Experimental Mechanics

, Volume 42, Issue 1, pp 123–128

In-situ tensile testing of nano-scale specimens in SEM and TEM

Authors

  • M. A. Haque
    • Department of Mechanical & Industrial EngineeringUniversity of Illinois at Urbana-Champaign
  • M. T. A. Saif
    • Department of Mechanical & Industrial EngineeringUniversity of Illinois at Urbana-Champaign
Article

DOI: 10.1007/BF02411059

Cite this article as:
Haque, M.A. & Saif, M.T.A. Experimental Mechanics (2002) 42: 123. doi:10.1007/BF02411059

Abstract

We present a new experimental method for the mechanical characterization of freestanding thin films with thickness on the order of nanometers to micrometers. The method allows, for the first time, in-situ SEM and TEM observation of materials response under uniaxial tension, with measurements of both stresses and strains under a wide variety of environmental conditions such as temperature and humidity. The materials that can be tested include metals, dielectrics, and multi-layer composites that can be deposited/grown on a silicon substrate. The method involves lithography and bulk micromachining techniques to pattern the specimen of desired geometry, release the specimen from the substrate, and co-fabricate a force sensor with the specimen. Co-fabrication provides perfect alignment and gripping. The tensile testing fits an existing TEM straining stage, and a SEM stage. We demonstrate the proposed methodology by fabricating a 200 nm thick, 23.5 μm wide, and 185 μm long freestanding sputter deposited aluminum specimen. The testing was done in-situ inside an environmental SEM chamber. The stress-strain diagram of the specimen shows a linear elastic regime up to the yield stress σy MPa, with an elastic modulusE=74.6 GPa.

Key Words

Mechanical propertiesMEMS fabricationtensile testingthin films

Copyright information

© Society for Experimental Mechanics, Inc. 2002