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Nuclear Magnetic Resonance (NMR): Modern Methods

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Springer Handbook of Advanced Catalyst Characterization

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Abstract

Amplification of the available magnetic field strengths in the previous decades made modern solid-state NMR one of the most informative tools in many physical and chemical areas including heterogeneous catalysis. However, in some cases, the magnetic field strength is not the decisive factor in the experiment. That is where modern advanced techniques such as intricate pulse programs, correlation experiments, dynamic nuclear polarization, and selective isotope enrichment come in handy. This review does not aim to encompass every possible application of solid-state NMR in catalysis, but the authors have tried to include the examples of the most advanced and state-of-the-art experiments with supported oxide catalysts, zeolites, and metal-organic frameworks that allowed tackling even the most challenging problems.

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Authors and Affiliations

  1. Boreskov Institute of Catalysis, Novosibirsk, Russia

    Olga Lapina & Ilya Yakovlev

  2. Physics Department, Novosibirsk State University, Novosibirsk, Russia

    Olga Lapina & Ilya Yakovlev

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  1. Olga Lapina
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  2. Ilya Yakovlev
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Correspondence to Olga Lapina .

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  1. Operando Molecular Spectroscopy & Catalysis Laboratory, Department of Chemical & Biomolecular Engineering Lehigh University, Bethlehem, PA, USA

    Israel E. Wachs

  2. Catalytic Spectroscopy Laboratory, Spectroscopy and Industrial Catalysis, SpeiCat Institute for Catalysis and Petroleum Chemistry, CSIC, Madrid, Spain

    Miguel A. Bañares

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Lapina, O., Yakovlev, I. (2023). Nuclear Magnetic Resonance (NMR): Modern Methods. In: Wachs, I.E., Bañares, M.A. (eds) Springer Handbook of Advanced Catalyst Characterization. Springer Handbooks. Springer, Cham. https://doi.org/10.1007/978-3-031-07125-6_35

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