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Synthesis and properties of calcium hydroxyapatite/silk fibroin organomineral composites

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Inorganic Materials Aims and scope

Abstract

The coprecipitation of calcium hydroxyapatite (HA) (Ca10(PO4)6(OH)3) and silk fibroin (SF) from an aqueous solution in the Ca(NO3)2–(NH4)2HPO4–NH3–H2O–SF system has been used to synthesize HA/SF organomineral composites based on nanocrystalline HA, containing 2, 5, and 10 wt % SF. The synthesis products were characterized by X-ray diffraction, thermogravimetric analysis, infrared spectroscopy, scanning electron microscopy, and electron spectroscopy for chemical analysis.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russia

    N. A. Zakharov, M. A. Orlov, T. V. Zakharova & N. T. Kuznetsov

  2. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russia

    L. I. Demina, A. D. Aliev, M. R. Kiselev & V. V. Matveev

Authors
  1. N. A. Zakharov
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  2. L. I. Demina
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  3. A. D. Aliev
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  4. M. R. Kiselev
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  5. V. V. Matveev
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  6. M. A. Orlov
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  7. T. V. Zakharova
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  8. N. T. Kuznetsov
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Correspondence to N. A. Zakharov.

Additional information

Original Russian Text © N.A. Zakharov, L.I. Demina, A.D. Aliev, M.R. Kiselev, V.V. Matveev, M.A. Orlov, T.V. Zakharova, N.T. Kuznetsov, 2017, published in Neorganicheskie Materialy, 2017, Vol. 53, No. 3, pp. 322–332.

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Zakharov, N.A., Demina, L.I., Aliev, A.D. et al. Synthesis and properties of calcium hydroxyapatite/silk fibroin organomineral composites. Inorg Mater 53, 333–342 (2017). https://doi.org/10.1134/S0020168517030128

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  • DOI: https://doi.org/10.1134/S0020168517030128

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