Abstract
Iron (Fe) is commonly found in aluminum (Al), but its contents are usually kept as low as possible, because the formation of intermetallic phases may induce fracture. In this study, high-pressure torsion (HPT) was used to control the microstructure in an Al-2 %Fe alloy in conjunction with wire drawing and an aging treatment, in order to improve not only their mechanical properties but also the electrical conductivity. It is shown that HPT processing of ring-shaped samples produced ultrafine grains with a size of ~150 nm in the matrix, while intermetallic phases were fragmented to nanosizes with some Fe fraction dissolved in the matrix. Semi-rings were extracted from the HPT-processed samples and swaged to a round section with 0.4-mm diameter. The HPT-processed sample was successfully drawn to a final diameter of 0.08 mm (25:1 ratio, 96 % reduction in area), whereas the sample without HPT processing failed after drawing to 0.117-mm diameter (12:1 ratio, 91 % reduction in area). The electrical conductivity increased to ~65 IACS % in the HPT-processed rings and to ~54 IACS % in the wires by aging for 1 h after the drawing.
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References
Sverdlin A (2003) Properties of pure aluminum. In: Totten GE, MacKenzie DS (eds) Handbook of aluminum, vol I., Physical Metallurgy and ProcessesMarcel Dekker Inc, New York, pp 33–79
Tenório JAG, Espinosa DCR (2003) Recycling of aluminum. In: Totten GE, MacKenzie DS (eds) Handbook of aluminum, vol II., Alloy production and materials manufacturingMarcel Dekker Inc, New York, pp 115–153
Schlesinger ME (2006) Aluminum recycling. Taylor & Francis Group, Boca Raton
Belov NA, Aksenov AA, Eskin DG (2002) Iron in aluminum alloys: impurity and alloying element. Taylor & Francis, London
Valiev RZ, Islamgaliev RK, Alexandrov IV (2000) Bulk nanostructured materials from severe plastic deformation. Prog Mater Sci 45:103
Senkov ON, Froes FH, Stolyarov VV, Valiev RZ, Liu J (1998) Microstructure and microhardness of an Al-Fe alloy subjected to severe plastic deformation and aging. Nanostruct Mater 10:691
Senkov ON, Froes FH, Stolyarov VV, Valiev RZ, Liu J (1998) Microstructure of aluminum-iron alloys subjected to severe plastic deformation. Scripta Mater 38:1516
Cubero-Sesin JM, Horita Z (2012) Mechanical properties and microstructures of Al-Fe alloys processed by high-pressure torsion. Metall Mater Trans A 43:5182
Cubero-Sesin JM, Horita Z (2013) Strengthening of Al through addition of Fe and by processing with high-pressure torsion. J Mater Sci 48:4713
Pippan R, Scheriau S, Taylor A, Hafok M, Hohenwarter A, Bachmaier A (2010) Saturation of fragmentation during severe plastic deformation. Annu Rev Mater Res 40:319
Harai Y, Ito Y, Horita Z (2008) High-pressure torsion using ring specimens. Scripta Mater 58:469
Harai Y, Edalati K, Horita Z, Langdon TG (2009) Using ring samples to evaluate the processing characteristics in high-pressure torsion. Acta Mater 57:1147
Fujioka T, Horita Z (2009) Development of high-pressure sliding process for microstructural refinement of rectangular metallic sheets. Mater Trans 50:930
Edalati K, Horita Z (2010) Continuous high-pressure torsion. J Mater Sci 45:4578
Edalati K, Lee S, Horita Z (2012) Continuous high-pressure torsion using wires. J Mater Sci 47:473
Strid J, Porter DA, Easterling KE (1985) Microstructure and plasticity of an Al-Al6Fe directionally solidified eutectic alloy. Mater Sci Tech 1:161
Walford LK (1965) The structure of the intermetallic phase FeAl6. Acta Crystallogr 18:287
Black PJ (1955) The Structure of FeAl3 I. Acta Crystallogr 8:43
Black PJ (1955) The Structure of FeAl3 II. Acta Crystallogr 8:175
Dieter GE (1986) Mechanical metallurgy, 3rd edn. McGraw-Hill, New York
Valiev RZ, Estrin Y, Horita Z, Langdon TG, Zehetbauer MJ, Zhu YT (2006) Producing bulk ultrafine-grained materials by severe plastic deformation. JOM 58:33
Koch CC (2003) Optimization of strength and ductility in nanocrystalline and ultrafine-grained metals. Scripta Mater 49:657
Horita Z, Ohashi K, Fujita T, Kaneko K, Langdon TG (2005) Achieving high strength and high ductility in precipitation-hardened alloys. Adv Mater 17:1599
Zhao YH, Liao XZ, Cheng S, Ma E, Zhu YT (2006) Simultaneously increasing the ductility and strength of nanostructured alloys. Adv Mater 18:2280
Sabirov I, Murashkin MYu, Valiev RZ (2013) Nanostructured aluminium alloys produced by severe plastic deformation: new horizons in development. Mater Sci Eng A 560:1
Estrin Y, Vinogradov A (2013) Extreme grain refinement by severe plastic deformation: a wealth of challenging science. Acta Mater 61:782
Acknowledgements
This study was carried out as a part of a materials development program in the Japan Aluminum Association. One of the authors (JC) thanks the Ministry of Education, Culture, Sports, Science and Technology (MEXT) of Japan for a PhD scholarship. This work was supported in part by the Light Metals Educational Foundation of Japan, in part by a Grant-in-Aid for Scientific Research from the Ministry of Education, Culture, Sports, Science and Technology of Japan in the Innovative Area “Bulk Nanostructured Metals”(22102004).
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Cubero-Sesin, J.M., In, H., Arita, M. et al. High-pressure torsion for fabrication of high-strength and high-electrical conductivity Al micro-wires. J Mater Sci 49, 6550–6557 (2014). https://doi.org/10.1007/s10853-014-8240-1
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DOI: https://doi.org/10.1007/s10853-014-8240-1