Preparative isolation of (+)-beta-eudesmol fromAmyris balsamifera
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Optically pure (+)-beta-eudesmol is a possible starting material for the synthesis of several termite defense compounds. A two step procedure for the isolation of gram quantities of (+)-beta-eudesmol from commercially availableAmyris balsamifera oil (syn. West Indian sandalwood oil), containing 8% beta-eudesmol, was developed. Step one consisted of an efficient vacuum distillation of the total oil. Step two was a medium pressure LC separation with an AgNO3 impregnated silica gel stationary phase. Several other separation procedures failed due to the presence of many closely related sesquiterpene alcohols (75% of the oil).
- R. Kesselmans, J.P.B.A. Wijnberg andAE. de Groot, in preparation to be submitted for publication in J. org. Chem.
- T.A. van Beek, R. Kleis, M.A. Posthumus andA. van Veldhuizen, Phytochemistry (1989) in press.
- Preparative isolation of (+)-beta-eudesmol fromAmyris balsamifera
Volume 28, Issue 3-4 , pp 126-128
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- Column liquid chromatography
- Preparative isolation
- Amyris balsamifera
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