Crystal structure of N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine
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- Ramazani, A., Dolatyari, L., Morsali, A. et al. JICS (2006) 3: 367. doi:10.1007/BF03245960
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N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine crystallizes in orthorhombic space group Pbca with a = 9.5634(6), b = 14.2917(9), c = 16.9181(8) Å and Z = 4. The crystal structure was solved by direct methods and refined by full-matrix least squares to final values R1 = 0.0 + 399 and wR2 = 0.1004 with 2755 reflections (I > 2σ(I)). The N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine molecules exhibit intramolecular N-H...O and are connected by C-H...O and C-H...π interactions to form a 2D supramolecular network.