A procedure for the microwave sample preparation of nickel alloys to determine the mass fractions of Al, Ti, Cr, Co, Nb, Mo, Ru, Ta, W, and Re by atomic-emission spectrometry with an inductively coupled plasma is described. The compositions of the mixtures for solution and the parameters of the microwave dispersion are chosen. The limits of the relative error in measuring the mass fraction of the elements from 0.1% to 20% do not exceed 4% (P = 0.95).
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References
A. A. Papyshev and D. A. Danilova, “The use of atomic-emission spectrometry with an inductively coupled plasma to analyze materials and products of ferrous metallurgy,” Analit. Kontrol, 11, No. 2–3, 131–181 (2007).
E. A. Tormysheva, E. V. Smirnova, and T. N. Ermolaeva, “Microwave sample preparation of fused materials for analysis by atomic-emission spectroscopy with an inductively coupled plasma,” Zavod. Lab. Diagn. Mater., 76, No. 10, 10–13 (2010).
E. N. Kablov, G. A. Morozov, V. N. Krutikov, and N. P. Muravskaya, “Certification of standard samples of a compound of multiply-doped alloys using a standard,” Aviats. Mater. Tekhnol., No. 2, 9–11 (2012).
A. F. Letov, F. N. Karachevtsev, N. V. Gundobin and V. I. Titov, “The development of standard samples of a compound of alloys for aviation purposes,” Aviats. Mater. Tekhnol., No. 5, 393–398 (2012).
B. S. Lomberg, M. M. Bakradze, E. B. Chabina, and E. V. Filonova, “The relation between the structure and properties of highly heat-resisting nickel alloys for the disks of gas turbine engines,” Aviats. Mater. Tekhnol., No. 2, 25–30 (2011).
E. B. Chabina, E. V. Filonova, B. S. Lomberg, and M. M. Bakradze, “The structure of modern deformable nickel alloys,” All Materials: Encyclopedic Handbooh (2012), Vol. 6, pp. 22–27.
N. V. Petrushin, E. S. Elyutin, E. B. Chabina, and O. B. Timofeeva, “Phase and structural transitions in heat resistant rhenium-containing alloys of single-crystal structure,” Lit. Proizv., No. 7, 1–7 (2008).
N. V. Petrushin, I. L. Svetlov, A. P. Samoilov, et al., “High-temperature phase and structural transitions in single crystals of heat-resistant nickel-alloy, containing rhenium and ruthenium,” Materialovedenie, No. 11, 26–31 (2008).
E. N. Kablov, N. V. Petrushin, I. L. Svetlov, and I. H. Demonis, “Nickel lithium heat-resistant alloys of a new generation,” Aviats. Mater. Tekhnol., No. 5, 36–52 (2012).
B. S. Lomberg, S. V. Ovsepyan, M. M. Bakradze, and I. S. Mazalov, “High-temperature heat-resistant nickel alloys for the components of gas turbine engines,” ibid., 52–57.
B. S. Lomberg, S. V. Ovsepyan, and M. M. Bakradze, “Features of the doping and heat treatment of heat-resistant nickel alloys for the disks of a new generation of gas turbine engines,” Aviats. Mater. Tekhnol., No. 2, 3–8 (2010).
B. S. Lomberg, S. V. Ovsepyan, and M. M. Bakradze, “A new heat-resistant nickel alloy for the disks of gas turbine engines and gas turbine equipment,” Materialovedenie, No. 7, 24–28 (2010).
J. L. Todoli, L. Gras, V. Hernandis, and J. Mora, “Elemental matrix effects in ICP-AES,” J. Anal. At. Spectrom., No. 17, 142–169 (2002).
GOST R ISO12284–2009, Steel and Cast Iron. Selection and Preparation of Samples for Determining the Chemical Composition.
GOST 8.563–2009, GSI. Measurement Procedures (Methods).
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Translated from Metrologiya, No. 1, pp. 60–68, January–March, 2015.
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Zagvozdkina, T.N., Karachevtsev, F.N., Dvoretskov, R.M. et al. The Use of Optical Methods of Measurement to Investigate the Composition of New Aviation Materials. Meas Tech 58, 362–366 (2015). https://doi.org/10.1007/s11018-015-0717-z
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DOI: https://doi.org/10.1007/s11018-015-0717-z