Journal of Nanoparticle Research

, Volume 10, Issue 6, pp 1059–1062

Synthesis and characterization of myristic acid capped silver nanoparticles

  • P. K. Khanna
  • Deepti Kulkarni
  • Rupinder K. Beri
Brief Communication

DOI: 10.1007/s11051-008-9366-3

Cite this article as:
Khanna, P.K., Kulkarni, D. & Beri, R.K. J Nanopart Res (2008) 10: 1059. doi:10.1007/s11051-008-9366-3

Abstract

Reduction of silver myristate (AgMy) under mild thermal reaction conditions in a dipolar aprotic solvent i.e. N, N-dimethylformamide (DMF) has been carried out. UV–visible absorption measurements of dried and re-dispersible brown flocculants showed broad features of surface plasmon resonance (SPR) due to silver nanoparticles. The freshly isolated particles showed absorption bands at 414 and 485 nm, respectively, due to inter-particle coupling or clustering of silver ions and silver atoms. X-ray diffraction (XRD) pattern of fcc zero-valent silver resulted in crystallite size of about 10 nm. Scanning electron microscopy (SEM) revealed formation of rod shaped silver with increasing reaction temperature. Thermal analysis (TGA) showed about 10% weight loss due to organic capping.

Keywords

ReductionNoble metalChemical synthesisXRDColloids

Copyright information

© Springer Science+Business Media B.V. 2008

Authors and Affiliations

  • P. K. Khanna
    • 1
  • Deepti Kulkarni
    • 1
  • Rupinder K. Beri
    • 1
  1. 1.Nanoscience Group, Centre for Materials for Electronics Technology (C-MET)PuneIndia