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SEMPA Studies of Thin Films, Structures, and Exchange Coupled Layers

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Part of the book series: NanoScience and Technology ((NANO))

Abstract

Scanning electron microscopy with polarization analysis (SEMPA) has developed into a powerful technique to study domains in ultrathin films. In this chapter, we discuss from a very general point of view the instrumental aspects of the method. Examples of thin film investigations are given that demonstrate unique features of SEMPA. New solutions around apparent limitations of the technique are presented at the end, i.e., analyzing samples with contaminated surfaces and imaging in external fields.

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References

  1. R.J. Celotta and D.T. Pierce in: Microbeam Analysis-1982, K.F.J. Heinrich (ed.), San Francisco Press, p. 469.

    Google Scholar 

  2. J. Kirschner, Scanning Electron Microsc. III, 1179 (1984).

    Google Scholar 

  3. K. Koike and K. Hayakawa, Jpn. J. Appl. Phys. 23, L187 (1984).

    Article  Google Scholar 

  4. J. Unguris, G. Hembree, R.J. Cellota, and D.T. Pierce, J. Microscopy 139, RP1 (1985).

    CAS  Google Scholar 

  5. H.P. Oepen and J. Kirschner, Scanning Micros. 5, 1 (1991).

    CAS  Google Scholar 

  6. R. Allenspach, J. Magn. Magn. Mater. 129, 160 (1994).

    Article  CAS  Google Scholar 

  7. T. VanZandt, R. Browning, C.R. Helms, H. Poppa, and M. Landolt, Rev. Sci. Instrum. 60, 3430 (1989).

    Article  Google Scholar 

  8. E.A. Seddon, Y.B. Xu, D. Greig, J.R.M. Wardell, D. Rubio-Temprano, and M. Hardiman, J. Appl. Phys. 81, 4063 (1997).

    Article  CAS  Google Scholar 

  9. Y. Iwasaki, M. Takiguchi, and K. Bessho, J. Appl. Phys. 81, 5021 (1997).

    Article  CAS  Google Scholar 

  10. Y. Lee, A.R. Koymen, and M.J. Haji-Sheikh, Appl. Phys. Lett. 72, 851 (1998).

    Article  CAS  Google Scholar 

  11. C. Stamm, F. Marty, A. Vaterlaus, V. Weich, S. Egger, U. Maier, U. Ramsperger, H. Fuhrmann, and D. Pescia, Science 282, 449 (1998).

    Article  CAS  Google Scholar 

  12. H. Hopster, Phys. Rev. Lett. 83, 1227 (1999).

    Article  CAS  Google Scholar 

  13. J. Barnes, L. Mei, B.M. Lairson, and F.B. Dunning, Rev. Sci. Instrum. 70, 246 (1999).

    Article  CAS  Google Scholar 

  14. G. Steierl, H.P. Oepen, and J. Kirschner, to be published.

    Google Scholar 

  15. J. Kessler: “Polarized Electrons”, 2nd edn., Springer, Berlin, 1985.

    Google Scholar 

  16. T.J. Gay and F.B. Dunning, Rev. Sci. Instrum. 63, 1635 (1992).

    Article  CAS  Google Scholar 

  17. G.C. Burnett, T.J. Monroe, and F.B. Dunning, Rev. Sci. Instrum. 65, 1893 (1994).

    Article  CAS  Google Scholar 

  18. J. Unguris, D.T. Pierce, and R.J. Cellota, Rev. Sci. Instrum. 57, 1314 (1986)

    Article  CAS  Google Scholar 

  19. M.R. Scheinfein, D.T. Pierce, J. Unguris, J.J. McClelland, R.J. Celotta, and M.H. Kelley, Rev. Sci. Instrum. 60, 1 (1989).

    Article  CAS  Google Scholar 

  20. J. Kirschner and R. Feder, Phys. Rev. Lett. 42, 1008 (1979).

    Article  CAS  Google Scholar 

  21. J. Kirschner: “Polarized Electrons at Surfaces”, Springer, Berlin, 1985.

    Google Scholar 

  22. G.G. Hembree, J. Unguris, R.J. Celotta, and D.T. Pierce, Scanning Microsc. Intern. Suppl. 1, 229 (1987).

    Google Scholar 

  23. K. Koike, H. Matsuyama, and K. Hayakawa, Scanning Microsc. Intern. Suppl. 1, 241 (1987).

    Google Scholar 

  24. K. Koike, H. Matsuyama, K. Hayakawa, K. Mitsuoka, S. Narishige, Y. Sugita, K. Shiiki, and C. Saka, Appl. Phys. Let. 49, 980 (1986).

