Skip to main content
SpringerLink
Log in

Investigation of Fe-Co catalyst active component during multi-walled carbon nanotube synthesis by means of synchrotron radiation X-ray diffraction

  • Published:
Bulletin of the Russian Academy of Sciences: Physics Aims and scope

Abstract

The investigation of the catalyst active component formation during multi-walled carbon nanotube (MWCNT) synthesis was carried out by means of in situ and ex situ synchrotron radiation X-ray diffraction. The data on phase composition transformations obtained with 1 s time-resolution allows optimization the carbon nanotubes synthesis in industrial fluidized bed reactors.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Dresselhaus, M.S., Dresselhaus, G., and Eklund, P.C., Science of Fullerences and Carbon Nanotubes, San Diego Acad. Press, 1996.

    Google Scholar 

  2. Eletskii, A.V., Usp. Fiz. Nauk, 1997, vol. 167, pp. 945–972.

    Article  Google Scholar 

  3. Harris, P.J.F., in Novye materily XXI (New Materials of 21st Century), Moscow: Tekhnosfera, 2003, p. 336.

    Google Scholar 

  4. Rakov, E.G., Usp. Khim., 2001, vol. 70, no. 10, pp. 934–973.

    Article  Google Scholar 

  5. Carbon Nanotechnology, Dai, L., Ed., Amsterdam, Oxford: Elsevier, 2006.

    Google Scholar 

  6. D’yachkov, P.N., Elektronnye svoistva i primenenie nanotrubok (Nanotubes: Electronic Properties and Application), Moscow: BINOM, 2010.

    Google Scholar 

  7. See, C.H. and Harris, A.T., Ind. Eng. Chem. Res., 2007, vol. 46, no. 4, pp. 997–1012.

    Article  Google Scholar 

  8. Couteau, E., Hernadi, K., Seo, J.W., et al., Chem. Phys. Lett., 2003, vol. 378, p. 9.

    Article  ADS  Google Scholar 

  9. Kathyayini, H., Nagaraju, N., Fonseca, A., and Nagy, J.B., J. Mol. Catal. A, 2004, vol. 223, p. 129.

    Article  Google Scholar 

  10. Seo, J.W., Magrez, A., Milas, M., et al., J. Phys. D: Appl. Phys., 2007, vol. 40, p. 109.

    Article  ADS  Google Scholar 

  11. Mionic, M., Alexander, D.T.L., Forro, L., and Magrez, A., Phys. Status. Solidi. (b), 2008, vol. 245, p. 1915.

    Article  ADS  Google Scholar 

  12. See, C.H. and Harris, A.T., Amer. Instit. Chem. Eng. J., 2008, vol. 54, p. 657.

    Article  Google Scholar 

  13. Usoltseva, A., Kuznetsov, V., Rudina, N., Moroz, E., Haluska, M., and Roth, S., Phys. Status Solidi B, 2007, vol. 244, p. 3920.

    Article  ADS  Google Scholar 

  14. Aulchenko, V.M. and Kutovenko, V.D., Nucl. Instrum. Methods. Phys. Res. A, 2009, vol. 603, pp. 76–79.

    Article  ADS  Google Scholar 

  15. West, A.R., Solid State Chemistry and Its Applications, John Wiley & Sons, 1984; Moscow: Mir, 1988, vol. 1.

    Google Scholar 

  16. www.calphad.com/phase-diagrams.html

Download references

Author information

Authors and Affiliations

  1. Boreskov Institute of catalysis SBRAS, Novosibirsk, 630090, Russia

    D. V. Krasnikov, A. N. Shmakov, V. L. Kuznetsov, K. V. Elumeeva & A. V. Ishchenko

  2. Novosibirsk State University, Novosibirsk, 630090, Russia

    D. V. Krasnikov & V. L. Kuznetsov

Authors
  1. D. V. Krasnikov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. A. N. Shmakov
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. V. L. Kuznetsov
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. K. V. Elumeeva
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. A. V. Ishchenko
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to V. L. Kuznetsov.

Additional information

Original Russian Text © D.V. Krasnikov, A.N. Shmakov, V.L. Kuznetsov, K.V. Elumeeva, A.V. Ishchenko, 2013, published in Izvestiya Rossiiskoi Akademii Nauk. Seriya Fizicheskaya, 2013, Vol. 77, No. 2, pp. 177–180.

The article was translated by the authors.

About this article

Cite this article

Krasnikov, D.V., Shmakov, A.N., Kuznetsov, V.L. et al. Investigation of Fe-Co catalyst active component during multi-walled carbon nanotube synthesis by means of synchrotron radiation X-ray diffraction. Bull. Russ. Acad. Sci. Phys. 77, 155–158 (2013). https://doi.org/10.3103/S1062873813020184

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3103/S1062873813020184

Keywords

Search

Navigation