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Advanced Materials pp 15–26Cite as

The Effect of Mechanical Activation on the Synthesis and Properties of Multiferroic Lead Iron Niobate

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Part of the book series: Springer Proceedings in Physics ((SPPHY,volume 152))

Abstract

The present work studies the effect of high-energy mechanical activation using the planetary-centrifugal ball mill AGO-2 and subsequent annealing on the synthesis and magnetic properties of PbFe0.5Nb0.5O3 (PFN). This technique enables one to perform the mechanically activated synthesis of PFN at much shorter time. The results of X-ray phase analysis, electron microscopic studies and transmission Mössbauer 57Fe spectra measurement are presented and discussed. Mössbauer studies show that the temperature of magnetic phase transition in PbFe0.5Nb0.5O3 powders can be changed by mechanical activation and subsequent annealing.

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Acknowledgments

This work was partially supported by the Russian Foundation for Basic Research (RFBR) by grants #13-03-00869_a, #12-08-00887_a, and the Research Committee of the University of Macau under Research & Development Grant for Chair Professor. Dr. Raevskaya S. I. thanks the Southern Federal University for financial support in fulfillment of this research.

Author information

Authors and Affiliations

  1. Institute of Solid State Chemistry and Mechanochemistry SB RAS, Novosibirsk, Russia

    A. A. Gusev, E. G. Avvakumov & V. P. Isupov

  2. Research Institute of Physics, and Physical Faculty, Southern Federal University, Rostov-on-Don, Russia

    I. P. Raevski, S. P. Kubrin, D. A. Sarychev, V. V. Titov, S. I. Raevskaya & V. V. Stashenko

  3. University of Macau, Macau, China

    H. Chen

  4. National Taiwan University of Science and Technology, Taipei, 10607, Republic of China (Taiwan)

    C.-C. Chou

  5. Institute of Automation and Electrometry, SB RAS, Novosibirsk, Russia

    A. M. Pugachev

Authors
  1. A. A. Gusev
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  2. I. P. Raevski
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  3. E. G. Avvakumov
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  4. V. P. Isupov
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  5. S. P. Kubrin
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  6. H. Chen
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  7. C.-C. Chou
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  8. D. A. Sarychev
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  9. V. V. Titov
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  10. A. M. Pugachev
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  11. S. I. Raevskaya
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  12. V. V. Stashenko
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Corresponding author

Correspondence to S. I. Raevskaya .

Editor information

Editors and Affiliations

  1. Dept. of Microelectronics Engineering, National Kaohsiung Marine University, Kaohsiung, Taiwan

    Shun-Hsyung Chang

  2. Mechanics and Applied Mathematics Research Inst., Southern Federal University, Rostov-on-Don, Russia

    Ivan A. Parinov

  3. Dept. Physics, Southern Federal University, Rostov on Don, Russia

    Vitaly Yu. Topolov

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© 2014 Springer International Publishing Switzerland

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Gusev, A.A. et al. (2014). The Effect of Mechanical Activation on the Synthesis and Properties of Multiferroic Lead Iron Niobate. In: Chang, SH., Parinov, I., Topolov, V. (eds) Advanced Materials. Springer Proceedings in Physics, vol 152. Springer, Cham. https://doi.org/10.1007/978-3-319-03749-3_2

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