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Synthesis of MgFe1.6Ga0.4O4 by Gel Combustion Using Glycine and Hexamethylenetetramine

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Abstract

A powderlike material of composition MgFe1.6Ga0.4O4 was synthesized by gel combustion using a glycine–hexamethylenetetramine mixture. The gel produced by the synthesis was studied by thermal analysis (TGA/DSC) and IR spectroscopy. This mixture was shown to be efficient for obtaining homogeneous nanosized MgFe1.6Ga0.4O4. The morphology of the powders was characterized by scanning electron microscopy and X-ray powder diffraction analysis.

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Correspondence to M. N. Smirnova.

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Original Russian Text © M.N. Smirnova, M.A. Kop’eva, E.N. Beresnev, L.V. Goeva, N.P. Simonenko, G.E. Nikiforova, V.A. Ketsko, 2018, published in Zhurnal Neorganicheskoi Khimii, 2018, Vol. 63, No. 4, pp. 411–415.

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Smirnova, M.N., Kop’eva, M.A., Beresnev, E.N. et al. Synthesis of MgFe1.6Ga0.4O4 by Gel Combustion Using Glycine and Hexamethylenetetramine. Russ. J. Inorg. Chem. 63, 439–443 (2018). https://doi.org/10.1134/S0036023618040198

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  • DOI: https://doi.org/10.1134/S0036023618040198

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