Skip to main content
Log in

Influence of multiple thermal cycles on microstructure of heat-affected zone in TIG-welded super duplex stainless steel

  • Research Paper
  • Published:
Welding in the World Aims and scope Submit manuscript

Abstract

The influence of heat input and multiple welding cycles on the microstructure of the heat-affected zone in autogenously TIG-welded 6 mm 2507 type super duplex stainless steel plates was investigated. In order to produce multiple thermal cycles, one to four pass bead-on-plate welds were made with arc energies of 0.47 and 1.08 kJ/mm, corresponding to heat inputs of 0.37 and 0.87 kJ/mm. Several thermocouples were attached to record thermal cycles on the front and back sides of the plates. Finite element modelling was successfully done to map and correlate measured and calculated peak temperatures. Only minor changes were seen in the ferrite content at 1 and 2 mm from the fusion boundary. Nitrides formed in all passes of the low heat input samples in a region next to the fusion boundary, but only after the third and fourth passes of the high heat input samples. Sigma phase precipitated only in a zone heated to a peak temperature in the range of approximately 828 to 1028 °C. Multiple reheating was found to promote precipitation of sigma phase relatively more than slower cooling. A precipitation free zone was observed between the nitride and sigma phase bands. The precipitation behaviour could be understood from equilibrium phase diagrams, evaluation of local thermal cycles and by correlating results from the modelling and measurements of peak temperatures. It is suggested that the peak temperature, the accumulated time in the critical temperature range between approximately 828 and 1028 °C, and the number of thermal cycles are the most relevant criteria when evaluating the risk of sigma phase formation.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  1. Gunn RN (1997) Duplex stainless steels: microstructure, properties and applications. Woodhead Publishing

  2. Tan H, Jiang Y, Deng B, Sun T, Xu J, Li J (2009) Effect of annealing temperature on the pitting corrosion resistance of super duplex stainless steel UNS S32750. Mater Charact 60(9):1049–1054

    Article  Google Scholar 

  3. Karlsson L (1995) Welding duplex and super duplex stainless steels. Anti-Corros Methods Mater 42(6):30–35

    Article  Google Scholar 

  4. Pohl M, Storz O, Glogowski T (2007) Effect of intermetallic precipitations on the properties of duplex stainless steel. Mater Charact 58(1):65–71

    Article  Google Scholar 

  5. Nilsson J-O (1992) Super duplex stainless steels. Mater Sci Technol 8(8):685–700

    Article  Google Scholar 

  6. Pettersson N, Pettersson RF, Wessman S (2015) Precipitation of Chromium Nitrides in the Super Duplex Stainless Steel 2507. Metall Mater Trans A 46(3):1062–1072

    Article  Google Scholar 

  7. Taban E, Kaluc E (2011) Welding behaviour of Duplex and Superduplex Stainless Steels using Laser and Plasma ARC Welding processes. Weld World 55(7–8):48–57

    Article  Google Scholar 

  8. Karlsson L, Tolling J Experiences and New Possibilities in Welding Duplex Stainless Steels. IIW Regional Congress on Welding and Related Inspection Technologies,, South Africa, 2006

  9. Wang H-S (2005) Effect of welding variables on cooling rate and pitting corrosion resistance in super duplex stainless weldments. Mater Trans 46(3):593–601

    Article  Google Scholar 

  10. Atamert S, King J (1992) Super duplex stainless steels part 1 heat affected zone microstructures. Mater Sci Technol 8(10):896–912

    Article  Google Scholar 

  11. Nishimoto K, Saida K, Katsuyama O (2006) Prediction of Sigma Phase Precipitation in Super Duplex Stainless Steel Weldments. Weld World 50(3–4):13–28

    Article  Google Scholar 

  12. Tao RL, Liu J, Fan GW, Chang X. The study on welding HAZ microstructure of SAF 2507 Duplex stainless steel by simulation tests. Conf. processdings: Materials Science Forum, 2015. Trans Tech Publ, pp 277–280

  13. Attarha M, Sattari-Far I (2011) Study on welding temperature distribution in thin welded plates through experimental measurements and finite element simulation. J Mater Process Technol 211(4):688–694

