Abstract
The effect of casting porosity on the mechanical behavior of investment cast 17-4PH stainless steel was studied as well as the effect of heat treatment on the alloy’s sensitivity to casting defects. Interdendritic porosity, formed during solidification and shrinkage of the alloy, reduces the yield strength and ultimate tensile strength roughly in proportion to the reduction in load bearing cross-section. The effects of casting porosity on ductility (% strain, % reduction in area) are more severe, in agreement with research on other alloy systems. In this study, 10% porosity reduced the ductility of 17-4PH stainless steel by almost 80% for the high-strength H925 condition. Tensile testing at -10°C (263 K) further reduces the alloy ductility with and without pores present. In the lower strength H1100 condition, the ductility is higher than the H925 condition, as expected, and somewhat less sensitive to porosity. By measuring the area % porosity on the fracture surface of tensile specimens, the trend in failure strain versus area % porosity was obtained and analyzed using two methods: an empirical approach to determine an index of defect susceptibility with a logarithmic fit and an analytical approach based on the constitutive stress-strain behavior and critical strain concentration in the vicinity of the casting voids. The applicability of the second method depends on the amount of non-uniform strain (necking) and, as such, the softer H1100 material did not correlate well to the model. The behavior of 17-4PH was compared to previous work on cast Al alloys, Mg alloys, and other cast materials.
Similar content being viewed by others
References
Aerospace Materials Specification 5355, Issue H, Society of Automotive Engineers Inc., 2001
H.J. Rack, Physical and Mechanical Properties of Cast 17-4PH Stainless Steel, Sandia Report SAND80-2302, Sandia National Laboratories, 1981
H.J. Rack and D. Kalish, The Strength, Fracture Toughness, and Low Cycle Fatigue Behavior of 17-4PH Stainless Steel, Met. Trans., 1974, 5, p 1595–1605
G. Caligiana, L. Ceschini, and G.L. Garagnani, Effect of Aging on Fracture Toughness Parameters and Tensile Properties of 17-4PH Stainless Steel, ECF 8 Fracture Behavior and Design of Materials and Structures, 1990, Pergamon Press, Headington, p 410-16.
J.R. Kattus, Aerospace Structural Metals Handbook, Code 1501, Belfour Stulen Inc., 1978
E.A. Lauchner, The Microstructure and Ductility of 17-4PH and 15-5PH Steels, J. Mater., 1970, 5(1), p 129–139
R. Bhambroo, S. Roychowdhury, V. Kain, and V.S. Raja, Effect of Reverted Austenite on Mechanincal Properties of Precipitation Hardenable 17-4 Stainless Steel, Mater. Sci. Eng. A, 2013, A568, p 127–133
C.N. Hsiao, C.S. Chiou, and J.R. Yang, Aging Reactions in a 17-4 PH Stainless Steel, Mater. Chem. Phys., 2002, 74, p 134–142
A.M. Gokhale and G.R. Patel, Origins of Variability in the Mechanical Properties of AM60 Magnesium Alloy Castings, Magnesium Technology 2001, J. Hryn, Ed., 2001, TMS, Warrendale, p 195–199.
A.M. Gokhale and G.R. Patel, Effect of Casting Defects on Mechanical Properties of AZ91D Magnesium Alloy Castings, Aluminum 2002, Proc.TMS 2002 Annual Meeting, TMS, Warrendale, p 65–73
A.M. Gokhale and G.R. Patel, Origins of Variability in the Fracture-Related Mechanical Properties of a Tilt-Pour-Permanent-Mold Cast Al Alloy, Scripta Mater., 2005, 52, p 237–241
A.M. Gokhale and G.R. Patel, Analysis of Variability in Tensile Ductility of a Semi-Solid Metal Cast A356 Al-Alloy, Mater. Sci. Eng. A, 2005, A392, p 184–190
S.G. Lee, G.R. Patel, A.M. Gokhale, A. Sreeranganathan, and M.F. Horstemeyer, Variability in the Tensile Ductility of High-Pressure Die-Cast AM50Mg-Alloy, Scripta Mater., 2005, 53, p 851–856
M.K. Surappa, E. Blank, and J.C. Jaquet, Effect of Macro-Porosity on the Strength and Ductility of Cast Al-7Si-0.3Mg Alloy, Scripta Metall., 1986, 20, p 1281–1286
J.P. Weiler, J.T. Wood, R.J. Klassen, E. Maire, R. Berkmortel, and G. Wang, Relationship Between Internal Porosity and Fracture Strength of Die-Cast Magnesium AM60B Alloy, Mater. Sci. Eng. A, 2005, A395, p 315–322
A. Herrera and V. Kondic, Effect of Porosity on Tensile Properties of Two Al-Si Alloys, Proc. Intl. Conf. Solidification, Vol 3, Metals Society, London, 1979, p 460–465.
