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Sonochemical Synthesis of Bismuth(III) Nano Coordination Compound and Direct Synthesis of Bi2O3 Nanoparticles from a Bismuth(III) Nano Coordination Compound Precursor

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Abstract

A new coordination Compound [Bi(L)(NO3)2(ONO2)(CH3OH)] (1) [L: C5H4NCH=NNHCONC5H4] has been synthesized by the reaction of Bismuth(III) bromide with the ligand pyridine-2-carbaldehyde isoniazid and characterized by elemental analysis, FT-IR spectroscopy and single-crystal X-ray diffraction. Single crystal X-ray diffraction reveals that the compound 1 is mononuclear complex, contains Bismuth(III) in a distorted tricapped trigonal prismatic geometry environment of NNO donors of Schiff base ligand, five oxygen atoms of Nitrate molecules and one oxygen atom of methanol molecule. We also synthesized a nano form of the compound 1 by the sonochemical method and characterized it by elemental analysis, scanning electron microscopy (SEM), X-ray powder diffraction (XRD) and IR spectroscopy. The δ-Bi2O3 nano-particle was obtained by calcinations of the nano compound 1 at 500 ºC under air atmosphere and was characterized by SEM and XRD.

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References

  1. S. Kitagawa, R. Matsuda, Coord. Chem. Rev. 251, 2490–2509 (2007)

    Article  CAS  Google Scholar 

  2. A.P. Côté, A.I. Benin, N.W. Ockwig, M. O’Keeffe, A.J. Matzger, O.M. Yaghi, Science 310, 1166–1170 (2005)

    Article  Google Scholar 

  3. H. Kanoh, A. Kondo, H. Noguchi, H. Kajiro, A. Tohdoh, Y. Hattori, W.-C. Xu, M. Inoue, T. Sugiura, H. Tanaka, T. Ohba, K. Kaneko, J. Colloid Interface Sci. 334, 1–7 (2009)

    Article  CAS  Google Scholar 

  4. Y. Jin, Y. Zhu, W. Zhang, CrystEngComm. 15, 1484 (2012)

    Article  Google Scholar 

  5. G.E. Smith, G.A. Baraff, J.M. Rowell, Phys. Rev. 135, A1118 (1964)

    Article  Google Scholar 

  6. F.Y. Yang, K. Liu, K. Hong, D.H. Reich, P.C. Searson, C.L. Chien, Phys. Rev. Lett. 82, 3328 (1999)

    Article  CAS  Google Scholar 

  7. F.Y. Yang, K. Liu, K. Hong, D.H. Reich, P.C. Searson, C.L. Chien, Science 284, 1355 (1999)

    Article  Google Scholar 

  8. J.M. Goicoechea, S.C. Sevov, Angew. Chem., Int. Ed. 45, 5147 (2006)

    Article  CAS  Google Scholar 

  9. H. Sun, Y. Sakka, H. Gao, Y. Miwa, M. Fujii, N. Shirahata, Z. Bai, J. Li, J. Mater. Chem. 21, 4060 (2011)

    Article  CAS  Google Scholar 

  10. N.N. Greenwood, A. Earnshaw, Chemistry of the Elements (Pergamon Press, Oxford, 1984), pp. 235–236

    Google Scholar 

  11. R.D. Rogers, A.H. Bond, S. Aguinaga, J. Am. Chem. Soc. 114, 1967 (1992)

    Google Scholar 

  12. G.A. Bowmaker, F.M.M. Hannaway, P.C. Junk, A.M. Lee, B.W. Shelton, A.H. White, Aust. J. Chem. 51, 331 (1998). and references therein

