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Preparation of magnetic TS-1 and its catalytic activity

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Abstract

Magnetic TS-1 was synthesized with nanosized nickelferrite particles as nuclei via the hydrothermal synthesis and solvent vaporation method. The prepared samples were characterized with N2 adsorption-desorption isotherms, FTIR spectrometry, Raman spectrometry, X-ray diffraction, Ultraviolet-visible spectroscopy and Vibrating sample magnetometry. The results show that the composite obtained was composed of TS-1 with MFI structure and NiFe2O4 with spinel structure, its specific surface area was about 316 m2/g, pore volume was 0.12 cm3/g and pore size distribution was in the range of 0.5–0.7 nm. The catalytic activity of the composite was also investigated by its catalyzing the decomposition of rhodamine B oxidized by H2O2 in aqueous solution. In this case Rhodamine B pollutant could be completely degraded within 150 min. Magnetic TS-1 exhibited high photocatalytic efficiency and super paramagnetic nature for cleaning polluted water with the help of magnetic separation.

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Authors and Affiliations

  1. School of Chemical Engineering and Environment, North University of China, Taiyuan, 030051, P. R. China

    Yu Li, Zehui Xue, Qi Zhang, Cuitao Sun, Junping Li & Laishuan Liu

Authors
  1. Yu Li
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  2. Zehui Xue
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  3. Qi Zhang
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  4. Cuitao Sun
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  5. Junping Li
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  6. Laishuan Liu
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Corresponding author

Correspondence to Yu Li.

Additional information

Supported by the Major Program of Science and Technology of Shanxi Province, China(No.20111101013).

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Li, Y., Xue, Z., Zhang, Q. et al. Preparation of magnetic TS-1 and its catalytic activity. Chem. Res. Chin. Univ. 31, 430–433 (2015). https://doi.org/10.1007/s40242-015-4434-6

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  • DOI: https://doi.org/10.1007/s40242-015-4434-6

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