Journal of Electronic Materials

, Volume 42, Issue 2, pp 272–279

Micro- and Nanostructure of Zn Whiskers and Their Coating

  • A. Etienne
  • E. Cadel
  • A. Lina
  • L. Cretinon
  • P. Pareige
Article

DOI: 10.1007/s11664-012-2185-4

Cite this article as:
Etienne, A., Cadel, E., Lina, A. et al. Journal of Elec Materi (2013) 42: 272. doi:10.1007/s11664-012-2185-4

Abstract

To understand the mechanisms at the origin of whisker formation and growth, a Zn-electroplated steel prone to whiskering was studied. Several samples were prepared from different locations of the electroplated plate. Care was taken to extract samples at the root, in the nodule, or away from whiskers. Samples were characterized using electron backscattered diffraction (EBSD). Crystallographic data from EBSD show that recrystallized regions are present at the root of whiskers and in their nodules. These observations support whisker growth models based on recrystallization. In addition, atom probe tomography samples were prepared in the center of whiskers. The distribution of Zn atoms is almost homogeneous and no impurities are present in the whiskers.

Keywords

Electroplatingwhiskerselectron scattering diffractionrecrystallizationfocused ion beamatom probe tomography
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Copyright information

© TMS 2012

Authors and Affiliations

  • A. Etienne
    • 1
  • E. Cadel
    • 1
  • A. Lina
    • 2
  • L. Cretinon
    • 3
    • 4
  • P. Pareige
    • 1
  1. 1.Groupe de Physique des MatériauxUniversité et INSA de Rouen, UMR CNRS 6634Saint Etienne du Rouvray CedexFrance
  2. 2.Department Material and Mechanic Components, Corrosion Studies LaboratoryEDF R&DMoret sur Loing CedexFrance
  3. 3.Department Electrical Equipment LaboratoryEDF R&DMoret sur Loing CedexFrance
  4. 4.EDF SEPTENVilleurbanne CedexFrance