J.A. Eady and D.M. Smith, The Effect of Porosity on the Tensile Properties of Aluminum Castings, Mater. Forum, 1986, 9(4), p 217–223
J.T. Berry and E.P. Coleman, Linking Solidification Conditions and Mechanical Behavior in Al Castings—A Quarter Century of Evolving Evidence, AFS Trans., 1995, p 837–847.
C.H. Cáceres, On the Effect of Macroporosity on the Tensile Properties of the Al-7%Si-0.4%Mg Casting Alloy, Scripta Met. Mater., 1995, 32(11), p 1851–1856
C.H. Cáceres and B.I. Selling, Casting Defects and the Tensile Properties of an Al-Si-Mg Alloy, Mater. Sci. Eng. A, 1996, A220, p 109–116
C.D. Lee, Dependence of Tensile Properties of AM60 Magnesium Alloy on Microporosity and Grain Size, Mater. Sci. Eng. A, 2007, A454–455, p 575–580
C.D. Lee, Variability in the Tensile Properties of Squeeze-Cast Al-Si-Cu-Mg Alloy, Mater. Sci. Eng. A, 2008, A488, p 296–302
M. Tiryakioğlu, On the Ductility of Cast Al-7 Pct Si-Mg Alloys, Metall. Mater. Trans. A, 2009, 40A, p 1000–1007
M. Tiryakioğlu, On Estimating the Fracture Stress and Elongation of Al-7%Si-0.3%Mg Alloy Castings with Single Pores, Mater. Sci. Eng. A, 2010, 527, p 4546–4549
L.J. Mattek and R.D. Woodward, Correlation of Tensile Properties of Steel Castings and Materials Imperfections as Determined by Radiography, Vol 60, Issue 450 of WADD technical report (Wright Air Development Division, Air Research and Development Command, U.S. Air Force), 1961
K.-F. Nilsson and V. Vokál, Analysis of Ductile Cast iron Tensile tests to Relate Ductility Variation to Casting Defects and Materials Microstructure, Mater. Sci. Eng. A, 2009, A502, p 54–63
A.K. Ghosh, Acta Met., 1977, 25, p 1413–1424
G.E. Dieter, Chapter 8, Mechanical Metallurgy, 3rd ed., McGraw-Hill, New York, 1986,
D.F. Susan, A.C. Kilgo, T.B. Crenshaw, R.P. Grant, and R.D. Wright, Quantitative Fractography of 17-4PH Stainless Steel Investment Castings, Symp. Defect Formation, Detection, and Elimination During Casting, Welding, and Solidification, Materials Science and Technology (MS&T) 2005, Pittsburgh, PA, p 13–21.
Acknowledgments
Mark Reece and Charles Walker are acknowledged for sample machining and heat treatment. Special thanks to Dr. Jon Madison for helpful discussions. Dick Grant and Amy Allen provided SEM characterization and Alice Kilgo and Dr. Lisa Deibler provided metallography and quantitative image analysis. Thoughtful reviews of the manuscript by Dr. Jay Carroll and Dr. Mike Maguire are much appreciated. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the US Dept. of Energy’s national Nuclear Security Administration under contract DE-AC04-94AL85000.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Susan, D.F., Crenshaw, T.B. & Gearhart, J.S. The Effects of Casting Porosity on the Tensile Behavior of Investment Cast 17-4PH Stainless Steel. J. of Materi Eng and Perform 24, 2917–2924 (2015). https://doi.org/10.1007/s11665-015-1594-y
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-015-1594-y