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Synthesis of Nanoparticles via Solvothermal and Hydrothermal Methods

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Handbook of Nanoparticles

Abstract

This chapter summarizes the synthesis of various types of nanoparticles as well as surface modifications of nanomaterials using hydrothermal and solvothermal methods. First, the definition, history, instrumentation, and mechanism of hydrothermal and solvothermal methods as well as the important parameters affecting the nucleation and crystal growth of nanomaterials are briefly introduced. Then, the specific hydrothermal and solvothermal methods used to grow oxides; Groups II–VI, III–V, and IV; transitional metals; and metal-organic framework nanoparticles are summarized. Finally, the hydrothermal and solvothermal strategies used for the surface modification of nanomaterials are discussed.

This submission was written by the author(s) acting in his own independent capacity and not on behalf of UT-Battelle, LLC, or its affiliates or successors. All authors make same contribution to this book chapter.

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Abbreviations

AC:

Acetone

BDC:

Terephthalic acid

CTAB:

Cetyltrimethylammonium bromide

HKF:

Helgeson-Kirkham-Flowers

HMDS:

Hexamethyldisiloxane

MOF:

Metal-organic framework

NC:

Nanocrystal

NP:

Nanoparticle

PFTE:

Polytetrafluoroethylene

PVP:

Polyvinylpyrrolidone

SEM:

Scanning electron microscope

SAED:

Selected-area electron diffraction

TEM:

Transmission electron microscope

XRD:

X-ray diffraction

References

  1. K. Byrappa, M. Yoshimura, Handbook of Hydrothermal Technology (William Andrew, Norwich, 2001)

    Google Scholar 

  2. K.F.E. Schafthaul, Gelehrte Anzeigen Bayer. Akad. 20, 557 (1845)

    Google Scholar 

  3. K. Byrappa, T. Adschiri, Progr. Cryst. Growth Character. Mater. 53, 117 (2007)

    Google Scholar 

  4. Z.L. Wang, Adv. Mater. (Weinheim, Germany) 15, 1497 (2003)

    Google Scholar 

  5. H.C. Helgeson, D.H. Kirkham, Am. J. Sci. 274, 1089 (1974)

    Google Scholar 

  6. H.C. Helgeson, D.H. Kirkham, Am. J. Sci. 276, 97 (1976)

    Google Scholar 

  7. H.C. Helgeson, D.H. Kirkham, G.C. Flowers, Am. J. Sci. 281, 1249 (1981)

    Google Scholar 

  8. E.L. Shock, E.H. Oelkers, J.W. Johnson, D.A. Sverjensky, H.C. Helgeson, J. Chem. Soc. Faraday Trans. 88, 803 (1992)

    Google Scholar 

  9. W. Dawson, J. Am. Ceramic Soc. Bull. 67, 1673 (1988)

    Google Scholar 

  10. I. Sunagawa, K. Tsukamoto, K. Maiwa, K. Onuma, Progr. Crystal. Growth Character. Mater. 30, 153 (1995)

    Google Scholar 

  11. B.E. Etschmann, W. Liu, D. Testemale, H. Mueller, N.A. Rae, O. Proux, J.L. Hazemann, J. Brugger, Geochim. Cosmochim. Acta 74, 4723 (2010)

    Google Scholar 

  12. C. Gerardin, M. Haouas, C. Lorentz, F. Taulelle, Magn. Reson. Chem. 38, 429 (2000)

    Google Scholar 

  13. S.R. Higgins, C.M. Eggleston, G. Jordan, K.G. Knauss, C.O. Boro, Mineral. Mag. 62A, 618 (1998)

    Google Scholar 

  14. K. Kawamura, H. Nagayoshi, T. Yao, Anal. Chim. Acta 667, 88 (2010)

    Google Scholar 

  15. J.E. Maslar, W.S. Hurst, W.J. Bowers Jr., J.H. Hendricks, Corrosion (Houston, TX, United States) 58, 739 (2002)

    Google Scholar 

  16. J.E. Maslar, W.S. Hurst, W.J. Bowers, J.H. Hendricks, M.I. Aquino, I. Levin, Appl. Surf. Sci. 180, 102 (2001)

    Google Scholar 

  17. P. Norby, Mater. Sci. Forum 228, 147 (1996)

    Google Scholar 

  18. G.S. Pokrovski, J. Roux, J.L. Hazemann, A.Y. Borisova, A.A. Gonchar, M.P. Lemeshko, Mineral. Mag. 72, 667 (2008)

    Google Scholar 

  19. K. Sue, M. Suzuki, K. Arai, T. Ohashi, H. Ura, K. Matsui, Y. Hakuta, H. Hayashi, M. Watanabe, T. Hiaki, Green Chem. 8, 634 (2006)

