Skip to main content
SpringerLink
Log in

Synthesis of Pt/C Fuel Cell Electrocatalysts: Residual Content of Chloride and Activity in Oxygen Reduction

  • Letters
  • Published:
Electrocatalysis Aims and scope Submit manuscript

Transmission electron micrographs (TEM), the corresponding Pt particle size distribution histograms, and chemical analysis for residual Cl content by instrumental neutron activation analysis (INAA) and X-ray photoelectron spectroscopy (XPS) of selected representative Pt/C fuel cell catalysts.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4

References

  1. V.S. Bagotsky, Fuel Cells, Problems and Solutions, 2nd edn. (Wiley, Hoboken, 2012). pp. 43–69

    Book  Google Scholar 

  2. J.R. Anderson, M.F. García, Supported Metals in Catalysis (Imperial College Press, London, 2012). pp. 447–456

    Google Scholar 

  3. H. Bönnemann, W. Brijoux, R. Brinkmann, R. Fretzen, T. Joussen, R. Köppler, B. Korall, P. Neiteler, J. Richter, J. Mol. Catal. 86, 129 (1994)

    Article  Google Scholar 

  4. C. Coutanceau, S. Brimaud, C. Lamy, J.M. Léger, L. Dubau, S. Rousseau, F. Vigier, Electrochim. Acta 53, 6865 (2008)

    Article  CAS  Google Scholar 

  5. C.J. Jia, F. Schüth, Phys. Chem. Chem. Phys. 132, 2457 (2011)

    Article  Google Scholar 

  6. N. Job, M. Chatenet, S. Berthon-Fabry, S. Hermans, F. Maillard, J. Power Sources 240, 294 (2013)

    Article  CAS  Google Scholar 

  7. J.X. Wang, N.M. Markovic, R.R. Adzic, J. Phys. Chem. B 108, 4127 (2004)

    Article  CAS  Google Scholar 

  8. L. Kaluža, M.J. Larsen, M. Zdražil, D. Gulková, Z. Vít, O. Šolcová, K. Soukup, M. Koštejn, J.L. Bonde, L. Maixnerová, M. Odgaard, Catal. Today 256, 375 (2015)

    Article  Google Scholar 

  9. L. Kaluža, M.J. Larsen, M. Zdražil, D. Gulková, M. Odgaard, Chem. Eng. Trans. 43, 913 (2015)

    Google Scholar 

  10. S. Cavaliere, I. Jimenez-Morales, G. Ercolano, I. Savych, D. Jones, J. Rozière, Chem. Electro. Chem. 2, 1966 (2015)

    CAS  Google Scholar 

  11. U.S. National Institute of Standards and Technology, Certificate of Analysis, Standard Reference Material 1547 (Peach Leaves, Gaithersburg, 1993) pp. 1–5

  12. A. Ohma, K. Shinohara, A. Iiyama, T. Yoshida, A. Daimaru, ECS Trans. 41, 775 (2011)

    Article  CAS  Google Scholar 

  13. S.K. Jo, X.Y. Zhu, D. Lennon, J.M. White, Surf. Sci. 241, 231 (1991)

    Article  CAS  Google Scholar 

  14. S.J. Gregg, K.S.W. Sing, Adsorption, Surface Area and Porosity, 2nd edn. (Academic, London, 1982). pp. 111–190

    Google Scholar 

Download references

Acknowledgments

Imerys Graphite & Carbon Ltd. (Switzerland) is kindly acknowledged for providing experimental moderate-surface area carbon back support. The research leading to these results has received funding from the European Union’s 7th Framework Programme (FP7/2007–2013) for the Fuel Cells and Hydrogen Joint Undertaking under Grant Agreement number 303466 with acronym IMMEDIATE. L.K. and D.G. also highly appreciate and acknowledge the co-financing of the Ministry of Education, Youth and Sports of the Czech Republic (grant no. 7HX13003).

Author information

Authors and Affiliations

  1. Institute of Chemical Process Fundamentals of CAS v.v.i., Prague 6, Czech Republic

    Luděk Kaluža, Pavel Dytrych & Daniela Gulková

  2. IRD Fuel Cells A/S, Emil Neckelmanns Vej 15 A&B, DK-5220, Odense SØ, Denmark

    Mikkel J. Larsen & Madeleine Odgaard

  3. Institut Charles Gerhardt Montpellier, UMR CNRS 5253, Agrégats Interfaces Matériaux pour l’Energie, Université de Montpellier, 34095, Montpellier, Cedex 5, France

    Ignacio Jiménez Morales, Sara Cavaliere, Deborah J. Jones & Jacques Rozière

  4. Institute of Geology of CAS v.v.i., Prague 6, Czech Republic

    Anna Kallistová

Authors
  1. Luděk Kaluža
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Mikkel J. Larsen
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Ignacio Jiménez Morales
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Sara Cavaliere
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Deborah J. Jones
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Jacques Rozière
    View author publications

    You can also search for this author in PubMed Google Scholar

  7. Anna Kallistová
    View author publications

    You can also search for this author in PubMed Google Scholar

  8. Pavel Dytrych
    View author publications

    You can also search for this author in PubMed Google Scholar

  9. Daniela Gulková
    View author publications

    You can also search for this author in PubMed Google Scholar

  10. Madeleine Odgaard
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Luděk Kaluža.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Kaluža, L., Larsen, M.J., Morales, I.J. et al. Synthesis of Pt/C Fuel Cell Electrocatalysts: Residual Content of Chloride and Activity in Oxygen Reduction. Electrocatalysis 7, 269–275 (2016). https://doi.org/10.1007/s12678-016-0312-3

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12678-016-0312-3

Keywords

Search

Navigation