Growth and structure of La3Zr0.5Ga5Si0.5O14 crystals
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- Pugacheva, A.A., Maksimov, B.A., Mill’, B.V. et al. Crystallogr. Rep. (2004) 49: 53. doi:10.1134/1.1643964
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The complete X-ray structure determination of Czochralski grown La3Zr0.5Ga5Si0.5O14 single crystals with the Ca3Ga2Ge4O14 structure is performed (sp. gr. P321, a = 8.226(1) Å, c = 5.1374(6) Å, Z = 1, Mo Kα1 radiation, 1920 crystallographically independent reflections, R = 0.0166, Rw = 0.0192). The absolute structure is determined. It is shown that possible transition of some of La atoms (∼1.2%) from the 3e to 6g position may give rise to the formation of structural defects.