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The Effect of Mechanical Activation on the Structure and Dielectric Properties of PbYb1/2Nb1/2O3–PbFe1/2Nb1/2O3 Solid Solution Ceramics

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Advanced Materials

Part of the book series: Springer Proceedings in Physics ((SPPHY,volume 224))

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Abstract

Recently we have found out that high-energy mechanical activation during mechanochemical synthesis stimulates disordering of Yb3+ and Nb5+ cations in the PbYb1/2Nb1/2O3 (PYN) ceramics. However, one could expect a contamination of thus obtained ceramics by iron as the planetary mill AGO-2 with both jars and balls made of the stainless steel was used for mechanical activation. To elucidate the effect of iron doping on the compositional ordering of PYN, in the present work several (1 − x)PYN–xPbFe1/2Nb1/2O3 (PYN–xPFN) solid solution compositions have been fabricated by both the usual solid-state synthesis and by high-energy mechanochemical synthesis and their structure and properties were compared. Basing on these data the (x, T)-phase diagrams for the PYN – xPFN solid solutions fabricated by both methods were constructed. It was found out that the difference in the lattice parameters values and dielectric properties of ceramics fabricated by different methods are partially due to the formation of the (1–x)PYN–xPFN solid solutions with PFN content larger than nominal one and partially due to the effect of high-energy mechanical activation.

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Acknowledgements

This work was supported in part by the Ministry of Education and Science of the Russian Federation (research project No. 3.1649.2017/4.6) and by the Russian Foundation for Basic Research (grant No 17-03-01293_a). IPR acknowledges the support from the CAS President’s International Fellowship Initiative through the project 2018VEA0011.

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Authors and Affiliations

  1. Faculty of Physics, Research Institute of Physics, Southern Federal University, 344090, Rostov-on-Don, Russia

    I. P. Raevski, M. A. Evstigneeva, S. I. Raevskaya, A. G. Lutokhin, S. P. Kubrin, I. N. Zakharchenko, Y. A. Kuprina, V. V. Titov, M. A. Malitskaya & O. A. Bunina

  2. Institute of Solid State Chemistry and Mechanochemistry, SB RAS, 630128, Novosibirsk, Russia

    A. A. Gusev & V. P. Isupov

  3. Shanghai Institute of Ceramics, Chinese Academy of Sciences, 200050, Shanghai, China

    G. R. Li

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  1. I. P. Raevski
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Corresponding author

Correspondence to I. P. Raevski .

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Editors and Affiliations

  1. I. I. Vorovich Mathematics, Mechanics and Computer Sciences Institute, Southern Federal University, Rostov-on-Don, Russia

    Ivan A. Parinov

  2. Department of Microelectronics Engineering, National Kaohsiung University of Science and Technology, Kaohsiung, Taiwan

    Shun-Hsyung Chang

  3. Mechanical Engineering Department, Korea Maritime and Ocean University, Busan, Korea (Republic of)

    Yun-Hae Kim

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Raevski, I.P. et al. (2019). The Effect of Mechanical Activation on the Structure and Dielectric Properties of PbYb1/2Nb1/2O3–PbFe1/2Nb1/2O3 Solid Solution Ceramics. In: Parinov, I., Chang, SH., Kim, YH. (eds) Advanced Materials. Springer Proceedings in Physics, vol 224. Springer, Cham. https://doi.org/10.1007/978-3-030-19894-7_4

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