Abstract
This study concentrates on nanomechanical analysis and fractography of an extruded Mg-Dy-Nd-Zn-Zr alloy in different microstructures. The focus here lies on the reduced elastic modulus evaluated from nanoindentation and the fracture behavior evaluated by scanning electron microscopy (SEM). The initial hot-extruded condition shows a fine-grained microstructure consisting of lamellar long-period stacking-ordered (LPSO) within the Mg-matrix and blocky LPSO-phases and precipitates. Solution heat treatment causes grain growth and dissolution of the LPSO phases and precipitates, the Mg-matrix becomes enriched by solid solution. Except for the blocky LPSO in the extruded microstructure, where the value is higher, the reduced elastic modulus does not change across the microstructural features. C-ring compression tests in Ringer solution were used to evaluate the fracture behavior, mostly transgranular cleavage facets with some ductile features are present. The amount of sub-cracks forming from the main crack are influenced by the heat treatment time. Blocky LPSO do not show very present on the fracture surface.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Similar content being viewed by others
References
US patents: 9,566,367 B2 & 9,522,219 B2, EU patents: 744531 & 2744532.
Meko Laser Materials Processing, www.meko.de/RESOLOY.
Fort Wayne Metals, www.fwmetals.com/RESOLOY-a-magnesium-alloy-for-absorbable-devices.
P. Maier et al., Magnesium Technology 2019, 175–181 (2019).
R. Menze, E. Wittchow, J. Biomed. Mater. Res. B Appl. Biomater., 109(9), 1292–1302 (2021).
D. Li, J. Dong, X. Zeng, C. Lu, and W. Ding, J Alloys Compounds 439/1–2, 254–257 (2007).
P. Maier, A. Steinacker, B. Clausius and N. Hort, JOM, 72, 5, 1870–1879 (2020).
S. Ahlers et al., Metals, 11, 1372 (2021).
D. Egusa, E. Abe, Acta Mater. 60, 1, 166–178 (2012).
J. Zhang et al. J. Magnes. Alloys, 6, 3, 277–291 (2018).
W.T. Sun et al., Mater. Sci. Eng. A, 738, 238–252 (2018).
Z. Zhang et al., Mater. Trans., 59, 669–673 (2018).
S.M. Ramezani et al. J Alloys Compounds 2019, 793, 134–145.
K. Kittner et al., Crystals, 10, 513 (2020).
C. Xu et al., Sci. Rep., 7, 40846 (2017).
L. Yuan et al., Trans. Nonferrous Met. Soc. China, 27, 11, 2381–2389 (2017).
X. Cai et al., Metal Mater. Trans. A, 45, 3703–3707 (2014).
J. Yuan et al., Materials, 14, 1737 (2021).
P. Maier et al., Magnesium Technology 2021, 19–26 (2021).
P. Maier et al., Materials, 14(13), 3686 (2021).
H.X. Zhang et al. Acta Metall. Sin. (Engl. Lett.), 32, 9, 1122–1134 (2019).
Z. Zhang et al., J. Magnes. Alloys, 6, 255–262(2018).
O. Sahin et al., Acta Physica Polonica A, 130 (2016).
B. Bhushan, Microsyst Technol 23, 1595–1649 (2017).
J. Rymarczyk et al. Open Physics, 9, 2, 300–306 (2011).
A. Naughton-Duszová et al. Metals, 9, 502 (2019).
A. Ruiz-Moreno, P. Hähner, Mater. Design, 145, 168–180, (2018).
M. Haghshenas, M. Gupta, Nanocomposites, 6:1, 22–30, (2020).
W.C. Oliver, G.M. Pharr, J. Mater. Res. 7 (06) 1564–1583 (1992).
J. Bi et al., Mater. Sci. Eng. A, 768, 138478 (2019).
L. Pramod et al., Mater. Sci. Eng. A, 739, 383–394 (2019).
D. Huebler et al. J. Mater. Sci., 55, 10582–10592 (2020).
S. Chabri et al.: J. Mater. Sci. Technol., 29, 11 (2013).
J. Deng et al., Proceedings of the International Congress (APCF/SIF-2014) 142–146 (2014).
D. Jeddi et al., J. of Mater. Eng. and Perform., 14, 37–49 (2005).
P. Maier et al., Metals, 10, 5, 584 (2020).
H. Liu et al., J. Alloy. Compd. 704, 509–517 (2017).
Y. Kawamura et al., Mater. Trans., 48, 11, 2986–2992 (2007).
E. Oñorbe et al., J. Mater. Sci. 47, 1085–1093 (2012).
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2022 The Minerals, Metals & Materials Society
About this paper
Cite this paper
Maier, P., Richter, A., Clausius, B., Hort, N. (2022). Nanomechanical Analysis and Fractography of Extruded Mg-Dy-Nd Based Alloy Influenced by Solution Heat Treatment. In: Maier, P., Barela, S., Miller, V.M., Neelameggham, N.R. (eds) Magnesium Technology 2022. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-92533-8_31
Download citation
DOI: https://doi.org/10.1007/978-3-030-92533-8_31
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-030-92532-1
Online ISBN: 978-3-030-92533-8
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)