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Reinforcement of SC-15 epoxy with CNT/CNF under high magnetic field: an investigation of mechanical and thermal response

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Abstract

We report here reinforcement of SC-15 epoxy matrix with 1.0 wt% loading of carbon nanotubes (CNTs)/carbon nanofibers (CNFs), and cured under a high (28 T) magnetic field. The improvement in mechanical properties such as compressive strength and stiffness was phenomenal with CNT inclusion, about 126% and 166% increase in strength and modulus, respectively. Enhancement in the glass transition (T g) and thermal decomposition temperatures was also significant, by about 30 and 23 °C, respectively. Although the degree of anisotropy introduced by the magnetic field was not significant, it was observed that almost half of the improvement was due to magnetic flocculation. In the following is described the results of initial experiments conducted in the National High Magnetic Field Laboratory (NHMFL). Enhanced properties of the nanocomposites strongly suggest improved ordering of nanoparticles within the matrix.

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References

  1. Barclay GG, Ober CK, Papathomas KI, Wang DW (1992) Macromolecules 25:2947

    Article  CAS  Google Scholar 

  2. Barclay GG, McNamee SG, Ober CK, Papathomas KI, Wang DW (1992) J Polym Sci A Polym Chem 30:1845

    Article  CAS  Google Scholar 

  3. Ober CK, Barclay GG (1991) Mater Res Soc Symp Proc 227:281

    Article  CAS  Google Scholar 

  4. Lincoln MD, Douglas EP (1999) Polym Eng Sci 39:1903

    Article  CAS  Google Scholar 

  5. Reynaud E, Gautier C, Perez J (1999) Rev Metall 96:169

    Article  CAS  Google Scholar 

  6. Chun LW, Ming QZ, Min ZR, Klaus F (2002) Comp Sci Tech 62:1327

    Article  Google Scholar 

  7. Mahfuz H, Islam M, Rangari V, Saha M, Jeelani S (2004) Compos B 35:543

    Article  Google Scholar 

  8. Mahfuz H, Adnan A, Rangari VK, Hasan MM, Jeelani S, Wright WJ, De Teresa SJ (2006) Appl Phys Lett 88:083119

    Article  Google Scholar 

  9. Camponeschi E, Vance R, Al-Haik M, Garmestani H, Tannenbaum R (2007) Carbon 45:2037

    Article  CAS  Google Scholar 

  10. Treacy MMJ, Ebbesen TW, Gibsoj JM (1996) Nature 381:6584

    Article  Google Scholar 

  11. Yu MF, Lourie O, Dyer MJ, Noloni K, Kelly TF, Ruoff RS (2000) Science 287:637

    Article  CAS  Google Scholar 

  12. Mahfuz H, Rangari V, Adnan A, Jeelani S (2004) Compos A Appl Sci Manuf 35:519

    Article  Google Scholar 

  13. Parker MR, Al-Saadi T, Mahfuz H, Zainuddin S, Rangari V, Jeelani S (2005) In: The 2nd international conference on nanocomposites and nanotechnologies (NN 2005), Crete, Greece, June 14–18

  14. Wang XK, Chang RPH, Patashinski A, Ketterson JB (1994) J Mater Res 9:1578

    Article  CAS  Google Scholar 

  15. Byszewski P, Baran M (1995) Europhys Lett 31:363

    Article  CAS  Google Scholar 

  16. Tsui F, Jin L, Zhou O (2000) Appl Phys Lett 76:145

    Google Scholar 

  17. Svoboda J (1981) Int J Miner Process 8:377

    Article  CAS  Google Scholar 

  18. Parker MR, Van Kleef RPAR, Myron HW, Wyder P (1982) J Mag Mag Mater 27:250

    Article  CAS  Google Scholar 

  19. Mahfuz H, Zainuddin S, Parker MR, Al-Saadi T, Rangari VK, Jeelani S (2007) Mater Lett 61:2535

    Article  CAS  Google Scholar 

  20. Rodin YP, Molchanov YM (1988) Effect of conformal changes caused by a homogeneous static magnetic field on curing of epoxy resin. Mech Compos Mater 24(3):380

    Article  Google Scholar 

  21. Mahfuz H, Rangari V, Islam M, Jeelani S (2004) Compos A Appl Sci Manuf 35:453

    Article  Google Scholar 

  22. Mahfuz H, Adnan A, Rangari V, Jeelani S (2005) Int J Nanosci (IJN) 4(1):55

    Article  CAS  Google Scholar 

  23. Rodgers RM, Mahfuz H, Rangari VK, Chisholm N, Jeelani S (2005) Macromol Mater Eng 290(5):423

    Article  CAS  Google Scholar 

  24. Shia D, He P, Lian J, Chaud X, Bud’ko SL, Beaugnon E, Wang LM, Ewing RC, Tournier R (2005) J Appl Phys 97:064312

    Article  Google Scholar 

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Acknowledgement

A portion of this work was performed at the National High Magnetic Field Laboratory (NHMFL) which was supported by NSF Cooperative Agreement No. DMR-0084173, by the State of Florida, and by the DOE. We also acknowledge with appreciation the support for this work by ONR.

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Correspondence to Hassan Mahfuz.

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Mahfuz, H., Zainuddin, S., Parker, M.R. et al. Reinforcement of SC-15 epoxy with CNT/CNF under high magnetic field: an investigation of mechanical and thermal response. J Mater Sci 44, 1113–1120 (2009). https://doi.org/10.1007/s10853-008-3161-5

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  • DOI: https://doi.org/10.1007/s10853-008-3161-5

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