Skip to main content
SpringerLink
Log in

Molecular structure of 3-OXO-URS-12-EN-28-OIC acid anhydride

  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

The molecular structure of 3-oxo-urs-12-en-28-oic acid anhydride is determined. Crystals of C60H90O5 compound (III) are monoclinic, space group С2, at 100 K a = 15.1308(13) Å, b = 23.5150(19) Å, c = 15.1275(12) Å, β = 108.276(2)°. Molecules in the crystal are located in a special position on axis 2.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. T. Honda, E. M. Padegimas, E. David, C. Sundararajan, K. T. Liby, C. Williams, M. B. Sporn, and M. Visnick, Bioorg. Med. Chem. Lett., 20, No. 7, 2275 (2010).

    Article  CAS  Google Scholar 

  2. O. B. Kazakova, G. V. Giniyatullina, G. A. Tolstikov, V. E. Kataev, and R. Z. Musin, Russ. J. Bioorg. Chem., 35, No. 5, 714 (2009).

    Article  CAS  Google Scholar 

  3. I. E. Smirnova, E. V. Tretyakova, O. B. Kazakova, L. V. Spirikhin, G. A. Tolstikov, V. E. Kataev, and R. Z. Musin, Chem. Nat. Compd., 46, No. 3, 324 (2010).

    Article  Google Scholar 

  4. R. N. Khaybullin, I. Yu. Strobykina, A. B. Dobrynin, A. T. Gubaydullin, R. V. Chestnova, V. M. Babaev, and V. E. Kataev, Bioorg. Med. Chem. Lett., 22, No. 22, 6909 (2012).

    Article  CAS  Google Scholar 

  5. X. Liu, B. Shi, and B. Yu, Tetrahedron, 60, No. 50, 11647 (2004).

    Article  CAS  Google Scholar 

  6. H. Nakai, Acta Crystallogr., C45, 1465 (1989).

    CAS  Google Scholar 

  7. V. E. Kataev, O. I. Militsina, I. Yu. Strobykina, A. T. Gubaidullin, V. V. Zverev, O. N. Kataeva, O. V. Fedorova, M. S. Valova, and G. L. Rusinov, J. Inclusion Phenom., 60, Nos. 1/2, 51 (2008).

    Article  CAS  Google Scholar 

  8. V. E. Kataev, A. P. Timosheva, A. I. Nugmanov, I. Yu. Strobykina, R. R. Shagidullin, L. V. Avvakumova, and O. I. Militsina, Russ. J. Gen. Chem., 77, No. 6, 981 (2007).

    Article  Google Scholar 

  9. D. M. Doddrell, D. A. Pegg, and M. R. Bendall, J. Magn. Res., 48, No. 15, 323 (1982).

    CAS  Google Scholar 

  10. K. Nagayama, A. Kumar, K. Wuthrich, and R. R. Ernst, J. Magn. Res., 40, No. 2, 321 (1980).

    CAS  Google Scholar 

  11. W. P. Aue, E. Bartholdi, and R. R. Ernst, J. Chem. Phys., 64, No. 5, 2229 (1976).

    Article  CAS  Google Scholar 

  12. A. L. Davis, J. Keeler, E. D. Laue, and D. Moskau, J. Magn. Res., 98, No. 1, 207 (1992).

    CAS  Google Scholar 

  13. R. E. Hurd and B. K. John, J. Magn. Res., 91, No. 3, 648–653 (1991).

    CAS  Google Scholar 

  14. W. Willker, D. Leibfritz, R. Kerssebaum, and W. Bermel, Magn. Res. Chem., 31, No. 3, 287 (1993).

    Article  CAS  Google Scholar 

  15. J. Jeener, B. H. Meier, P. Bachmann, and R. R. Ernst, J. Chem. Phys., 71, No. 11, 4546 (1979).

    Article  CAS  Google Scholar 

  16. R. Wagner and S. Berger, J. Magn. Res. A, 123, No. 1, 119 (1996).

    Article  CAS  Google Scholar 

  17. APEX2, Bruker AXS Inc., Madison, Wisconsin, USA (2009).

  18. G. M. Sheldrick, Acta Crystallogr., A64, 112 (2008).

    Article  Google Scholar 

  19. O. B. Kazakova, E. V. Tretyakova, O. S. Kukovinets, A. R. Abdrakhmanova, N. N. Kabalnova, D. V. Kazakov, G. A. Tolstikov, and A. T. Gubaidullin, Tetrahedron Lett., 51, No. 14, 1832 (2010).

    Article  CAS  Google Scholar 

  20. O. B. Kazakova, D. V. Kazakov, E. Yu. Yamansarov, N. I. Medvedeva, G. A. Tolstikov, K. Yu. Suponitsky, and D. E. Arkhipov, Tetrahedron Lett., 52, No. 9, 976 (2011).

    Article  CAS  Google Scholar 

  21. O. B. Kazakova, E. Yu. Yamansarov, O. S. Kukovinets, N. I. Medvedeva, D. V. Kazakov, O. K. Kornilov, and K. Yu. Suponitskii, Chem. Nat. Compd., 47, No. 5, 738 (2011).

    Article  CAS  Google Scholar 

  22. O. B. Kazakova, E. F. Khusnutdinova, N. I. Medvedeva, A. N. Lobov, and K. Yu. Suponitskii, J. Struct. Chem., 53, No. 5, 954 (2012).

    Article  CAS  Google Scholar 

  23. O. B. Kazakova, I. E. Smirnova, H. Do Tkhi Tkhu, Tkhankh Tra Nguyen, G. N. Apryshko, O. S. Zhukova, N. I. Medvedeva, T. I. Nazyrov, E. V. Tretyakova, I. V. Chudov, A. F. Ismagilova, K. Yu. Suponitskii, D. V. Kazakov, F. E. Safarov, and G. A. Tolstikov, Russ. J. Bioorg. Chem., 39, No. 2, 230 (2013).

    Article  CAS  Google Scholar 

  24. A. Simon, C. Delage, M. Saux, A. J. Chulia, A. Nmid, and M. Rigaud, Acta Crystallogr., C48, 726 (1992).

    CAS  Google Scholar 

  25. H. Nakai, Acta Crystallogr., C45, 1465 (1989).

    CAS  Google Scholar 

  26. L. Yu. Ukhin, K. Yu. Suponitskii, L. V. Belousova, and Zh. I. Orlova, Russ. Chem. Bull., 58, No. 12, 2399 (2009).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Organic Chemistry, Ufa Scientific Centre, Russian Academy of Sciences, Ufa, Russia

    N. I. Medvedeva, T. V. Lopatina, A. N. Lobov, A. I. Poptsov & O. B. Kazakova

  2. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia

    K. Yu. Suponitskii

Authors
  1. N. I. Medvedeva
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. K. Yu. Suponitskii
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. T. V. Lopatina
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. A. N. Lobov
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. A. I. Poptsov
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. O. B. Kazakova
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to O. B. Kazakova.

Additional information

Original Russian Text © 2015 N. I. Medvedeva, K. Yu. Suponitskii, T. V. Lopatina, A. N. Lobov, A. I. Poptsov, O. B. Kazakova.

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 5, pp. 1010–1015, September–October, 2015.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Medvedeva, N.I., Suponitskii, K.Y., Lopatina, T.V. et al. Molecular structure of 3-OXO-URS-12-EN-28-OIC acid anhydride. J Struct Chem 56, 953–958 (2015). https://doi.org/10.1134/S0022476615050194

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476615050194

Keywords

Search

Navigation