Abstract
Piezoresponse force microscopy (PFM) was customer-built based on the commercial atomic force microscope and used to characterize ferroelectric domains of functional materials. The PFM imaging contrast mechanism, domain configuration and their evolution behavior under the inhomogeneous tip fields in ferroelectric thin film, lead-free piezoelectric ceramics and relaxor-type single crystals are presented in details in this chapter.
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References
Abplanalp M, Eng L M, Gunter P (1998) Mapping the domain distribution at ferroelectric surfaces by scanning force microscopy. Appl Phys A 66(S1):s231–s234
Abplanalp M, Fousek J, Günter P (2001) Higher order ferroic switching induced by scanning force microscopy. Phys Rev Lett 86:5799
Abplanalp M, Günter P (1998) Imaging of ferroelectric domains with sub micrometer resolution by scanning force microscopy. Proc of 11th IEEE-ISAF, Montreux, 98CH36245:423
Agronin A, Molotskii M, Rosenwaks Y, et al (2006) Dynamics of ferroelectric domain growth in the field of atomic force microscope. J. Appl. Phys. 99(10):102–104
Ahn C H, Tybell T, Antognazza L, et al (1997) Local, nonvolatile electronic writing of ppitaxial Pb(Zr0.52Ti0.48)O3/SrRuO3 heterostructures. Science 276(5315):1100–1103
Alexe M, Harnagea C, Erfurth W, et al (2000) 100 nm lateral size ferroelectric memory cells fabricated by electron-beam direct writing. Appl Phys A 70(3):247–251
Binnig G, Quate C F (1986) Atomic Force Microscope. Phys Rev Lett 56(9):930–933
Binnig G, Rohrer H, Gerber Ch (1982) Tunneling through a controllable vacuum gap. Appl Phys Lett 40(2):178–180
Birk H, Glatz-Reichenbach J, Li J, et al (1991) The local piezoelectric activity of thin polymer films observed by scanning tunneling microscopy. J Vac Sci Tech B9(2):1162–1165
Chai F K (1997) Domain switching and spatial dependence of permittivity in ferroelectric thin films. J Appl Phys 82(5):2505–2516
Chu M W, Szafraniak I, Scholz R, et al (2004) Impact of misfit dislocation on the polarization instability of epitaxial nanostructured ferroelectric perovskites. Nature material 3:87
Chu R Q, Zhang L N, Xu Z J, et al (2004) Phys Stat Sol 201: R45–R48
Colla E L, Taylor D V Tagantsev A K, et al (1998) Discrimination between bulk and interface scenarios for the suppression of the switchable polarization (fatigue) in Pb(Zr,Ti)O3 thin films capacitors with Pt electrodes. Appl Phys Lett 72(19):2748–2750
Dunn S, Shaw C P, Huang Z, et al (2002) Ultrahigh resolution of lead zirconate titanate 30/70 domains as imaged by piezoforce microscopy. Nanotechnology 13:456–459
Franke K, Besold J, Haessler W, et al (1992) Modification and detection of domains on ferroelectric PZT films by scanning force microscopy. Surf Sci Lett 302(1–2): L283–L288
Fu H, Cohen R E (2000) Polarization rotation mechanism for ultrahigh electromechanical response in single-crystal piezoelectrics. Nature 403(20):281–283
Gopalan V, Mitchell T E (1998) Wall velocities, switching times, and the stabilization mechanism of 180° domains in congruent LiTaO3 crystals. J Appl Phys 83(2):941–954
Gruverman A and Tokumoto H (2001) On the imaging mechanism of ferroelectric domains in scanning force microscopy. Nano Letters 1(2):93–95
Gruverman A, Auciello O, Tokumoto H (1998) Imaging and control of domain structures in ferroelectric thin films via scanning force microscopy. Ann Rev Mater Sci 28:101–123
Güthner P, Dransfeld K (1992) Local poling of ferroelectric polymers by scanning force microscopy. Appl Phys Lett 61(9):1137–1139
Harnagea C (2001) Ph.D thesis, Martin Luther University, Germany
Hidaka T, Maruyama T, Saitoh M et al (1996) Formation and observation of 50 nm polarized domains in PbZr1−xTixO3 thin film using scanning probe microscope. Appl Phys Lett 68:2358–2360
Hong S, Setter N (2002) Evidence for forward domain growth being rate-limiting step in polarization switching in 〈111〉-oriented-Pb(Zr0.45Ti0.55)O3 thin-film capacitors. Appl Phys Lett 81(18):3437–3439
Hong S, Shin H, Woo J (2002) Effect of cantilever-sample interaction on piezoelectric force microscopy. Appl Phys Lett 80(8):1453–1455
Hong S, Woo J, Shin H, et al (2001) Principle of ferroelectric domain imaging using atomic force microscope. J Appl Phys 89(92):1377–1386
Ivanchik I I (1993) Spontaneous polarization screening in a single domain ferroelectric. Ferroelectrics 145:149–161
Kalinin S V, Bonnell D (2002) Contrast mechanism maps for piezoresponse force microscopy. J Mater Res 17(55):936–939
Kholkin A L, Shvartsman V V, Yu A, et al (2003) Stress-induced suppression of piezoelectric properties in PbTiO3:La thin films via scanning force microscopy. Appl Phys Lett 82(13):2127–2129
Likodimos V, et al (2000) Dynamical studies of the ferroelectric domain structure in triglycine sulfate by voltage-modulated scanning force microscopy. J Appl Phys 87(1):443–451
Martin Y, Abraham D W, Wickramasinghe H K (1988) High-resolution capacitance measurement and potentiometry by force microscopy. Appl Phys Lett 52(13):1103–1105