    Article  CAS  Google Scholar 

  13. A. Morsali, A. Tadjarodi, R. Mohammadi, A.R. Mahjoub, Z. Kristallogr, NCS 216, 379–380 (2001)

    CAS  Google Scholar 

  14. Y. Gong, W. Ji, L. Zhang, B. Xie, H. Wang, J. Power Sources 196, 928 (2011)

    Article  CAS  Google Scholar 

  15. F.L. Zheng, G.R. Li, Y.N. Ou, Z.L. Wang, C.Y. Su, Y.X. Tong, Chem. Commun. 46, 5021 (2010)

    Article  CAS  Google Scholar 

  16. H. Zhang, P. Wu, Y. Li, L. Liao, Z. Fang, X. Zhong, Chem. Cat. Chem. 2, 1115 (2010)

    CAS  Google Scholar 

  17. W. Li, Mater. Chem. Phys. 99, 174 (2006)

    Article  CAS  Google Scholar 

  18. M.G. Ma, J.F. Zhu, R.C. Sun, Y.J. Zhu, Mater. Lett. 64, 1524 (2010)

    Article  CAS  Google Scholar 

  19. T.P. Gujar, V.R. Shinde, D.D. Lokhande, R.S. Mane, S.H. Han, Appl. Surf. Sci. 252, 2747 (2006)

    Article  CAS  Google Scholar 

  20. T.P. Gujar, V.R. Shinde, C.D. Lokhande, Appl. Surf. Sci. 254, 4186 (2008)

    Article  CAS  Google Scholar 

  21. T. Takeyama, N. Takahashi, T. Nakamura, S. Itoh, Solid State Commun. 133, 771 (2005)

    Article  CAS  Google Scholar 

  22. H.W. Kim, J.W. Lee, S.H. Shim, Sens. Actuators B 126, 306 (2007)

    Article  CAS  Google Scholar 

  23. L. Li, Y.W. Yang, G.H. Li, L.D. Zhang, Small 2, 548 (2006)

    Article  CAS  Google Scholar 

  24. C. Wang, C. Shao, L. Wang, L. Zhang, X. Li, Y. Liu, J. Colloid Interface Sci. 333, 242 (2009)

    Article  CAS  Google Scholar 

  25. D.R. Richardson, E. Becker, P.V. Bernhardt, Acta. Cryst. C55, 2102–2105 (1999)

    CAS  Google Scholar 

  26. S. Banerjee, S. Sen, S. Basak, S. Mitra, D.L. Hughes, R.J. Butcher, S.R. Batten, D.R. Turner, Inorg. Chim. Acta 361, 2692 (2008)

    Article  CAS  Google Scholar 

  27. S. Banerjee, S. Sen, S. Basak, S. Mitra, D.L. Hughes, C. Desplanches, Inorg. Chim. Acta 361, 2707 (2008)

    Article  CAS  Google Scholar 

  28. A. Ray, S. Banerjee, R.J. Butcher, C. Desplanche, S. Mitra, Polyhedron 27, 2409 (2008)

    Article  CAS  Google Scholar 

  29. T.E. Khalil, L. Labib, M.F. Iskander, L.S. Refaat, Polyhedron 13, 2569 (1994)

    Article  CAS  Google Scholar 

  30. N. Soltanzadeh, A. Morsali, Polyhedron 28, 703–710 (2009)

    Article  CAS  Google Scholar 

  31. J.M. Harrowfield, H. Miyamae, B.W. Skelton, A.A. Soudi, A.H. White, Aust. J. Chem. 49, 1165–1169 (1996). and references therein

    Article  Google Scholar 

  32. B. Mirtamizdoust, S. Ali-Asgari, S.W. Joo, E. Maskani, Y. Hanifehpour, T.H. Oh, J. Inorg. Organomet. Polym. 23, 751 (2013)

    Article  CAS  Google Scholar 

  33. J.M. Harrowfield, H. Miyamae, B.W. Skelton, A.A. Soudi, A.H. White, Aust. J. Chem. 49, 1165 (1996)

    Article  Google Scholar 

  34. Y. Hanifehpour, B. Mirtamizdoust, A. Morsali, S.W. Joo, Ultrason. Sonochem. 23, 275–281 (2015)

    Article  CAS  Google Scholar 

  35. N. Soltanzadeh, A. Morsali, Polyhedron 28, 1343–1347 (2009)

    Article  CAS  Google Scholar 

  36. B. Mirtamizdoust, B. Shaabani, S.W. Joo, D. Viterbo, G. Croce, Y. Hanifehpour, J. Inorg. Organomet. Polym. 22, 1397 (2012)

    Article  CAS  Google Scholar 

  37. G. Shahverdizadeh, F. Hakimi, B. Mirtamizdoust, A.A. Soudi, P. Hojati-Talemi, J. Inorg. Organomet. Polym. 22, 903 (2012)

    Article  CAS  Google Scholar 

  38. N. Soltanzadeh, Ali. Morsali. Ultrason. Sonochem. 17, 139–144 (2010)

    Article  CAS  Google Scholar 

  39. H. Sadeghzadeh, A. Morsali, P. Retailleau, Polyhedron 29, 925–933 (2010)

    Article  CAS  Google Scholar 

  40. B. Mirtamizdoust, B. Shaabani, A. Khandar, H.-K. Fun, S. Huang, M. Shadman, P. Hojati-Talemi, Z. Anorg. Allg. Chem. 638, 844 (2012)

    Article  CAS  Google Scholar 

  41. Agilent Technologies Crys Alis PRO, Yarnton (Oxfordshire, England, 2010)

    Google Scholar 

  42. M.C. Burla, M. Camalli, B. Carrozzini, G. Cascarano, C. Giacovazzo, G. Polidori, R. Spagna, SIR2002: the program. J. Appl. Cryst 36, 1103 (2003)

