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Inorganic Cryogels

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Polymeric Cryogels

Part of the book series: Advances in Polymer Science ((POLYMER,volume 263))

Abstract

Recent advances in the application of cryogels in the synthesis and processing of inorganic as well as carbon-based materials are briefly summarized. Synthesis of complex oxides by using polymeric cryogels causes a substantial reduction in phase formation temperature and thus promotes a significant decrease in grain size. Freeze-drying of co-precipitated gels and residues prevents the agglomeration of nanocrystallites usually observed during atmospheric drying. This feature is also widely used for the isolation of nanoparticles prepared by various wet chemical methods. Ceramic materials with oriented tubular pores and mesoporous pore walls can be obtained by using directed crystallization of ice from ceramic slurries. Carbon cryogels with a specific surface area of up to 2,000 m2 g−1 can be prepared by thermal processing of the corresponding polymeric precursors. Cryogel-derived composites of carbon nanotubes and graphene-based materials with various oxides demonstrate outstanding mechanical properties and enhanced electrical conductivity.

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Abbreviations

CNT:

Carbon nanotubes

FESEM:

Field emission SEM

GO:

Graphene oxide

HAP:

Hydroxyapatite

RGO:

Reduced graphene oxide

RF:

Resorcinol-formaldehyde

SEM:

Scanning electron microscopy

TEM:

Transmission electron microscopy

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Acknowledgements

Partial support by the Russian Foundation for Basic Research (grant 12-08-01241a) is gratefully acknowledged.

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  1. Inorganic Chemistry Division, Department of Chemistry, M.V. Lomonosov Moscow State University, 119991, Moscow, Russia

    Oleg A. Shlyakhtin

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  1. Oleg A. Shlyakhtin
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Correspondence to Oleg A. Shlyakhtin .

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  1. Department of Chemistry, Istanbul Technical University, Istanbul, Turkey

    Oguz Okay

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Shlyakhtin, O.A. (2014). Inorganic Cryogels. In: Okay, O. (eds) Polymeric Cryogels. Advances in Polymer Science, vol 263. Springer, Cham. https://doi.org/10.1007/978-3-319-05846-7_6

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