Monitoring Density and Temperature in C/C Composites Processing by CVI with Induction Heating

Abstract

Carbon/carbon composites are processed by chemical vapor infiltration (CVI) with radio-frequency inductive heating, which leads to inside-out temperature gradients, suitable for the production of homogeneously densified pieces if properly controlled throughout the whole processing. We present here a 2D axisymmetrical case where a comprehensive numerical model is tested against experimental runs. The numerical thermal model takes into account induction heating, radiative, conductive, and convective effects, intermediate regime diffusion and densification reactions in the pores, and the evolution of the porous medium. The results are the time evolution of the temperature, concentration, and composite material density field, as well as the input power necessary to ensure a given maximal temperature in the preform. Experimental data are measurements of the temperature and density fields at various infiltration stages. Comparison between experience and simulation, yielding an useful agreement, shows that porosity becomes trapped inside the preform as densification proceeds, because of the progressive lowering of the temperature gradient steepness. The discrepancies between computations and experimental data rely on the only approximate knowledge of some quantities, principally the reaction kinetics, which are currently under investigation.