    Article  CAS  Google Scholar 

  25. H.P. Oepen and J. Kirschner, Phys. Rev. Lett. 62, 819 (1989).

    Article  CAS  Google Scholar 

  26. M.R. Scheinfein, J. Unguris, R.J. Celotta, and D.T. Pierce, Phys. Rev. Lett. 63, 668 (1989).

    Article  CAS  Google Scholar 

  27. J. Unguris, to be published in: “Magnetic Imaging and Its Application to Materials”, see http://physics.nist.gov/Divisions/Div841/Gp3/epg_files/pub.html.

    Google Scholar 

  28. J. Kirschner and S. Suga, Solid State Commun. 64, 997 (1987).

    Article  CAS  Google Scholar 

  29. M.R. Scheinfein, J. Unguris, M.H. Kelley, and R.J. Celotta, Rev. Sci. Instrum. 61, 2501 (1990).

    Article  CAS  Google Scholar 

  30. T. Kohashi, H. Matsuyama, and K. Koike, Rev. Sci. Instrum. 66, 5537 (1995).

    Article  CAS  Google Scholar 

  31. J.L. Robins, R.J. Celotta, J. Unguris, D.T. Pierce, B.T. Jonker, and G.A. Prinz, Appl. Phys. Lett. 52, 1918 (1988).

    Article  CAS  Google Scholar 

  32. H.P. Oepen, M. Benning, H. Ibach, C.M. Schneider, and J. Kirschner, J. Magn. Magn. Mater. 86, L137 (1990).

    Article  CAS  Google Scholar 

  33. R. Allenspach, M. Stampanoni, and A. Bischof, Phys. Rev. Lett. 65, 3344 (1990).

    Article  CAS  Google Scholar 

  34. H. Matsuyama and K. Koike, J. Electron. Microsc. 43, 157 (1994).

    Google Scholar 

  35. T. Kohashi and K. Koike, Jpn. J. Appl. Phys. 40, L1264 (2001).

    Article  CAS  Google Scholar 

  36. R. Allenspach, IBM J. Res. Develop. 44, 553 (2000).

    Article  CAS  Google Scholar 

  37. See Chapter 4 in G. Prinz (eds.). Plenum Press, New York. p. 657. [48].

    Google Scholar 

  38. E. Kisker, W. Gudat, and K. Schröder, Solid State Commun. 44, 591 (1982).

    Article  CAS  Google Scholar 

  39. J. Unguris, D.T. Pierce, A. Galejs, and R.J. Cellota, Phys. Rev. Lett. 49, 72 (1982).

    Article  CAS  Google Scholar 

  40. H. Hopster, R. Raue, E. Kisker, G. Güntherodt, and M. Campagna, Phys. Rev. Lett. 50, 70 (1983).

    Article  CAS  Google Scholar 

  41. M.S. Hammond, G. Fahsold, and J. Kirschner, Phys. Rev. B 45, 6131 (1992).

    Article  CAS  Google Scholar 

  42. J. Kirschner in “Surface and interface characterization by electron optical methods”, A. Howie & U. Valdré (eds), Plenum Publishing Corporation, 267.

    Google Scholar 

  43. H.C. Siegmann, D.T. Pierce, and R.J. Celotta, Phys. Rev. Lett. 46, 452 (1981).

    Article  CAS  Google Scholar 

  44. D. Tillmann, R. Thiel, and E. Kisker, Z. Phys. B 77, 1 (1989).

    Article  CAS  Google Scholar 

  45. R. Bertacco, M. Merano, and F. Ciccacci, Appl. Phys. Lett. 72, 2050 (1998).

    Article  CAS  Google Scholar 

  46. R. Bertacco, D. Onofrio, and F. Ciccacci, Rev. Sci. Instrum. 70, 3572 (1999).

    Article  CAS  Google Scholar 

  47. H.P. Oepen, unpublished.

    Google Scholar 

  48. L. Reimer: “Scanning Electron Microscopy: Physics of Image Formation and Microanalysis”, Springer Series in Optical Sciences Vol. 45, Berlin, 1985.

