Abstract
A powderlike material of composition MgFe1.6Ga0.4O4 was synthesized by gel combustion using a glycine–hexamethylenetetramine mixture. The gel produced by the synthesis was studied by thermal analysis (TGA/DSC) and IR spectroscopy. This mixture was shown to be efficient for obtaining homogeneous nanosized MgFe1.6Ga0.4O4. The morphology of the powders was characterized by scanning electron microscopy and X-ray powder diffraction analysis.
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G. D. Nipan, A. I. Stognii, V. A. Ketsko, et al., Usp. Khim. 81, 458 (2012).
A. I. Stognii, A. V. Trukhanov, V. A. Ketsko, et al., Inorg. Mater. 47, 204 (2011).
A. A. Geras’kin, A. I. Stognii, N. N. Novitskii, et al., Russ. J. Inorg. Chem. 59, 183 (2014).
M. N. Smirnova, A. A. Geras’kin, A. I. Stognii, et al., Russ. J. Inorg. Chem. 59, 778 (2014).
A. M. Glezer, Nanocrystals Quenched from Melt (Fizmatlit, Moscow, 2011) [in Russian].
V. A. Ketsko, E. N. Beresnev, M. A. Kop’eva, et al., Russ. J. Inorg. Chem. 55, 427 (2010).
M. N. Smirnova, A. A. Geras’kin, G. E. Nikiforova, et al., Russ. J. Inorg. Chem. 60, 930 (2015).
M. N. Smirnova, L. V. Goeva, N. P. Simonenko, et al., Russ. J. Inorg. Chem. 61, 1301 (2016).
D. M. Yufanyi, A. M. Ondoh, J. Foba-Tendo, et al., Am. J. Chem. 5, 1 (2015).
Inorganic Biochemistry, Ed. by G. Eichhorn. (Elsevier, Amsterdam, 1975), Vol.1.
K. Nakamoto, Infrared Spectra of Inorganic and Coordination Compounds (Wiley, New York, 1963).
K. I. Turte, A. G. Lazaresku, Yu. A. Simonov, et al., Russ. J. Coord. Chem. 22, 42 (1996).
E. N. Beresnev, M. N. Smirnova, N. P. Simonenko, et al., Russ. J. Inorg. Chem. 61, 1026 (2016).
I. N. Bronshtein and K. A. Semendyaev, Handbook of Mathematics for Engineers and Students of Technical Universities (Nauka, Moscow, 1981).
M. W. Janaf, Phys. Chem. Ref. Data 14, 156 (1985).
A. G. Kasatkin, Unit Operations and Equipment of Chemical Engineering (Khimiya, Moscow, 2004) [in Russian].
V. M. Khot, A. B. Salunkhe, M. R. Phadatare, et al., Mat. Chem. Phys. 132, 782 (2012).
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Original Russian Text © M.N. Smirnova, M.A. Kop’eva, E.N. Beresnev, L.V. Goeva, N.P. Simonenko, G.E. Nikiforova, V.A. Ketsko, 2018, published in Zhurnal Neorganicheskoi Khimii, 2018, Vol. 63, No. 4, pp. 411–415.
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Smirnova, M.N., Kop’eva, M.A., Beresnev, E.N. et al. Synthesis of MgFe1.6Ga0.4O4 by Gel Combustion Using Glycine and Hexamethylenetetramine. Russ. J. Inorg. Chem. 63, 439–443 (2018). https://doi.org/10.1134/S0036023618040198
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DOI: https://doi.org/10.1134/S0036023618040198