Journal of Nanoparticle Research

, Volume 12, Issue 1, pp 209–215

Nano-powders of Na0.5K0.5NbO3 made by a sol–gel method

  • Anirban Chowdhury
  • Jonathan Bould
  • Yifan Zhang
  • Craig James
  • Steven J. Milne
Research Paper

DOI: 10.1007/s11051-009-9595-0

Cite this article as:
Chowdhury, A., Bould, J., Zhang, Y. et al. J Nanopart Res (2010) 12: 209. doi:10.1007/s11051-009-9595-0

Abstract

Sodium potassium niobate (NKN) nano-particle powders were synthesised through the thermal decomposition of a sol–gel NKN precursor. Powders and gels were characterised by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA) and transmission electron microscopy (TEM). Hydrated carbonate phases formed as a result of reaction with evolved vapours during organic decomposition, and by reaction of NKN powders with H2O and CO2 on exposure to air. The primary particle size of the powders increased from <50 to <250 nm as decomposition temperatures were raised from 500 to 950 °C.

Keywords

Nano-powdersSol–gelSodium potassium niobateX-ray diffractionFourier transform infrared spectroscopyTransmission electron microscopySynthesis method

Copyright information

© Springer Science+Business Media B.V. 2009

Authors and Affiliations

  • Anirban Chowdhury
    • 1
  • Jonathan Bould
    • 1
  • Yifan Zhang
    • 1
  • Craig James
    • 1
  • Steven J. Milne
    • 1
  1. 1.Institute for Materials Research, Houldsworth BuildingUniversity of LeedsLeedsUK