    Google Scholar 

  49. J. Unguris, M.R. Scheinfein, D.T. Pierce, and R.J. Cellota, Appl. Phys. Lett. 55, 2553 (1989).

    Article  CAS  Google Scholar 

  50. A. Hubert and R. Schäfer: “Magnetic Domains: The Analysis of Magnetic Microstructures”, Springer, Berlin, 1998.

    Google Scholar 

  51. U. Gradmann in “Handbook of Magnetic Materials” Vol. 7, ed. K.H.J. Buschow, North Holland, Amsterdam, 1993.

    Google Scholar 

  52. J.A.C. Bland and B. Heinrich (eds.): “Ultrathin Magnetic Structures” Vol. 1 & 2, Springer, Berlin, 1994.

    Google Scholar 

  53. M. Farle, Rep. Prog. Phys. 61, 755 (1998).

    Article  CAS  Google Scholar 

  54. C. Chappert, D. Renard, P. Beauvillain, J.P. Renard, and J. Seiden, J. Magn. Magn. Mater. 54–57, 795 (1986).

    Article  Google Scholar 

  55. F.J.A. den Broeder, D. Kuiper, A.P. van de Mosselaer, and W. Hoving, Phys. Rev. Lett. 60, 2769 (1988).

    Article  Google Scholar 

  56. C.H. Lee, H. He, F. Lamelas, W. Vavra, C. Uher, and R. Clarke, Phys. Rev. Lett. 62, 653 (1989).

    Article  CAS  Google Scholar 

  57. J. Pommier, P. Meyer, G. Pémissard, J. Ferré, P. Bruno, and D. Renard, Phys. Rev. Lett. 65, 2054 (1990).

    Article  CAS  Google Scholar 

  58. B. Voigtländer, G. Meyer, and N.M. Amer, Phys. Rev. B 44, 10354 (1991).

    Article  Google Scholar 

  59. M. Speckmann, H.P. Oepen, and H. Ibach, Phys. Rev. Lett. 75, 2035 (1995).

    Article  CAS  Google Scholar 

  60. Z. Málek and V. Kamberský, Czech. J. Phys. 21, 416 (1958).

    Article  Google Scholar 

  61. B. Kaplan and G.A. Gehring, J. Magn. Magn. Mater. 128, 111 (1993).

    Article  CAS  Google Scholar 

  62. Y.T. Millev and J. Phys. Cond. Matt. 8, 3671 (1996).

    Article  CAS  Google Scholar 

  63. H.P. Oepen, M. Speckmann, Y.T. Millev, and J. Kirschner, Phys. Rev. B 55, 2752 (1997).

    Article  CAS  Google Scholar 

  64. M. Dreyer, M. Kleiber, A. Wadas, and R. Wiesendanger, Phys. Rev. B 59, 4273 (1999).

    Article  CAS  Google Scholar 

  65. P. Beauvillain, A. Bounouh, C. Chappert, R. Mégy, S. Ould-Mahfoud, J.P. Renard, P. Veillet, D. Weller, and J. Corno, J. Appl. Phys. 76, 6078 (1994).

    Article  CAS  Google Scholar 

  66. J. Kohlhepp and U. Gradmann, J. Magn. Magn. Mater. 139, 347 (1995).

    Article  CAS  Google Scholar 

  67. B.N. Engel, M.H. Wiedmann, R.A. Van Leeuwen, and C.M. Falco, Phys. Rev. B 48, 9894 (1993).

    Article  CAS  Google Scholar 

  68. H.B.G. Casimir, J. Smit, U. Enz, J.F. Fast, H.P.J. Wijn, E.W. Gorter, A.J.W. Duyvesteyn, J.D. Fast, and J.J. de Jong, J. Phys. Radium 20, 360 (1959).