    Google Scholar 

  20. T. Andelman, M.C. Tan, R.E. Riman, Mater. Res. Innov. 14, 9 (2010)

    Google Scholar 

  21. T. Adschiri, Y. Hakuta, K. Arai, Ind. Eng. Chem. Res. 39, 4901 (2000)

    Google Scholar 

  22. R.E. Riman, W.L. Suchanek, M.M. Lencka, Ann. Chim. (Paris, France) 27, 15 (2002)

    Google Scholar 

  23. M.M. Lencka, R.E. Riman, J. Am. Ceram. Soc. 76, 2649 (1993)

    Google Scholar 

  24. K.S. Pitzer, J. Phys. Chem. 77, 268 (1973)

    Google Scholar 

  25. L.A. Bromley, AIChE J. 19, 313 (1973)

    Google Scholar 

  26. J.F. Zemaitis Jr., D.M. Clark, M. Rafal, N.C. Scrivner, Handbook of Aqueous Electrolyte Thermodynamics: Theory and Application, 1st edn. (Wiley-AIChE, Hoboken, 1986)

    Google Scholar 

  27. K. Minami, T. Suzuki, T. Aizawa, K. Sue, K. Arai, R.L. Smith Jr., Fluid Phase Equilib. 257, 177 (2007)

    Google Scholar 

  28. A.V. Plyasunov, E.L. Shock, Geochim. Cosmochim. Acta 65, 3879 (2001)

    Google Scholar 

  29. D.A. Sverjensky, E.L. Shock, H.C. Helgeson, Geochim. Cosmochim. Acta 61, 1359 (1997)

    Google Scholar 

  30. T. Adschiri, Y. Hakuta, K. Sue, K. Arai, J. Nanoparticle Res. 3, 227 (2001)

    Google Scholar 

  31. D. Kashchiev, J. Chem. Phys. 76, 5098 (1982)

    Google Scholar 

  32. B. Schoeman, J. Micro. Meso. Mater. 22, 9 (1998)

    Google Scholar 

  33. C.E.A. Kirschhock, R. Ravishankar, P.A. Jacobs, J.A. Martens, J. Phys. Chem. B 103, 11021 (1999)

    Google Scholar 

  34. V. Nikolakis, E. Kokkoli, M. Tirrell, M. Tsapatsis, D.G. Vlachos, Chem. Mater. 12, 845 (2000)

    Google Scholar 

  35. M. Uematsu, E.U. Franck, J. Phys. Chem. Refer. Data 9, 1291 (1981)

    Google Scholar 

  36. S. Yin, Y. Fujishiro, J. Wu, M. Aki, T. Sato, J. Mater. Process. Technol. 137, 45 (2003)

    Google Scholar 

  37. M. Kang, J. Mol. Catal. A: Chem. 197, 173 (2003)

    Google Scholar 

  38. C.-S. Kim, B.K. Moon, J.-H. Park, S.T. Chung, S.-M. Son, J. Crystal Growth 254, 405 (2003)

    Google Scholar 

  39. Y. Zhu, T. Mei, Y. Wang, Y. Qian, J. Mater. Chem. 21, 11457 (2011)

    Google Scholar 

  40. J. Li, Z. Chen, R.J. Wang, D.M. Proserpio, Coord. Chem. Rev. 192, 707 (1999)

    Google Scholar 

  41. K. Han, S. Xia, P. Ma, F. Yan, T. Liu, J. Chem. Thermodyn. 62, 111 (2013)

    Google Scholar 

  42. N.W. Krase, J.B. Goodman, Ind. Eng. Chem. 22, 13 (1930)

    Google Scholar 

  43. A.S. Teja, D. Rosenthal, J. DIPPR Data Ser. 1, 96 (1991)

