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Synthesis of basic yttrium nitrate

  • Synthesis and Properties of Inorganic Compounds
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Abstract

The reaction between yttrium nitrate and potassium hydroxide solutions was conducted at 25 and 50°C and at the boiling point of the reaction mixture, and the reaction products were studied. The Schreinemakers method, X-ray diffraction and crystal-optical analyses, IR spectroscopy, and electron microscopy demonstrated that X-ray amorphous yttrium hydroxide Y(OH)3 and basic yttrium nitrate Y(OH)2.5(NO3)0.5 · H2O are formed at 25 and 50°C as a poorly crystallized precipitate depending on the ratio between the initial reagents. Keeping the reaction products at the boiling temperature gives rise to a well-crystallized sample of basic yttrium nitrate.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russia

    E. A. Frolova, D. F. Kondakov, A. D. Yapryntsev, A. E. Baranchikov, V. K. Ivanov & V. P. Danilov

  2. Moscow State University, Moscow, Russia

    A. D. Yapryntsev & V. K. Ivanov

Authors
  1. E. A. Frolova
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  2. D. F. Kondakov
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  3. A. D. Yapryntsev
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  4. A. E. Baranchikov
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  5. V. K. Ivanov
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  6. V. P. Danilov
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Corresponding author

Correspondence to A. E. Baranchikov.

Additional information

Original Russian Text © E.A. Frolova, D.F. Kondakov, A.D. Yapryntsev, A.E. Baranchikov, V.K. Ivanov, V.P. Danilov, 2015, published in Zhurnal Neorganicheskoi Khimii, 2015, Vol. 60, No. 3, pp. 307–312.

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Frolova, E.A., Kondakov, D.F., Yapryntsev, A.D. et al. Synthesis of basic yttrium nitrate. Russ. J. Inorg. Chem. 60, 259–264 (2015). https://doi.org/10.1134/S0036023615030043

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  • DOI: https://doi.org/10.1134/S0036023615030043

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