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Covalent Attachment of Some Phenol Derivatives to the Silica Surface by Use of Single-stage Aminomethylation

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Abstract

The reaction conditions and component ratios were established for the attachment of 4-(2-pyridylazo)resorcinol (PAR), 1-(2-pyridylazo)-2-naphthol (PAN) and 8-hydroxyquinoline (8-HQ) to the silica surface by means of a single-stage Mannich reaction. The modified sorbents that were synthesized were characterized by an adsorption method, and DRIFT and UV spectroscopies. The concentrations of PAR, PAN and 8-HQ grafted to the silica surface that were attained were 2.8×10−5, 8.5×10−5 and 2.7×10−4 mol g−1, respectively.

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REFERENCES

  1. V. A. Tertykh and L. A. Belyakova, Chemical Reactions Involving Silica Surface, Naukova Dumka, Kiev 1991 (in Russian).

    Google Scholar 

  2. J. F. Biernat, P. Konieczka, B. J. Tarbet, J. S. Bradshaw and R. M. Izatt, Separation and Purification Methods, 23 (1994) 77.

    CAS  Google Scholar 

  3. V. N. Zaitsev, Complexing Silicas, Syntheses, Structure of Bonded Layer and Surface Chemistry, Folio, Khar'kov 1997 (in Russian).

    Google Scholar 

  4. H. A. M. Elmahadi and G. M. Greenway, Microchemical Journal, 53 (1996) 188.

    Article  CAS  Google Scholar 

  5. I. Kasahara, N. Takayama, H. Yamamoto, K. Sakurai and S. Taguchi, Bunseki-Kagaku, 46 (1997) 211.

    CAS  Google Scholar 

  6. F. Liu, K. A. Li, Y. S. Wu, X. Wang and S. Y. Tong, Microchemical Journal, 52 (1995) 274.

    Article  CAS  Google Scholar 

  7. Chi-Ren Lan and Mo-Hsiung Yang, Analytica Chimica Acta, 287 (1994) 101.

    Article  CAS  Google Scholar 

  8. Chi-Ren Lan and Mo-Hsiung Yang, Analytica Chimica Acta, 287 (1994) 111.

    Article  CAS  Google Scholar 

  9. Q. Pu, Z. Su, Z. Hu, X. Chang and M. Yang, J. Anal. Atomic Spectrometry, 13 (1998) 249.

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Institute of Surface Chemistry, National Academy of Sciences of Ukraine, Prospekt Nauki 31, 252022, Kyiv, Ukraine

    V. A. Tertykh, V. V. Yanishpolskii & O. Yu. Panova

Authors
  1. V. A. Tertykh
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  2. V. V. Yanishpolskii
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  3. O. Yu. Panova
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Tertykh, V.A., Yanishpolskii, V.V. & Panova, O.Y. Covalent Attachment of Some Phenol Derivatives to the Silica Surface by Use of Single-stage Aminomethylation. Journal of Thermal Analysis and Calorimetry 62, 545–549 (2000). https://doi.org/10.1023/A:1010187508531

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