    Google Scholar 

  44. S.-H. Yu, J. Ceramic Soc. Japan 109, S65 (2001)

    Google Scholar 

  45. Y. Konishi, T. Kawamura, S. Asai, Ind. Eng. Chem. Res. 32, 2888 (1993)

    Google Scholar 

  46. D. Chen, R. Xu, J. Mater. Chem. 8, 965 (1998)

    Google Scholar 

  47. Z.-X. Deng, C. Wang, X.-M. Sun, Y.-D. Li, Inorg. Chem. 41, 869 (2002)

    Google Scholar 

  48. J. Lu, P. Qi, Y. Peng, Z. Meng, Z. Yang, W. Yu, Y. Qian, Chem. Mater. 13, 2169 (2001)

    Google Scholar 

  49. Y. Gao, M. Fan, Q. Fang, W. Han, New J. Chem. 37, 670 (2013)

    Google Scholar 

  50. Z.-Y. Yuan, B.-L. Su, Colloid. Surf. A: Phys. Eng. Aspect. 241, 173 (2004)

    Google Scholar 

  51. A. Nakahira, W. Kato, M. Tamai, T. Isshiki, K. Nishio, H. Aritani, J. Mater. Sci. 39, 4239 (2004)

    Google Scholar 

  52. R. Lu, J. Yuan, H. Shi, B. Li, W. Wang, D. Wang, M. Cao, CrystEngComm 15, 3984 (2013)

    Google Scholar 

  53. M. Safaei, R. Sarraf-Mamoory, M. Rashidzadeh, M. Manteghian, J. Porous Mater. 17, 719 (2010)

    Google Scholar 

  54. G.W. Morey, P. Niggli, J. Am. Chem. Soc. 35, 1086 (1913)

    Google Scholar 

  55. R. Nacken, Chemiker-Zeitung 74, 745 (1950)

    Google Scholar 

  56. R.M. Barrer, Nature 157, 734 (1946)

    Google Scholar 

  57. R.H. Ewell, H. Insley, J. Res. Nat. Bur. Stand. 15, 173 (1935)

    Google Scholar 

  58. S.F. Adams, Econ. Geol. Bull. Soc. Econ. Geol. 15, 623 (1920)

    Google Scholar 

  59. A.C. Walker, J. Am. Ceram. Soc. 36, 250 (1953)

    Google Scholar 

  60. R.M. Barrer, C. Marcilly, J. Chem. Soc. [Section] A: Inorg. Phys. Theor. 2735 (1970)

    Google Scholar 

  61. P.B. Moore, Am. Mineral. 55, 135 (1970)

    Google Scholar 

  62. H.C. Helgeson, Am. J. Sci. 267, 729 (1969)

    Google Scholar 

  63. H.C. Helgeson, R.M. Garrels, F.T. Mackenzie, Geochim. Cosmochim. Acta 33, 455 (1969)

    Google Scholar 

  64. F. Dachille, P.Y. Simons, R. Roy, Am. Mineral. 53, 1929 (1968)

    Google Scholar 

  65. D.B. Rogers, J.L. Gillson, T.E. Gier, Solid State Commun. 5, 263 (1967)

    Google Scholar 

  66. P. Toulmin III, P.B. Barton Jr., Geochim. Cosmochim. Acta 28, 641 (1964)

    Google Scholar 

  67. A.J. Ellis, W.A.J. Mahon, Geochim. Cosmochim. Acta 28, 1323 (1964)

    Google Scholar 

  68. R.A. Laudise, in Progress in Inorganic Chemistry, ed. by F. Albert Cotton, vol. 3 (Interscience, New York, 1962), p. 1