Martin Y, Wickramasinghe H K (1987) Magnetic imaging by “force microscopy” with 1000 Å resolution. Appl Phys Lett 50(20):1455–1457
Martin Y, Williams C C, Wickramasinghe H K (1987) Atomic force microscope—force mapping and profiling on a sub 100Å scale. J Appl Phys 61(10):4723–4729
Mate C M, McClelland G M, Erlandsson R, et al (1987) Atomicscale friction of a tungsten tip on a graphite surface. Phys Rev Lett 59(17):1942–1945
Molotskii M (2003) Generation of ferroelectric domains in atomic force microscope. J Appl Phys 93(10):6234–6237
Noguchi Y, Miyayama M (2001) Large remanent polarization of vanadium-doped Bi4Ti3O12. Appl Phys Lett 78(913):1903–1905
Nonnemacher M, O’Boyle M P, Wickramasinghe H K (1991) Kelvin probe force microscopy. Appl Phys Lett 58(25):2921–2923
Paruch P, Giamarchi T, Tybell T, et al (2006) Nanoscale studies of domain wall motion in epitaxial ferroelectric thin films. J Appl Phys 100(5):051608
Pertsev N A, Zembilgotor A G, Tagantsev A K (1998) Effect of Mechanical Boundary Conditions on Phase Diagrams of Epitaxial Ferroelectric Thin Films. Phys Rev Lett 80(9):1988–1991
Rodriguez B J, R. Nemanich J, Kingon A, et al (2005) Domain growth kinetics in lithium niobate single crystals studied by piezoresponse force microscopy. Appl Phys Lett 86(1):012906
Sarid D, Elings J (1991) Review of scanning force microscopy. J. Vac Sci Technol B 9(2):431–437
Service R F (1997) Shape-changing crystals get shiftier. Science 275(5308):1877–1878
Synge E H (1928) A suggested method for extending the resolution into the ultra-microscopic region. Phil Mag 6:356–362
Tagantsev A K (1996) Mechanisms of polarization switching in ferroelectric thin films. Ferroelectrics 184:79–88
Tybell T, Paruch P, Giamarchi T, et al (2002) Domain wall creep in epitaxial ferroelectric Pb(Zr0.2Ti0.8)O3 thin films. Phys Rev Lett 89(9):097601
Xu Z, Kim M C, Li J F, et al (1996) Observation of a sequence of domain-like states with increasing disorder in ferroelectrics. Phil Mag A 74(1):395–406
Yin J, Cao W (2001) Polarization reversal study using ultrasound. Appl Phys Lett 79(27):4556–4558
Yu H F, Zeng H R, Zhang L N, et al (2005) In-situ characterization of local domain structure and elasticity in Nb-doped Bi4Ti3O12 piezoelectric ceramics by scanning probe microscopy. Material Letters 59(12):1538–5341
Yu H F, Zeng, H R, Chu R Q, et al (2004) Distribution and formation mechanism of the domain structure in PMN-PT single crystals. J Phys D: Appl Phys 37:2914–2917
Yu H F, Zeng, H R, Wang H X, et al (2005) Domain structure in tetragonal PMN-PT single crystals studied by piezoresponse force microscopy. Solid State Communications 133:311–314
Zavala G, Fendler J H, McKinstry S T (1997) Characterization of ferroelectric lead zirconate titanate films by scanning force microscopy. J Appl Phys 81(11):7480–7491
Zeng H R, Li G R, Yin Q R, et al (2003) Nanoscale domain switching mechanism in Pb(Zr,Ti)O3 thin film. Appl Phys A 76(1):401–403
Zeng H R, Li G R, Yin Q R, et al (2003) Local characterization of compositionally graded Pb(Zr,Ti)O3 thin films by scanning force microscope. Mater Sci and Eng B 99(1–3):234–237
Zeng H R, Shimamura K, Villora E A G, et al (2007) Domain growth kinetics and wall strain behavior in BaMgF4 ferroelectric crystal by piezoresponse force microscopy. J Apple phys 101: 074109
Zeng H R, Shimamura K, Villora E A G, et al (2007) Piezoresponse imaging and local characterization of ferroelectric domains in Pb(Zn1/3Nb2/3)O3-7%PbTiO3 single crystals. Physics Status Solidi: Rapid Research Letter 1(2):R62–R64
Zeng H R, Yin Q R, Li G R (2003) Abnormal piezoresponse of relaxor ferroelectric PMN-PT single crystal. Science Bulletin (in Chinese) 48(10):1023–1026
Zeng H R, Yu H F, Li G R, et al (2005) Local elasticity imaging of domain structures in ferroelectrics. Solid State Communication 133(8):521–525
Zeng Huarong (2003) Scanning force microscopy of nanoscale ferroelectric domains. Ph.D. Thesies, Shanghai Institute of Ceramics, Chinese Academy of Sciences
Zeng H R, Yu H F, Chu R Q, et al (2004) Domain orientation imaging of PMN-PT single crystals by vertical and lateral piezoresponse force microscopy. J Cryst Growth 267(1–2):194–198
Zeng H R, Yu H F, Chu R Q, et al (2005) Spatial inhomogeneity of ferroelectric domain structure in PMN-PT single crystals. Material Letter 59(2–3):238–240
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© 2009 Metallurgical Industry Press, Beijing and Springer-Verlag GmbH Berlin Heidelberg
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(2009). Piezoresponse Force Microscopy of Functional Ceramics. In: Microstructure, Property and Processing of Functional Ceramics. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-01694-3_4
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DOI: https://doi.org/10.1007/978-3-642-01694-3_4
Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-642-01693-6
Online ISBN: 978-3-642-01694-3
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