Abstract
Until recently, the issue of the thermal gradients within TMDSC samples remained mostly a subject of theory and mathematical models — only the phase lag was subject to experimental verification, as this information is readily available from the analysis software of most instruments. There was no method to verify the transient behaviour and temperature gradients within a sample without making costly and intensive modifications to the equipment. Recently, however, a group of researchers were able to experimentally measure thermal profiles as a function of sample thickness with a high-speed, high-resolution infrared camera mounted on the TMDSC cell. Therefore, this paper is dedicated to comparing the predictions of our three-dimensional model with this newly available data.
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F. U. Buehler, C. J. Martin and J. C. Seferis, J. Therm. Anal. Cal., 54 (1998) 501.
F. U. Buehler and J. C. Seferis, Thermochim. Acta, 334 (1999) 49.
F. U. Buehler and J. C. Seferis, Thermochim. Acta, 348 (2000) 161.
R. Androsch, M. Pyda, H. Wang and B. Wunderlich, J. Therm. Anal. Cal., 61 (2000) 661.
H. Wang, M. Bartkowiak, F. A. Modine, R. B. Dinwiddie, L. A. Boatner and G. D. Mahan, J. American Ceramic Soc., 81 (1998) 2013.
H. Gröber and S. Erk, Fundamentals of Heat Transfer, McGraw-Hill, New York 1961.
J. Brandrup and E. H. Immergut, Polymer Handbook, Wiley, New York 1989.
Y. S. Touloukian, R. W. Powell, C. Y. Ho and M. C. Nicolaou, Thermophysical Properties of Matter Touloukian, Y. S., Ed. IFI/Penum, New York 1973.
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Buehler, F.U., Seferis, J.C. Thermal Gradients in TMDSC Samples: A comparison of theory and experimental data. Journal of Thermal Analysis and Calorimetry 63, 21–30 (2001). https://doi.org/10.1023/A:1010167815965
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DOI: https://doi.org/10.1023/A:1010167815965