    Google Scholar 

  69. R.A. Laudise, J.W. Nielsen, Solid State Phys. 12, 149 (1961)

    Google Scholar 

  70. S.A. Wood, Chem. Geol. 88, 99 (1990)

    Google Scholar 

  71. E.L. Shock, Orig. Life Evol. Biosph. 20, 331 (1990)

    Google Scholar 

  72. P.M. Dove, D.A. Crerar, Geochim. Cosmochim. Acta 54, 955 (1990)

    Google Scholar 

  73. A. Michard, Geochim. Cosmochim. Acta 53, 745 (1989)

    Google Scholar 

  74. J.C.I.V. Tanger, H.C. Helgeson, Am. J. Sci. 288, 19 (1988)

    Google Scholar 

  75. B.M. Lok, C.A. Messina, R.L. Patton, R.T. Gajek, T.R. Cannan, E.M. Flanigen, J. Am. Chem. Soc. 106, 6092 (1984)

    Google Scholar 

  76. E.B. Watson, T.M. Harrison, Earth Planet. Sci. Lett. 64, 295 (1983)

    Google Scholar 

  77. E. Tani, M. Yoshimura, S. Somiya, J. Am. Ceram. Soc. 66, 11 (1983)

    Google Scholar 

  78. S.T. Wilson, B.M. Lok, E.M. Flanigen, (Union Carbide Corp., USA). Application: EP, 108 pp (1982)

    Google Scholar 

  79. H. Ohmoto, A.C. Lasaga, Geochim. Cosmochim. Acta 46, 1727 (1982)

    Google Scholar 

  80. G. Perego, M. Taramasso, B. Notari, (Snamprogetti SpA, Italy). Application: BE, 18 pp (1981)

    Google Scholar 

  81. S. Miyata, Clays Clay Miner. 28, 50 (1980)

    Google Scholar 

  82. R.L. Penn, J.F. Banfield, Geochim. Cosmochim. Acta 63, 1549 (1999)

    Google Scholar 

  83. W.-J. Li, E.-W. Shi, W.-Z. Zhong, Z.-W. Yin, J. Crystal. Growth. 203, 186 (1999)

    Google Scholar 

  84. P. Feng, X. Bu, G.D. Stucky, Nature (London) 388, 735 (1997)

    Google Scholar 

  85. C.J. Barbe, F. Arendse, P. Comte, M. Jirousek, F. Lenzmann, V. Shklover, M. Gratzel, J. Am. Ceram. Soc. 80, 3157 (1997)

    Google Scholar 

  86. O.M. Yaghi, H. Li, J. Am. Chem. Soc. 117, 10401 (1995)

    Google Scholar 

  87. B.L. Cushing, V.L. Kolesnichenko, C.J. O'Connor, Chem. Rev. 104, 3893 (2004)

    Google Scholar 

  88. C.N.R. Rao, F.L. Deepak, G. Gundiah, A. Govindaraj, Progr. Solid State Chem. 31, 5 (2003)

    Google Scholar 

  89. B. Liu, H.C. Zeng, J. Am. Chem. Soc. 125, 4430 (2003)

    Google Scholar 

  90. L.E. Greene, M. Law, J. Goldberger, F. Kim, J.C. Johnson, Y. Zhang, R.J. Saykally, P. Yang, Angew. Chem. 42, 3031 (2003). International Edition

    Google Scholar 

  91. C.S. Cundy, P.A. Cox, Chem. Rev. 103, 663 (2003)

    Google Scholar 

  92. X. Wang, Y. Li, J. Am. Chem. Soc. 124, 2880 (2002)

    Google Scholar 

  93. S. Inagaki, S. Guan, T. Ohsuna, O. Terasaki, Nature 416, 304 (2002)

    Google Scholar 

  94. H. Zhang, X.-J. Lv, Y.-M. Li, Y. Wang, J.-H. Li, ACS Nano 4, 380 (2010)

    Google Scholar 

  95. C.-Y. Sun, S.-X. Liu, D.-D. Liang, K.-Z. Shao, Y.-H. Ren, Z.-M. Su, J. Am. Chem. Soc. 131, 1883 (2009)

    Google Scholar 

  96. B. Liu, E.S. Aydil, J. Am. Chem. Soc. 131, 3985 (2009)

    Google Scholar 

  97. S. Zhu, Q. Meng, L. Wang, J. Zhang, Y. Song, H. Jin, K. Zhang, H. Sun, H. Wang, B. Yang, Angew. Chem. Int. Ed. 52, 3953 (2013)

    Google Scholar 

  98. Q. Xiang, J. Yu, M. Jaroniec, Chem. Soc. Rev. 41, 782 (2012)

    Google Scholar 

  99. Q. Xiang, J. Yu, M. Jaroniec, J. Am. Chem. Soc. 134, 6575 (2012)

    Google Scholar 

  100. J. Jiang, K. Zhao, X. Xiao, L. Zhang, J. Am. Chem. Soc. 134, 4473 (2012)

    Google Scholar 

  101. X.-C. Dong, H. Xu, X.-W. Wang, Y.-X. Huang, M.B. Chan-Park, H. Zhang, L.-H. Wang, W. Huang, P. Chen, ACS Nano 6, 3206 (2012)

