Abstract
Carrier-free 32P was produced in KAlpakkam MINI reactor (KAMINI) via 32S (n, p) 32P using its small fast flux component. This method has established the flow-sheet for the production of 32P from sulphate targets such as magnesium sulphate and strontium sulphate which can withstand high temperatures of fast reactors unlike the conventionally used sulphur powder. The chemical processing involved (i) struvite precipitation method for magnesium sulphate and (ii) co-precipitation with ferric hydroxide method for strontium sulphate.
Similar content being viewed by others
References
Atkins HL (1998) Appl Radiat Isot 49:277–283
Murty Goddu S, Anupam B, Lionel GB, Wesley EB, Dandamudi VR, Roger WH (2000) J Nucl Med 41:941–951
Silberstein EB, Elgazzar AH, Kapilivsky A (1992) Semin Nucl Med 22:17–27
Ackery D, Yardley J (1993) Semin Oncol 20:27–31
Silberstein EB (2005) Semin Nucl Med 3:152–158
Lewington VJ (2005) J Nucl Med 46:38S–47S
Pandit Taskar N, Batraki M, Chaitanya RD (2004) J Nucl Med 45(8):1358–1365
Volkert WA, Hoffman TJ (1999) Chem Rev 99:2269–2292
Fettich J, Nair G, Padhy AK, Stare J, Nair N, Moralles R, Tanumihardia M, Riccabona G (2001) IAEA-TECDOC-1228, Vienna, pp 193–198
Health effects of project shad chemical agent: Phosphorous-32 (Radiotoxic effects) (2004) The Center for Research Information, Inc., Silver Spring. http://www.medresearchnow.com. Spring
Narendra N (1999) J Nucl Med 40:256–261
Cyclotron produced radionuclides: principles and practice (2008) IAEA Technical reports series no. 465, VIENNA
Kuznetsov RA, 32,33P-Orthophosphoric acid, A Review on the Current Status and Production Technology of 32,33P-Orthophosphoric acid, KAERI/AR-574/2000, 32/49
Wierczinski B, Claessens RAMJ, De Goeij JJM, Kolar ZI, Volkers KJ (2001) J Radioanal Nucl Chem 249:279–282
Vimalnath KV, Shetty P, Chakraborty S, Das T, Viju C, Sarma HD, Jagadeesan KC, Joshi PV (2013) Cancer Biother Radiopharm 28:423–428
Razbash AA, Nerozin NA, Panarin MV, Sevast’yanov YG, Polyakov ON, Podsoblyaev DV, Smetanin WY, Dubinkina TA, Nikulin MP (1991) At Energ 70:333–335
Karelin YA, Efimov VN, Filimonov VT, Kuznetsov RA, Revyakin YL, Angreev OI, Zhemkov Y, Bukh VG, Lebedev VM, Spiridonov YN (2000) Appl Radiat Isot 53:825–827
Hong YU (2003) JAERI-Conf, JP0350197, pp 230–240
Ananthakrishnan M (2003) Phosphorous-32 (32P15), manual for reactor produced radioisotopes, Radioisotope Centre, Poland, IAEA TECDOC-1340, pp 158–160
Ananthakrishnan M, Ramaswamy AN, Nagaraja PS, Kolhe OT (1999) Int. Symp. on Res. React. Util. Saf. and Manag. Lisbon (Portugal), 6–10 Sept 1999, IAEA-SM-360/1P
Chrustowski K (2003) Phosphorous-32 (32P15) (alternate procedure), manual for reactor produced radioisotopes. Radioisotope Centre, Poland, IAEA TECDOC-1340, pp 161–166
Alanis J, Navarrete JM (2007) J Radioanal Nucl Chem 273:659–662
Lima FW, ABRAO A e LT ATALLA (1960) Third Inter-American Symp Peac Appl Nucl Energ Petrópolis, Brazil, 16–23 July, PUBLICAÇÃO I.E.A, NO. 37
Du M, Knapp FF (2003) Phosphorus-33 (33P15), manual for reactor produced radioisotopes. Radioisotope Centre, Poland, IAEA TECDOC-1340, pp 167–170
Rahaman MS, Ellis N, Mavinic DS (2008) Water Sci Technol 57:647–654
Choudhary VR, Pataskar SG, Pandit MY, Gunjikar VG (1992) Thermochim Acta 194:361–373
Acknowledgments
We gratefully acknowledge the operational personnel of KAMINI reactor who helped for the target irradiations in the above experiments.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Ashok Kumar, G.V.S., Vithya, J., Kumar, R. et al. Development of a flow-sheet for the radiochemical processing of irradiated sulphate targets for the production of carrier-free 32P. J Radioanal Nucl Chem 302, 939–945 (2014). https://doi.org/10.1007/s10967-014-3339-z
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10967-014-3339-z