Abstract
Several methods for the rapid determination of the degree of acetylation of chitin and related polymers have been evaluated, including the use of the infrared and the mass spectra.
Chitin and chitosan have characteristic degradation temperatures and it is possible to determine the acetylation degree by the use of empirical correlations based on the weight losses associated with the main decomposition peaks.
References
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R. A. A. Muzzarelli, Chitin, Pergamon Press, 1977, p. 105.
G. K. Moore, Proceedings of the First International Conference on Chitin/Chitosan, Ed. R. A. A. Muzzarelli and E. R. Pariser, 1978, p.421.
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I. Garcia Alonso, Informe Técnico-Ciéntéfico, N∘ 165, Academia de Ciencias de Cuba, 1981, pp. 11.
C. Peniche-Covas, Resúmenés del I Congreso Nacional de la Sociedad Cubana de Química, 1982, pp. 172.
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Alonso, J.G., Peniche-Covas, C. & Nieto, J.M. Determination of the degree of acetylation of chitin and chitosan by thermal analysis. Journal of Thermal Analysis 28, 189–193 (1983). https://doi.org/10.1007/BF02105290
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DOI: https://doi.org/10.1007/BF02105290