    Google Scholar 

  102. M.M. Lencka, R.E. Riman, Chem. Mater. 5, 61 (1993)

    Google Scholar 

  103. W.L. Suchanek, R.E. Riman, Ceram. Sci. Technol. 3, 63 (2012)

    Google Scholar 

  104. H. Hayashi, Y. Hakuta, Materials 3, 3794 (2010)

    Google Scholar 

  105. M. Rajamathi, R. Seshadri, Curr. Opin. Solid State Mater. Sci. 6, 337 (2002)

    Google Scholar 

  106. S.M. Gupta, M. Tripathi, Cent. Eur. J. Chem. 10, 279 (2012)

    Google Scholar 

  107. G. Garnweitner, M. Niederberger, J. Am. Ceram. Soc. 89, 1801 (2006)

    Google Scholar 

  108. M. Niederberger, G. Garnweitner, Chem. Eur. J. 12, 7282 (2006)

    Google Scholar 

  109. M. Niederberger, G. Garnweitner, J. Ba, J. Polleux, N. Pinna, Int. J. Nanotechnol. 4, 263 (2007)

    Google Scholar 

  110. M. Niederberger, G. Garnweitner, J. Buha, J. Polleux, J. Ba, N. Pinna, J. Sol-Gel Sci. Technol. 40, 259 (2006)

    Google Scholar 

  111. M. Niederberger, G. Garnweitner, N. Pinna, G. Neri, Progr. Solid State Chem. 33, 59 (2006)

    Google Scholar 

  112. A. Chemseddine, T. Moritz, Eur. J. Inorg. Chem. 235, 235 (1999)

    Google Scholar 

  113. B. Tan, Y. Wu, J. Phys. Chem. B 110, 15932 (2006)

    Google Scholar 

  114. C. Sun, H. Li, H. Zhang, Z. Wang, L. Chen, Nanotechnology 16, 1454 (2005)

    Google Scholar 

  115. H. Toraya, M. Yoshimura, S. Somiya, J. Am. Ceram. Soc. 66, 148 (1983)

    Google Scholar 

  116. M. Yoshimura, S. Somiya, Mater. Chem. Phys. 61, 1 (1999)

    Google Scholar 

  117. Y. Zheng, Y. Cheng, Y. Wang, F. Bao, L. Zhou, X. Wei, Y. Zhang, Q. Zheng, J. Phys. Chem. B 110, 3093 (2006)

    Google Scholar 

  118. Z.-s. Hong, Y. Cao, J.-f. Deng, Mater. Lett. 52, 34 (2002)

    Google Scholar 

  119. C.L. Lu, J.G. Lv, L. Xu, X.F. Guo, W.H. Hou, Y. Hu, H. Huang, Nanotechnology 20, 215604/1 (2009)

    Google Scholar 

  120. Y.V. Kolen'ko, K.A. Kovnir, I.S. Neira, T. Taniguchi, T. Ishigaki, T. Watanabe, N. Sakamoto, M. Yoshimura, J. Phys. Chem. C 111, 7306 (2007)

