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Results of the Studies of Morphology and Granulometric Composition of Electro Erosive Tungsten-Free Hard-Alloy Powder Material

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Modern Problems in Construction (MPC 2022)

Abstract

The purpose of this work was to study the morphology and particle size distribution of new tungsten-free hard-alloy powder materials produced by electro erosive dispersion in an oxygen-containing medium (distilled water). To produce new tungsten-free hard-alloy powder materials, an experimental laboratory setup for electro erosive dispersion was used. The analysis of the grain size composition of electro erosive tungsten-free hard-alloy particles was carried out by means of an Analysette 22 Nano Tec laser particle size analyzer. The method of scanning electron microscopy using a QUANTA 600 FEG microscope was used to study the morphology of the experimental powder material. The results of the analysis of the particle size distribution of electro erosive tungsten-free hard-alloy particles showed that the particle size ranges from 0.372 µm to 65.5 µm. It is shown that the average size of the particles obtained in distilled water is 41.63 μm. The study of morphology showed that in the process of electro dispersion of metal waste, the particles that ejected from the electric discharge channel in molten form crystallized very quickly. The process of rapid crystallization of the molten material in a liquid working medium contributes to the formation of particles of the correct spherical and elliptical shape.

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References

  1. Ageeva EV, Ageev EV, Horyakova NM, Sabelnikov BN (2021) Tungsten-free hard alloys based on electroerosive powders of titanium carbonitride. Closed Joint Stock Company, University Book. ISBN 978-5-907441-07-1. EDN BQVXJL

    Google Scholar 

  2. Ageeva EV, Sabelnikov BN (2021) Structure and properties of a tungsten–free hard alloy based on titanium carbonitride sintered from electroerosive powders obtained in a carbon-containing medium. Hardening Technol Coat 4(196):158161. EDN EKGUJX

    Google Scholar 

  3. Serebrovsky V, Sabel’nikov B (2020) X-ray diffraction analysis of electroerosive powder materials, obtained from waste of tungsten-free hard alloy grade KNT16. In: MATEC web of conferences, vol 315. p 01002. https://doi.org/10.1051/matecconf/202031501002

  4. Ageev EV, Selyutin VL, Pikalov SV (2020) X-ray microanalysis of electro-erosive powder materials, obtained from tungsten-nickel-iron (TNI) alloy wastes in water. In: MATEC web of conferences, vol 315. p 01004. https://doi.org/10.1051/matecconf/202031501004

  5. Latypov RA, Ageeva EV, Latypova GR (2019) X-ray microanalysis of powders, obtained by electroerosion dispersion of the alloy W-Ni-Fe. In: MATEC web of conferences, vol 298. p 00125. https://doi.org/10.1051/matecconf/201929800125

  6. Sabel’nikov BN, Ageeva AE, Podanov VO, Korolev MS (2020) Investigation of the microstructure and X-ray spectral microanalysis of powder material obtained from waste of the KNT16 brand tungsten-free hard alloy. In: MATEC web of conferences, vol 329. p 02011.https://doi.org/10.1051/matecconf/202032902011

  7. Ageev EV, Khardikov SV, Vorobyev EA, Sysoev AA (2019) Shape and morphology of the particles surface of electroerosive powders of micro- and nanometric fractions, obtained from H17MYuA steel in kerosene. In: MATEC web of conferences, vol 298. p 00127. https://doi.org/10.1051/matecconf/201929800127

  8. Ageev EV (2012) Patent 2449859, Russian Federation, C2, B22F9/14. Installation for producing nanodispersed powders from conductive materials, applicant and patent holder Southwestern State University. No. 2010104316/02; application 2010/08/02, publ. 2012/10/05

    Google Scholar 

  9. Pereverzev A, Ageev E (2019) X-ray diffraction analysis of products sintered from isostatically pressed leaded bronze powders. In: MATEC web of conferences, vol 298. p 00037. https://doi.org/10.1051/matecconf/201929800037

  10. Loktionova OG, Ageeva EV, Sabelnikov BN (2020) Results of X-ray studies of sintered samples obtained from the electroerosive powder material of the KNT16 alloy. Proc Southwest State University Ser: Eng Technol 10(4):22–34

    Google Scholar 

  11. Ageev EV, Ageeva EV, Sabelnikov BN (2021) Patent 2756465 C1, Russian Federation, IPC B22F 3/16, C22C 29/04, B22F 9/14. Method for producing tungsten-free hard alloy KNT from powder materials obtained in distilled water, applicant and patent holder Southwestern State University. No. 2020138425: application 2020/11/24, publ 2021/09/30

    Google Scholar 

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Correspondence to Boris Sabelnikov .

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Sabelnikov, B., Simonov, A., Ageeva, E. (2024). Results of the Studies of Morphology and Granulometric Composition of Electro Erosive Tungsten-Free Hard-Alloy Powder Material. In: Vatin, N., Pakhomova, E.G., Kukaras, D. (eds) Modern Problems in Construction. MPC 2022. Lecture Notes in Civil Engineering, vol 372. Springer, Cham. https://doi.org/10.1007/978-3-031-36723-6_12

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  • DOI: https://doi.org/10.1007/978-3-031-36723-6_12

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  • Publisher Name: Springer, Cham

  • Print ISBN: 978-3-031-36722-9

  • Online ISBN: 978-3-031-36723-6

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