Summary
A dichrometric procedure has now been developed for the direct volumetric titration of thallium(I), to an iodine monochloride end point. The concentration of the hydrochloric acid must be at least 7.5 N at the end point.
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References
Fresenius, W., and G. Jander: Handbuch der Analytischen Chemie, Dritter Teil, Bd.III, 2. Aufl., S. 104–107 (1956).
Rao, K. Bhaskara, G. Jagga Rao and G. Gopala Rao: Z. analyt. Chem. 157, 181 (1957).
Swift, E. H., and C. S. Garner: J. Amer. chem. Soc. 58, 113 (1936); cf. Z. analyt. Chem. 109, 43 (1937).
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Rao, K.B. Dichrometric determination of thallium (I). Z. Anal. Chem. 165, 193–195 (1959). https://doi.org/10.1007/BF00450292
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DOI: https://doi.org/10.1007/BF00450292