    Google Scholar 

  121. G.H. Du, Q. Chen, P.D. Han, Y. Yu, L.M. Peng, Phys. Rev. B. Condens. Matter Mater. Phys. 67, 035323/1 (2003)

    Google Scholar 

  122. A. Magrez, E. Vasco, J.W. Seo, C. Dieker, N. Setter, L. Forro, J. Phys. Chem. B 110, 58 (2006)

    Google Scholar 

  123. J.W. Liu, G. Chen, Z.H. Li, Z.G. Zhang, Int. J. Hydrogen Energ. 32, 2269 (2007)

    Google Scholar 

  124. Y. Li, X. Duan, H. Liao, Y. Qian, Chem. Mater. 10, 17 (1998)

    Google Scholar 

  125. M. Niederberger, N. Pinna, J. Polleux, M. Antonietti, Angew. Chem. Int. Ed. 43, 2270 (2004)

    Google Scholar 

  126. T. Adschiri, K. Kanazawa, K. Arai, J. Am. Ceram. Soc. 75, 1019 (1992)

    Google Scholar 

  127. K. Byrappa, K.M.L. Rai, M. Yoshimura, Environ. Technol. 21, 1085 (2000)

    Google Scholar 

  128. B. Zhao, L. Lin, D. He, J. Mater. Chem. A. Mater. Energ. Sustain. 1, 1659 (2013)

    Google Scholar 

  129. H. Cheng, J. Ma, Z. Zhao, L. Qi, Chem. Mater. 7, 663 (1995)

    Google Scholar 

  130. G.-S. Kim, Y.-S. Kim, H.-K. Seo, H.-S. Shin, Korean J. Chem. Eng. 23, 1037 (2006)

    Google Scholar 

  131. Y. Xu, X. Fang, J. Xiong, Z. Zhang, Mater. Res. Bull. 45, 799 (2010)

    Google Scholar 

  132. S. Kaewgun, C.A. Nolph, B.I. Lee, L.-Q. Wang, Mater. Chem. Phys. 114, 439 (2009)

    Google Scholar 

  133. Y. Wu, H.-M. Liu, B.-Q. Xu, Z.-L. Zhang, D.-S. Su, Inorg. Chem. 46, 5093 (2007)

    Google Scholar 

  134. S. Yin, Y. Aita, M. Komatsu, J. Wang, Q. Tang, T. Sato, J. Mater. Chem. 15, 674 (2005)

    Google Scholar 

  135. J. Liu, W. Qin, S. Zuo, Y. Yu, Z. Hao, J. Hazard. Mater. 163, 273 (2009)

    Google Scholar 

  136. G. Melcarne, L. De Marco, E. Carlino, F. Martina, M. Manca, R. Cingolani, G. Gigli, G. Ciccarella, J. Mater. Chem. 20, 7248 (2010)

    Google Scholar 

  137. X. Zhang, X. Ge, C. Wang, Crystal Growth Design 9, 4301 (2009)

    Google Scholar 

  138. B.-M. Wen, C.-Y. Liu, Y. Liu, New J. Chem 29, 969 (2005)

    Google Scholar 

  139. K. Das, S.K. Panda, S. Chaudhuri, J. Crystal Growth 310, 3792 (2008)

    Google Scholar 

  140. B. Santara, P.K. Giri, Mater. Chem. Phys. 137, 928 (2013)

    Google Scholar 

  141. L. Jiang, M. Yang, S. Zhu, G. Pang, S. Feng, J. Phys. Chem. C 112, 15281 (2008)

    Google Scholar 

  142. Y. Zhang, Y. Li, J. Phys. Chem. B 108, 17805 (2004)

    Google Scholar 

  143. P.D. Cozzoli, L. Manna, M.L. Curri, S. Kudera, C. Giannini, M. Striccoli, A. Agostiano, Chem. Mater. 17, 1296 (2005)

