assur 9:543–550

    Article  CAS  Google Scholar 

  24. Sharpless KE, Lindstrom RM, Nelson BC, Phinney KW, Rimmer CA, Sander LC, Schantz MM, Spatz RO, Thomas JB, Turk GC, Wise SA, Wood LJ (2010) Preparation and characterization of standard reference material 1849 Infant/adult nutritional formula. 93(4):1262–1274

    CAS  Google Scholar 

  25. Thomas JB, Yen JH, Sharpless KE (2013) Characterization of NIST food-matrix standard reference materials for their vitamin C content. Anal Bioanal Chem 405:4539–4548

    Article  CAS  PubMed  Google Scholar 

  26. AOAC International (2016) Official methods of analysis, 20th edn., 2016 (online). AOAC International, Rockville, MD

    Google Scholar 

  27. AACC International (2010) Approved methods of analysis, 11th edn (online), AACC International, St. Paul, MN

    Google Scholar 

  28. AOCS (2013) Official methods and recommended practices, 6th edn, 3rd printing, American Oil Chemists’ Society, Champaign, IL

    Google Scholar 

  29. Wehr HM, Frank JF (eds) (2004) Standard methods for the examination of dairy products, 17th edn. American Public Health Association, Washington, DC

    Google Scholar 

  30. Rice EW, Baird RB, Eaton AD, Clesceri LS (eds) (2012) Standard methods for the examination of water and wastewater, 22nd edn. American Public Health Association, Washington, DC

    Google Scholar 

  31. U.S. Pharmacopeia (USP) (2016) Food chemicals codex, 10th edn. United Book Press, Baltimore, MD

    Google Scholar 

  32. FDA (2014) CFSAN laboratory quality manual (last updated 12/10/14) http://www.fda.gov/downloads/Food/FoodScienceResearch/UCM216952.pdf

  33. FDA (2016) Elemental analysis manual for food and related products (last updated 1/08/16). http://www.fda.gov/food/foodscienceresearch/laboratorymethods/ucm2006954.htm

  34. FDA (2015) Drug and chemical residue methods (last updated 6/29/15) http://www.fda.gov/Food/FoodScienceResearch/LaboratoryMethods/ucm2006950.htm

  35. FDA (1999) Pesticide analytical manual volume I (PAM), 3rd edn (1994, updated October, 1999). http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/PesticideAnalysisManualPAM/ucm111455.htm

  36. FDA (2002) Pesticide analytical manual volume II (PAM) (updated January, 2002). http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/PesticideAnalysisManualPAM/ucm113710.htm

  37. FDA (2015) Macroanalytical Procedures Manual (last updated 6/05/15) http://www.fda.gov/Food/FoodScienceResearch/LaboratoryMethods/ucm2006953.htm

  38. USDA (2016) Chemistry laboratory guidebook (last updated 6/26/15) http://www.fsis.usda.gov/wps/portal/fsis/topics/science/laboratories-and-procedures/guidebooks-and-methods/chemistry-laboratory-guidebook. Food Safety and Inspection Service, US Department of Agriculture, Washington, DC

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Acknowledgments

The author thanks the numerous former students and others associated with quality assurance in the food industry who reviewed this chapter and contributed ideas for its revision. Special thanks go to the following for their help with specific topics: Chris Fosse (ConAgra Foods) and Ryan Lane (TreeHouse Foods), specifications for semolina; Samantha Park (TreeHouse Foods) and Yuezhen He (former student at Purdue University), quality tests for pasta; Sandy Zinn (General Mills), ISO; Ryan Ellefson (Covance), LIMS; Karen Andrews (USDA), food matrix and standard reference materials; and Julie Culp (General Mills), food analysis linked to consumer demand and government regulations.

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Authors and Affiliations

  1. Department of Food Science, Purdue University, West Lafayette, IN, 47907-2009, USA

    S. Suzanne Nielsen

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  1. S. Suzanne Nielsen
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Correspondence to S. Suzanne Nielsen .

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Editors and Affiliations

  1. Department of Food Science, Purdue University, West Lafayette, IN, USA

    S. Suzanne Nielsen

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Nielsen, S.S. (2017). Introduction to Food Analysis. In: Nielsen, S.S. (eds) Food Analysis. Food Science Text Series. Springer, Cham. https://doi.org/10.1007/978-3-319-45776-5_1

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