    Article  Google Scholar 

  14. Alexandrov B, Lippold J (2006) In-situ weld metal continuous cooling transformation diagrams. Weld World 50(9–10):65–74

    Article  Google Scholar 

  15. Karlsson (2012) Welding Duplex Stainless Steels — A Review Of Current Recommendations. Weld World 56(5–6):65–76. doi:10.1007/BF03321351

    Google Scholar 

  16. Nilsson J, Wilson A (1993) Influence of isothermal phase transformations on toughness and pitting corrosion of super duplex stainless steel SAF 2507. Mater Sci Technol 9(7):545–554

    Article  Google Scholar 

  17. Kim Y-J, Chumbley LS, Gleeson B (2008) Continuous Cooling Transformation in Cast Duplex Stainless Steels CD3MN and CD3MWCuN. J Mater Eng Perform 17(2):234–239

    Article  Google Scholar 

  18. Hurtig K, Choquet I, Scotti A, L.E. Svensson A critical analysis of weld heat input measurement with a water-cooled stationary anode calorimeter. Conf. proceedings: JOM 18, Helsingør, Denmark.

  19. ASTM International (2014) Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A262-14. West Conshohocken, PA

  20. Stenbacka N, Choquet I, Hurtig K Review of arc efficiency values for gas tungsten arc welding. In: IIW Commission IV-XII-SG212, Intermediate Meeting, BAM, Berlin, Germany, 18–20 April, 2012, 2012. pp 1–21

  21. ASTM E1245-03, Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis (2008). ASTM International, West Conshohocken, PA

  22. Taban E (2008) Toughness and microstructural analysis of superduplex stainless steel joined by plasma arc welding. J Mater Sci 43(12):4309–4315

    Article  Google Scholar 

  23. Westin EM, Keehan E, Ström M, Von Brömssen B Laser welding of a lean duplex stainless steel. In: 26th International Congress on Applications of Lasers and Electro-Optics, ICALEO 2007: Congress Proceedings, 2007. pp 335–344

  24. Karlsson L (2013) Welding duplex and super duplex stainless steels., Anti-Corrosion Methods and Materials

    Google Scholar 

  25. Meyer A, Du Toit M (2008) The influence of interstitial diffusion across the fusion line on the HAZ microstructure and properties in 12% chromium type 1.4003 steels. Weld World 52(11–12):42–49

    Article  Google Scholar 

  26. Karlsson L, Pak S (1995) Influence of intermetallic phases on the corrosion properties of duplex stainless steel weld metals. Weld Int 9(7):554–562

    Article  Google Scholar 

  27. Karlsson L (1999) Intermetallic phase precipitation in duplex stainless steels and weld metals: metallurgy, influence on properties, welding and testing aspects. Weld Res Counc Bull 438

  28. Hertzman S, Brolund B, Ferreira PJ (1997) An experimental and theoretical study of heat-affected zone austenite reformation in three duplex stainless steels. Metall Mater Trans A 28(2):277–285

    Article  Google Scholar 

Download references

Acknowledgments

The authors would like to thank Sten Wessman from Swerea KIMAB AB and University West for his valuable comments. The great support received from the project partners and their representatives: Joakim Wahlsten (Swerea KIMAB AB, Kista), Rachel Pettersson (Jernkontoret, Stockholm), Hans Åström (ELGA AB, Partille), Lars-Åke Bylund (voestalpine Böhler Welding Nordic AB, Avesta), Henrik Larsson (Thermo-Calc Software AB, Stockholm), Alexander Thulin (Outokumpu Stainless AB, Avesta) and Massimo Cocco (Forsmarks Kraftgrupp AB, Forsmark) is acknowledged. Financial support of the KK foundation for the DuplexWeld project is appreciatively acknowledged.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Vahid A. Hosseini.

Additional information

Recommended for publication by Commission IX - Behaviour of Metals Subjected to Welding

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Hosseini, V.A., Valiente Bermejo, M.A., Gårdstam, J. et al. Influence of multiple thermal cycles on microstructure of heat-affected zone in TIG-welded super duplex stainless steel. Weld World 60, 233–245 (2016). https://doi.org/10.1007/s40194-016-0300-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s40194-016-0300-5

Keywords (IIW Thesaurus)

Navigation