Abstract
In situ synchrotron X-ray diffraction testing was carried out on a martensitic and an austenitic NiTi wire to study the evolution of internal stresses and the stress-induced martensite (SIM) phase transformation during room temperature tensile deformation. From the point of lattice strain evolution, it is concluded that (1) for the martensitic NiTi wire, detwinning of the [011]B19′ type II twins and the {010}B19′ compound twins is responsible for internal strains formed at the early stage of deformation. (2) The measured diffraction moduli of individual martensite families show large elastic anisotropy and strong influences of texture. (3) For the austenitic NiTi wire, internal residual stresses were produced due to transformation-induced plasticity, which is more likely to occur in austenite families that have higher elastic moduli than their associated martensite families. (4) Plastic deformation was observed in the SIM at higher stresses, which largely decreased the lower plateau stresses.
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Acknowledgments
Use of the synchrotron X-ray at APS was granted by the U.S. Department of Energy, Office of Science, under Contract No. DE-AC02-06CH11357. Data analysis was performed using the FIT2D, GSAS and Maud software. DSC test was performed by our colleague J. Kolhoff. SC and JES benefited from discussions with Prof. A. Stebner at Colorado School of Mines, and gratefully acknowledge Fort Wayne Metals management for their continuous support to this project.
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Manuscript submitted October 29, 2014.
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Cai, S., Schaffer, J.E., Yu, C. et al. Evolution of Intergranular Stresses in a Martensitic and an Austenitic NiTi Wire During Loading–Unloading Tensile Deformation. Metall Mater Trans A 46, 2476–2490 (2015). https://doi.org/10.1007/s11661-015-2845-0
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DOI: https://doi.org/10.1007/s11661-015-2845-0