Abstract
The self-propagating high-temperature synthesis (SHS) method has been applied to the preparation of TiC powder from mixtures of TiO2, Mg, and C. The TiC/MgO product is leached by hydrochloric acid to remove the MgO. The optimum mixing ratio was TiO2∶Mg∶C=1∶2.2∶1.5. The final product TiC had > 99.9% purity and relatively uniform particle size of 0.3–0.4 μm.
Similar content being viewed by others
References
Z. A. Munir, Ceram. Bull. 67 (1988) 342.
J. F. Cider, Ceram. Eng. Sci. Proc. 3 (1982) 519.
M. Ouabdesselam and Z. A. Munir, J. Mater. Sci. 22 (1987) 1799
A. G. Merzhanov and I. P. Borovinskaya, Dokl. Akad. Nauk. SSSR (Chem.) 204 (1972) 429.
A. P. Hardt and P. V. Phung, Combust. Flame 21 (1973) 77
A. P. Hardt and R. W. Holsinger, ibid. 21 (1973) 90.
Editorial Committee of Fine Ceramics: “Encyclopedia of Fine Ceramics” (Kibodang Co., Tokyo, 1987 pp. 632–44.
L. E. Toth, in “Transition Metal Carbides and Nitrides” (Academic Press, New York, 1971) pp. 150–9.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Ko, S.G., Won, C.W., Chun, B.S. et al. The self-propagating high-temperature synthesis (SHS) of ultrafine high-purity TiC powder from TiO2+Mg+C. JOURNAL OF MATERIALS SCIENCE 30, 2835–2837 (1995). https://doi.org/10.1007/BF00349651
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/BF00349651