    Google Scholar 

  144. S. Biswas, S. Kar, S. Chaudhuri, J. Phys. Chem. B 109, 17526 (2005)

    Google Scholar 

  145. H. Zhang, L. Wang, H. Xiong, L. Hu, B. Yang, W. Li, Adv. Mater. 15, 1712 (2003)

    Google Scholar 

  146. S. Huang, Appl. Phys. B 84, 323 (2006)

    Google Scholar 

  147. Y. Li, Y. Ding, Z. Wang, Adv. Mater. 11, 847 (1999)

    Google Scholar 

  148. X.-H. Li, J.-X. Li, G.-D. Li, D.-P. Liu, J.-S. Chen, Eur. J. Chem. A 13, 8754 (2007)

    Google Scholar 

  149. H. Cao, G. Wang, S. Zhang, X. Zhang, D. Rabinovich, Inorg. Chem. 45, 5103 (2006)

    Google Scholar 

  150. M. Salavati-Niasari, M.R. Loghman-Estarki, F. Davar, Chem. Eng. J. 145, 346 (2008)

    Google Scholar 

  151. Y. Yin, A.P. Alivisatos, Nature 437, 664 (2005)

    Google Scholar 

  152. Y. Xie, Y. Qian, W. Wang, S. Zhang, Y. Zhang, Science 272, 1926 (1996)

    Google Scholar 

  153. L. Grocholl, J. Wang, E.G. Gillan, Chem. Mater. 13, 4290 (2001)

    Google Scholar 

  154. A.P. Purdy, Chem. Mater. 11, 1648 (1999)

    Google Scholar 

  155. K. Sardar, C.N.R. Rao, Adv. Mater. 16, 425 (2004)

    Google Scholar 

  156. K. Biswas, K. Sardar, C.N.R. Rao, Appl. Phys. Lett. 89, 132503 (2006)

    Google Scholar 

  157. S.V. Bhat, K. Biswas, C.N.R. Rao, Solid State Commun. 141, 325 (2007)

    Google Scholar 

  158. B. Mazumder, P. Chirico, A.L. Hector, Inorg. Chem. 47, 9684 (2008)

    Google Scholar 

  159. F. Xu, Y. Xie, X. Zhang, S. Zhang, X. Liu, X. Tian, Inorg. Chem. 43, 822 (2003)

    Google Scholar 

  160. S. Wei, J. Lu, W. Yu, Y. Qian, J. Appl. Phys. 95, 3683 (2004)

    Google Scholar 

  161. Y.-D. Li, X.-F. Duan, Y.-T. Qian, L. Yang, M.-R. Ji, C.-W. Li, J. Am. Chem. Soc. 119, 7869 (1997)

    Google Scholar 

  162. S. Gao, J. Lu, Y. Zhao, N. Chen, Y. Xie. Eur. J. Inorg. Chem. 2003, 1822 (2003)

    Google Scholar 

  163. S. Wei, J. Lu, W. Yu, H. Zhang, Y. Qian, Chem. Lett. 33, 386 (2004)

    Google Scholar 

  164. B. Hu, K. Wang, L. Wu, S.-H. Yu, M. Antonietti, M.-M. Titirici, Adv. Mater. 22, 813 (2010)

    Google Scholar 

  165. M.-M. Titirici, M. Antonietti, N. Baccile, Green Chem. 10, 1204 (2008)

    Google Scholar 

  166. M.M. Titirici, A. Thomas, M. Antonietti, Adv. Funct. Mater. 17, 1010 (2007)

    Google Scholar 

  167. M.-M. Titirici, M. Antonietti, Chem. Soc. Rev. 39, 103 (2010)

    Google Scholar 

  168. Y. Fang, D. Gu, Y. Zou, Z. Wu, F. Li, R. Che, Y. Deng, B. Tu, D. Zhao, Angew. Chem. Int. Ed. 49, 7987 (2010)

    Google Scholar 

  169. W.Z. Wang, J. Y. Huang, Z. F. Ren, Langmuir, 21, 751 (2004)

    Google Scholar 

  170. W.Z. Wang, B. Poudel, J.Y. Huang, D.Z. Wang, S. Kunwar, Z.F. Ren, Nanotechnology 16, 1126 (2005)

    Google Scholar 

  171. J. Qiu, W. Shen, R. Yu, B. Yao, Chem. Lett. 37, 644 (2008)

    Google Scholar 

  172. J.L.C. Rowsell, O.M. Yaghi, Angew. Chem. Int. Ed. 44, 4670 (2005)

    Google Scholar 

  173. J.-R. Li, R.J. Kuppler, H.-C. Zhou, Chem. Soc. Rev. 38, 1477 (2009)

    Google Scholar 

  174. M.K. Carpenter, T.E. Moylan, R.S. Kukreja, M.H. Atwan, M.M. Tessema, J. Am. Chem. Soc. 134, 8535 (2012)

    Google Scholar 

  175. J. Lee, O.K. Farha, J. Roberts, K.A. Scheidt, S.T. Nguyen, J.T. Hupp, Chem. Soc. Rev. 38, 1450 (2009)

    Google Scholar 

  176. W.J. Rieter, K.M. Taylor, H. An, W. Lin, J. Am. Chem. Soc. 128, 9024 (2006)

    Google Scholar 

  177. A.C. McKinlay, R.E. Morris, P. Horcajada, G. Férey, R. Gref, P. Couvreur, C. Serre, Angew. Chem. Int. Ed. 49, 6260 (2010)

