Abstract
The 13C NMR methods which can be used to study the local dynamics of solid samples through the cross-polarization and magic angle spinning technique are briefly reviewed. We present results obtained on solid polycycloalkyl methacrylates, polybutylene terephtalate, polystyrene and substituted polystyrenes and compare them with mechanical relaxation measurements.
This is a preview of subscription content, log in via an institution.
Preview
Unable to display preview. Download preview PDF.
References
Havens, J.R., Koenig, J.L., Appl. Spectroscopy 1983, 37, 226
Abragam, A., “The Principles of Nuclear Magnetism”, Oxford University, 1961
Wehrli, F.W., Wirthlin, T., “Interpretation of Carbon-13 N.M.R. spectra”, Heyden, London, 1976
Farrar, T.C., Becker, E.D., “Pulse and Fourier Transform N.M.R.”, Academic Press, New York, 1971
Mehring, M., “High Resolution N.M.R. Spectroscopy in Solids”, N.M.R., Vol. 11, Springer Verlag, Berlin, 1976
Heijboer, J., Ph.D. Theses, University of Leyden, 1972
Lauprêtre, F., Monnerie, L., Virlet, J., Macromolecules, 1984, 17, 1397
Lauprêtre, F., Virlet, J., Bayle, J.P., Macromolecules, 1985, 18, 1846
Jelinski, L.W., Schilling, F.C., Bovey, F.A., Macromolecules, 1981, 14, 1341
Jelinski, L.W., Macromolecules, 1981, 14, 1341
Jelinski, L.W., Dumais, J.J., Engel, A.K., Macromolecules, 1983, 16, 403
Jelinski, L.W., Dumais, J.J., Watnick, P.I., Engel, A.K., Sefcik, M.D., Macromolecules, 1983, 16, 409
Jelinski, L.W., Dumais, J.J., Engel, A.K., Macromolecules, 1983, 16, 492
Cholli, A.L., Dumais, J.J., Engel, A.K., Jelinski, L.W., Macromolecules, 1984, 17, 2399
Helfand, E., J. Chem. Phys., 1971, 54, 4651
Schatzki, T.F., Polym. Prepr. Am. Chem. Soc., Div. Polym. Chem., 1965, 6, 646
Gény, F., Monnerie, L., J. Polym. Sci., Polym. Phys. Ed., 1979, 17, 131, 147
Skolnick, J., Helfand, E., J. Chem. Phys., 1980, 72, 5489
Schaefer, J., Sefcik, M.D., Stejskal, E.O., Mc.Kay, R.A., Dixon, W.T., Cais, R.E., Macromolecules, 1984, 17, 1107
Gorin, S., J. Chim. Phys. (Fr.), 1970, 67, 878
Lauprêtre, F., Noël, C., Monnerie, L., J. Polym. Sci., Polym. Phys. Ed., 1977, 15, 2127
Garroway, AX, Ritchey, W.M., Moniz, W.B., Macromolecules, 1985, 15, 1051
Author information
Authors and Affiliations
Editor information
Rights and permissions
Copyright information
© 1987 Springer-Verlag
About this paper
Cite this paper
Monnerie, L. (1987). 13C NMR investigation of local motions involved in secondary relaxation of polymers. In: Dorfmüller, T., Williams, G. (eds) Molecular Dynamics and Relaxation Phenomena in Glasses. Lecture Notes in Physics, vol 277. Springer, Berlin, Heidelberg. https://doi.org/10.1007/3-540-17801-5_8
Download citation
DOI: https://doi.org/10.1007/3-540-17801-5_8
Published:
Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-540-17801-9
Online ISBN: 978-3-540-47838-6
eBook Packages: Springer Book Archive