    Google Scholar 

  69. Y.T. Millev and J. Kirschner, Phys. Rev. B 54, 4137 (1996).

    Article  CAS  Google Scholar 

  70. D.P. Pappas, K.-P. Kämper, and H. Hopster, Phys. Rev. Lett. 64, 3179 (1990).

    Article  CAS  Google Scholar 

  71. D.P. Pappas, C.R. Brundle, and H. Hopster, Phys. Rev. B 45, 8169 (1992).

    Article  CAS  Google Scholar 

  72. R. Allenspach and A. Bischof, Phys. Rev. Lett. 69, 3385 (1992).

    Article  CAS  Google Scholar 

  73. T. Duden and E. Bauer, Mater. Res. Soc. Symp. Proc. 475, 273 (1997).

    Google Scholar 

  74. E.Y. Vedmedenko, H.P. Oepen, and J. Kirschner, Phys. Rev. B submitted.

    Google Scholar 

  75. C. Liu, E.R. Moog, and S.D. Bader, Phys. Rev. Lett. 60, 2422 (1988).

    Article  CAS  Google Scholar 

  76. J. Thomassen, F. May, B. Feldmann, M. Wuttig, and H. Ibach, Phys. Rev. Lett. 69, 3831 (1992).

    Article  CAS  Google Scholar 

  77. C. Kittel, Phys. Rev. 70, 965 (1946).

    Article  CAS  Google Scholar 

  78. R. Carey & E.D. Isaac: “Magnetic Domains and Techniques for Their Observation”, The English Universities Press Limited, London, 1966.

    Google Scholar 

  79. H.P. Oepen, J. Magn. Magn. Mater. 93, 116 (1991).

    Article  CAS  Google Scholar 

  80. E. Feldtkeller in Proceedings of the International Symposium held in Clausthal-Göttingen, eds.: R. Niedermayer and H. Mayer, Van de Hoeck & Ruprecht, Göttingen, 1966.

    Google Scholar 

  81. P. Krams, F. Lauks, R.L. Stamps, B. Hillebrands, and G. Güntherodt, Phys. Rev. Lett. 69, 3674 (1992).

    Article  CAS  Google Scholar 

  82. A. Berger, U. Linke, and H.P. Oepen, Phys. Rev. Lett. 68, 839 (1992).

    Article  CAS  Google Scholar 

  83. L. Néel, Compt. Rend. Acad. Sci. Paris, 241, 533 (1955).

    Google Scholar 

  84. E. Feldtkeller, Z. Angew. Phys. 15, 206 (1963).

    CAS  Google Scholar 

  85. R. Kirchner and W. Döring, J. Appl. Phys. 39, 855 (1968).

    Article  CAS  Google Scholar 

  86. H. Riedel and A. Seeger, Phys. Stat. Sol. (b) 46, 377 (1971).

    Google Scholar 

  87. A. Berger and H.P. Oepen, Phys. Rev. B 45, 12596 (1992).

    Article  CAS  Google Scholar 

  88. E.E. Huber Jr., D.O. Smith, and J.B. Goodenough, J. Appl. Phys. 29, 294 (1958).

    Article  Google Scholar 

  89. R.M. Moon, J. Appl. Phys. 30, 82S (1959).

    Google Scholar 

  90. S. Methfessel, S. Middelhook, and H. Thomas, J. Appl. Phys. 31, 302S (1960).

    Article  Google Scholar 

  91. S. Middelhook, J. Appl. Phys. 34, 1054 (1963).

    Article  Google Scholar 

  92. G. Steierl, W. Lutzke, H.P. Oepen, S. Tegen, C.M. Schneider, and J. Kirschner, Magnetoelektronik, Beiträge zum BMBF-Statusseminar Magnetoelektronik, Dresden 2000, VDI-Technologiezentrum, Düsseldorf, 341 (2000).

    Google Scholar 

  93. P. Grünberg, R. Schreiber, Y. Pang, M.B. Brodsky, and H. Sowers, Phys. Rev. Lett. 57, 2442 (1986).

    Article  Google Scholar 

  94. M.N. Baibich, J.M. Broto, A. Fert, F. Nguyen Van Dau, F. Petroff, P. Etienne, G. Creuzet, A. Friederich, and J. Chazelas, Phys. Rev. Lett 61, 2472 (1988).