    Google Scholar 

  178. R.C. Huxford, J. Della Rocca, W. Lin, Curr. Opin. Chem. Biol. 14, 262 (2010)

    Google Scholar 

  179. J. Rocha, L.D. Carlos, F.A.A. Paz, D. Ananias, Chem. Soc. Rev. 40, 926 (2011)

    Google Scholar 

  180. M. Sadakiyo, T. Yamada, H. Kitagawa, J. Am. Chem. Soc. 131, 9906 (2009)

    Google Scholar 

  181. K.M.L. Taylor-Pashow, J.D. Rocca, Z. Xie, S. Tran, W. Lin, J. Am. Chem. Soc. 131, 14261 (2009)

    Google Scholar 

  182. K.M.L. Taylor, A. Jin, W. Lin, Angew. Chem. Int. Ed. 47, 7722 (2008)

    Google Scholar 

  183. K.M.L. Taylor, W.J. Rieter, W. Lin, J. Am. Chem. Soc. 130, 14358 (2008)

    Google Scholar 

  184. W.J. Rieter, K.M.L. Taylor, W. Lin, J. Am. Chem. Soc. 129, 9852 (2007)

    Google Scholar 

  185. Y. Chen, H. Chen, D. Zeng, Y. Tian, F. Chen, J. Feng, J. Shi, ACS Nano 4, 6001 (2010)

    Google Scholar 

  186. C.M. Niemeyer, Angew. Chem. 40, 4128 (2001)

    Google Scholar 

  187. P.V. Kamat, J. Phys. Chem. B 106, 7729 (2002)

    Google Scholar 

  188. T. Mousavand, S. Ohara, M. Umetsu, J. Zhang, S. Takami, T. Naka, T. Adschiri, J. Supercrit. Fluid. 40, 397 (2007)

    Google Scholar 

  189. W.C.W. Chan, S. Nile, Science. 281, 2016 (1998)

    Google Scholar 

  190. A. Singhal, G. Skandan, A. Wang, N. Glumac, B.H. Kear, R.D. Hunt, Nanostruct. Mater. 11, 545 (1999)

    Google Scholar 

  191. W. Posthumus, P.C.M.M. Magusin, J.C.M. Brokken-Zijp, A.H.A. Tinnemans, R. van der Linde, J. Colloid Interface Sci. 269, 109 (2004)

    Google Scholar 

  192. B. Shahmoradi, K. Byrappa, A. Maleki, J. Mater. Sci. Eng. A 3, 50 (2013)

    Google Scholar 

  193. T. Adschiri, Chem. Lett. 36, 1188 (2007)

    Google Scholar 

  194. H. Cai, X. An, J. Cui, J. Li, S. Wen, K. Li, M. Shen, L. Zheng, G. Zhang, X. Shi, ACS Appl. Mater. Interfaces 5, 1722 (2013)

    Google Scholar 

  195. K. Namratha, K. Byrappa, J. Supercrit. Fluid. 79, 251 (2013)

    Google Scholar 

  196. D. Voltzke, S. Gablenz, H.P. Abicht, R. Schneider, E. Pippel, J. Woltersdorf, Mater. Chem. Phys. 61, 110 (1999)

    Google Scholar 

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    Authors and Affiliations

    1. Energy and Transportation Science Division, Oak Ridge National Laboratory, Oak Ridge, TN, 37831, USA

      Jianlin Li

    2. Chemical Sciences and Engineering Division, Argonne National Laboratory, Argonne, IL, 60439, USA

      Qingliu Wu

    3. Department of Chemistry, Georgia Southern University, Statesboro, GA, 30460, USA

      Ji Wu

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    1. Jianlin Li
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    2. Qingliu Wu
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    3. Ji Wu
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    Correspondence to Jianlin Li , Qingliu Wu or Ji Wu .

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    Editors and Affiliations

    1. Materials Engineering, Tarbiat Modares University, Tehran, Iran

      Mahmood Aliofkhazraei

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    Li, J., Wu, Q., Wu, J. (2015). Synthesis of Nanoparticles via Solvothermal and Hydrothermal Methods. In: Aliofkhazraei, M. (eds) Handbook of Nanoparticles. Springer, Cham. https://doi.org/10.1007/978-3-319-13188-7_17-1

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    • DOI: https://doi.org/10.1007/978-3-319-13188-7_17-1

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