    Article  CAS  Google Scholar 

  43. J.C. Collings, K.P. Roscoe, E.G. Robins, A.S. Batsanov, L.M. Stimson, J.A.K. Howard, S.J. Clark, T.B. Marder, New J. Chem. 26, 1740 (2002)

    Article  CAS  Google Scholar 

  44. F. Bigdeli, A. Morsali, P. Retailleau, Polyhedron 29, 801–806 (2010)

    Article  CAS  Google Scholar 

  45. F. Bigdeli, A. Morsali, P. Retailleau, Polyhedron 29, 801–806 (2010)

    Article  CAS  Google Scholar 

  46. M.Y. Masoomi, A. Morsali, RSC Adv. 3, 19191–19218 (2013)

    Article  CAS  Google Scholar 

  47. M.Y. Masoomi, A. Morsali, P.C. Junk, RSC Adv. 4, 47894–47898 (2014)

    Article  CAS  Google Scholar 

  48. H.P. Xiao, A. Morsali, Helv. Chim. Acta 88, 2543 (2005)

    Article  CAS  Google Scholar 

  49. Y. Hanifehpour, B. Mirtamizdoust, S.W. Joo, J. Inorg. Organomet. Polym 22, 916–922 (2012)

    Article  CAS  Google Scholar 

  50. M.A.M. Abu-Youssef, A. Escuer, D. Gatteschi, M.A.S. Goher, F.A. Maunter, R. Vicente, Inorg. Chem. 38, 5716–5723 (1999)

    Article  CAS  Google Scholar 

  51. A. Escuer, R. Vicente, M.A.S. Goher, F.A. Maunter, Inorg. Chem. 37, 782–787 (1998)

    Article  CAS  Google Scholar 

  52. Z. Shen, J.-L. Zuo, Z. Yu, Y. Zhang, J.-F. Bai, C.-M. Che, H.K. Fun, J.J. Vittal, X.-Z. You, J. Chem. Soc. Dalton Trans. 19, 3393–3397 (1999)

    Article  Google Scholar 

  53. K. Akhbari, S. Beheshti, A. Morsali, V.T. Yilmaz, O. Buyukgungor, J. Mol. Struct. 1074, 279–283 (2014)

    Article  CAS  Google Scholar 

  54. M.Y. Masoomi, G. Mahmoudi, A. Morsali, J. Coord. Chem. 63, 1186–1193 (2010)

    Article  CAS  Google Scholar 

  55. A. Ramazani, S. Hamidi, A. Morsali, J. Mol. Liq. 157, 73–77 (2010)

    Article  CAS  Google Scholar 

  56. M.Y. Masoomi, A. Morsali, Coord. Chem. Rev. 256, 2921–2943 (2012)

    Article  CAS  Google Scholar 

  57. E. Tahmasebi, M.Y. Masoomi, Y. Yamini, A. Morsali, Inorg. Chem. 54, 425–433 (2015)

    Article  CAS  Google Scholar 

  58. M.Y. Masoomi, K.C. Stylianou, A. Morsali, P. Retailleau, D. Maspoch, Cryst Growth Des 14, 2092–2096 (2014)

    Article  CAS  Google Scholar 

  59. M.Y. Masoomi, S. Beheshti, A. Morsali, J. Mater. Chem. A 2, 16863–16866 (2014)

    Article  CAS  Google Scholar 

  60. M.Y. Masoomi, A. Morsali, P.C. Junk, CrystEngComm. 17, 686–692 (2015)

    Article  CAS  Google Scholar 

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Acknowledgements

The authors thank Tabriz University and Qom University for all the supports and also acknowledge the project Praemium Academiae of the Academy of Sciences of the Czech Republic.

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Authors and Affiliations

  1. Department of Inorganic Chemistry, Faculty of Chemistry, Tabriz University, 51666-14766, Tabriz, Iran

    Majid Sadeghi Roodsari & Behrouz Shaabani

  2. Department of Chemistry, Faculty of Science, University of Qom, PO Box 37185-359, Qom, Islamic Republic of Iran

    Babak Mirtamizdoust

  3. Institute of Physics of the ASCR v.v.i, Na Slovance 2, 18221, Prague 8, Czech Republic

    Michal Dusek & Karla Fejfarova

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  1. Majid Sadeghi Roodsari
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Correspondence to Majid Sadeghi Roodsari.

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Sadeghi Roodsari, M., Shaabani, B., Mirtamizdoust, B. et al. Sonochemical Synthesis of Bismuth(III) Nano Coordination Compound and Direct Synthesis of Bi2O3 Nanoparticles from a Bismuth(III) Nano Coordination Compound Precursor. J Inorg Organomet Polym 25, 1226–1232 (2015). https://doi.org/10.1007/s10904-015-0231-4

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  • DOI: https://doi.org/10.1007/s10904-015-0231-4

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