    Article  CAS  Google Scholar 

  95. S.S.P. Parkin, N. More, and K.P. Roche, Phys. Rev. Lett. 64, 2304 (1990).

    Article  CAS  Google Scholar 

  96. J. Unguris, R.J. Celotta, and D.T. Pierce, Phys. Rev. Lett. 67, 140 (1991).

    Article  CAS  Google Scholar 

  97. D.T. Pierce, J.A. Stroscio, J. Unguris, and R.J. Celotta, Phys Rev. B 49, 14564 (1994).

    Article  CAS  Google Scholar 

  98. D.T. Pierce, J. Unguris, R.J. Celotta, and M.D. Stiles, J. Magn. Magn. Mater. 200, 290 (1999).

    Article  CAS  Google Scholar 

  99. J. Unguris, R.J. Celotta, D.T. Pierce, and J.A. Stroscio, J. Appl. Phys. 73, 5984 (1993).

    Article  Google Scholar 

  100. J. Unguris, R.J. Celotta, and D.T. Pierce, J. Magn. Magn. Mater. 127, 205 (1993).

    Article  CAS  Google Scholar 

  101. J. Unguris, R.J. Celotta, and D.T. Pierce, J. Appl. Phys. 75, 6437 (1994).

    Article  CAS  Google Scholar 

  102. J. Unguris, R.J. Celotta, and D.T. Pierce, Phys. Rev. Lett. 79, 2734 (1997).

    Article  CAS  Google Scholar 

  103. D.A. Tulchinsky, J. Unguris, and R.J. Celotta, J. Magn. Magn. Mater. 212, 91 (2000).

    Article  CAS  Google Scholar 

  104. D.T. Pierce, A.D. Davis, J.A. Stroscio, D.A. Tulchinsky, J. Unguris, and R.J. Celotta, J. Magn. Magn. Mater. 222, 13 (2000).

    Article  CAS  Google Scholar 

  105. W.H. Meiklejohn and C.P. Bean, Phys. Rev. 102, 1413 (1956).

    Article  Google Scholar 

  106. J. Nouges and I.K. Schuller, J. Magn. Magn. Mater. 192, 203 (1999).

    Article  Google Scholar 

  107. T.G. Walker, A. Pang, H. Hopster, and S.F. Alvarado, Phys. Rev. Lett. 69, 1121 (1992).

    Article  CAS  Google Scholar 

  108. T.G. Walker and H. Hopster, Phys. Rev. B 48, 3563 (1993).

    Article  CAS  Google Scholar 

  109. J. Unguris, R.J. Cellota and D.T. Pierce, Phys. Rev. Lett. 69, 1125 (1992).

    Article  CAS  Google Scholar 

  110. P. Fuchs, V.N. Petrov, K. Totland, and M. Landolt, Phys. Rev. B 54, 9304 (1996).

    Article  CAS  Google Scholar 

  111. D.T. Pierce, R.J. Celotta, and J. Unguris, J. Appl. Phys. 73, 6201 (1993).

    Article  CAS  Google Scholar 

  112. H. Matsuyama, C. Haginoya, and K. Koike, Phys. Rev. Lett. 85, 646 (2000).

    Article  CAS  Google Scholar 

  113. J.C. Sloncewski, Phys Rev. Lett. 67, 3172 (1991).

    Article  Google Scholar 

  114. J.C. Slonczewski, J. Magn. Magn. Mater. 150, 13 (1995).

    Article  CAS  Google Scholar 

  115. N.C. Koon, Phys. Rev. Lett. 78, 4865 (1997).

    Article  CAS  Google Scholar 

  116. H. Hopster, J. Appl. Phys. 87, 5475 (2000).

    Article  CAS  Google Scholar 

  117. T. VanZandt, R. Browning, and M. Landolt, J. Appl. Phys. 69, 1564 (1991).

    Article  CAS  Google Scholar 

  118. Y. Iwasaki, K. Bessho,, J. Kondis, H. Ohmori, and H. Hopster, Applied Surface Science 113/114, 155 (1997).

    Article  CAS  Google Scholar 

  119. M. Haag and R. Allenspach, Geophysical Research Letters 20, 1943 (1993).

    CAS  Google Scholar 

  120. K.J. Kirk, J.N. Chapman, and C.D.W. Wilkinson, Appl. Phys. Lett. 71, 539 (1997).

    Article  CAS  Google Scholar 

  121. T. Schrefl, J. Fiedler, K.J. Kirk, and J. Chapman, J. Magn. Magn. Mater. 175, 193 (1997).

    Article  CAS  Google Scholar 

  122. G. Steirerl, G. Lin, D. Jorgov, and J. Kirschner, Rev. Sci. Instrum. 73, 4264 (2002).

    Article  CAS  Google Scholar 

  123. D.E. Eastman, Phys. Rev. B 2, 1 (1979)

    Article  Google Scholar 

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Oepen, H., Hopster, H. (2005). SEMPA Studies of Thin Films, Structures, and Exchange Coupled Layers. In: Hopster, H., Oepen, H.P. (eds) Magnetic Microscopy of Nanostructures. NanoScience and Technology. Springer, Berlin, Heidelberg. https://doi.org/10.1007/3-540-26641-0_7

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