Journal of the Iranian Chemical Society

, Volume 3, Issue 4, pp 367–370

Crystal structure of N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine

  • A. Ramazani
  • L. Dolatyari
  • A. Morsali
  • V. T. Yilmaz
  • O. Büyükgüngör
Article

DOI: 10.1007/BF03245960

Cite this article as:
Ramazani, A., Dolatyari, L., Morsali, A. et al. JICS (2006) 3: 367. doi:10.1007/BF03245960

Abstract

N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine crystallizes in orthorhombic space group Pbca with a = 9.5634(6), b = 14.2917(9), c = 16.9181(8) Å and Z = 4. The crystal structure was solved by direct methods and refined by full-matrix least squares to final values R1 = 0.0 + 399 and wR2 = 0.1004 with 2755 reflections (I > 2σ(I)). The N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine molecules exhibit intramolecular N-H...O and are connected by C-H...O and C-H...π interactions to form a 2D supramolecular network.

Keyword

N,N-disalicylidene-(R,S)(S,R)-1,2-ethanediamine Crystal structure Hydrogen bonding C-H...π interaction 

Copyright information

© Iranian Chemical Society 2006

Authors and Affiliations

  • A. Ramazani
    • 1
  • L. Dolatyari
    • 1
  • A. Morsali
    • 2
  • V. T. Yilmaz
    • 3
  • O. Büyükgüngör
    • 4
  1. 1.Department of ChemistryIslamic Azad University-Zanjan BranchZanjanIran
  2. 2.Department of Chemistry, Faculty of SciencesTarbiat Modares UniversityTehranIran
  3. 3.Department of Chemistry, Faculty of Arts and SciencesOndokuz Mayis UniversityKurupelit, SamsunTurkey
  4. 4.Department of Physisc, Faculty of Arts and SciencesOndokuz Mayis UniversityKurupelitTurkey