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Determining low concentrations of Zr, Ce, La, and Y in heat-resistant nickel alloys by inductively coupled plasma atomic emission

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Abstract

A technique for mass fraction determination of microalloying additions—Zr, Ce, La, and Y (from 0.001 to 0.1 wt %)—in heat-resistant nickel alloys by inductively coupled plasma atomic emission is described. Results from samples of nickel alloys are in good agreement with the data of spectrophotometric and chemical-spectral analysis. The values of thecontent of Zr, Ce, La, Y in artificial mixtures of nickel-based alloy are reproduced.

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References

  1. Parshin, A.M., Kirillov, N.B., Petkova, A.P., and Nikolaeva, O.V., Microalloying with Rare-Earth Elements and Properties of Steels and Alloys, Nauchno-Tekh. Vedomosti S-Peterb. Gos. Tekh. Univ., 2002, vol. 27, no. 1, p. 33.

    Google Scholar 

  2. GOST (State Standard) 12365-84: Alloy and High-Alloy Steels. Methods for Determination of Zirconium, 1984.

  3. GOST (State Standard) 12364-84: Alloy and High-Alloy Steels. Methods for Determination of Cerium, 1984.

  4. OST (Industry Standard) 1-90142-96: Heat-Resistant Nickel Alloys. Methods for Determination of Lanthanum and Cerium, 1996.

  5. OST (Industry Standard) 1-90433-96: Heat-Resistant Nickel Alloys. Methods for Determination of Zirconium and Hafnium, 1996.

  6. PI (Production Instruction) 1.2.417089: Quantitative Spectrum Analysis of Nickel Alloys with Photoelectric and Photographic Spectrum Recordings, 1989.

  7. Havarro, M.S., Ulbrich, H.H.G.J., Andrade, S., and Janasi, V.A., Adaption of ICP-OES Routine Determination Techniques for the Analysis of Rare Earth Elements by Chromatographic Separation in Geologic Materials: Tests with Reference Materials and Granitic Rocks J. Alloys Compd., 2002, vol. 344, nos. 1–2, p. 40.

    Google Scholar 

  8. De Aza, P.N., Quitian, F., De Aza, S., and Valle, F.J., Analytical Control of Wollastonite for Biomedical Applicatons by Use of Atomic Absorption Spectrometry and Inductively Coupled Plasma Atomic Emission Spectrometry, Analyst, 1998, vol. 123, no. 4, p. 681.

    Google Scholar 

  9. Kujirai, O. and Yamads, K., Application of Cobalt Ammine Complexes for the Simultaneous Determination of Traces of As, Fe, Ti, Anal. Bioanal. Chem., 1996, vol. 354, no. 4, p. 428.

    Article  CAS  Google Scholar 

  10. Yang, X.-J. and Rin, C., Determination of Trace Zirconium and Hafnium in Basaltic Rocks by Inductively Coupled Plasma Atomic Emission Spectrometry after Chemical Separation: an Evaluation of Two Methods Based on Extraction Chromatography, Analyst, 2000, vol. 125, no. 3, p. 453.

    Article  CAS  Google Scholar 

  11. Shizhong, C., Tianyou, P., Zucheng, J., Zhenhuan, L., and Bin, H., Direct Determination of Rare Earth Impurities in Lanthanum Oxide by Fluorination Assisted Electrothermal Vaporization Inductively Coupled Plasma Atomic Emission Spectrometry with Slurry Sampling, JAAS, 1999, vol. 14, no. 11, p. 1723.

    Google Scholar 

  12. Hilligoss, D., Krampitz, P., and Yates, D.A., Analysis of Complex Alloys Containing Ni, Cr, Cu and Al. ICP Optical emission, Application note, Norwalk: Perkin Elmer, 1999.

    Google Scholar 

  13. Ficher, P.T. and Ellgren, A.J., Analysis of rare earth-containing metallurgical samples by inductively coupled plasma-atomic emission spectrometry, Spectrochim. Acta, Part B, 1983, vol. 38, nos. 1–2, p. 309.

    Article  Google Scholar 

  14. OST (Industry Standard) 1-90126-85 Heat-Resistant Vacuum-Melted Alloys, 1986.

  15. GOST (State Standard) R 52802-2007: Heat-Resistant Granulatable Nickel Alloys. Grades, 2008.

  16. GOST (State Standard) 6689.13-92: Nickel, Nickel and Nickel-Copper Alloys. Arsenic Determining Methods, 1992; GOST (State Standard) 6689.17-92: Nickel, Nickel and Nickel-Copper Alloys. Methods for Determination of Bismuth, 1992.

  17. GOSTs (State Standard) 24018.0-80-24018.6-80: Heat-Resistant Nickel-Based Alloys. Methods for Determination of Tin, Antimony, Lead, Bismuth, and Arsenic Microadmixtures, 1980.

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Authors and Affiliations

  1. Institute of Metallurgy, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russia

    N. B. Romanova, N. V. Pechishcheva & K. Yu. Shunyaev

  2. All-Russian Scientific Research Institute of Aviation Materials (VIAM), Moscow, Russia

    V. I. Titov & N. V. Gundobin

Authors
  1. N. B. Romanova
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  2. N. V. Pechishcheva
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  3. K. Yu. Shunyaev
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  4. V. I. Titov
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  5. N. V. Gundobin
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Corresponding author

Correspondence to K. Yu. Shunyaev.

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Original Russian Text © N.B. Romanova, N.V. Pechishcheva, K.Yu. Shunyaev, V.I. Titov, N.V. Gundobin, 2011, published in Zavodskaya Laboratoriya. Diagnostika materialov, 2011, Vol. 77, No. 7, pp. 5–9.

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Romanova, N.B., Pechishcheva, N.V., Shunyaev, K.Y. et al. Determining low concentrations of Zr, Ce, La, and Y in heat-resistant nickel alloys by inductively coupled plasma atomic emission. Inorg Mater 48, 1315–1319 (2012). https://doi.org/10.1134/S0020168512140142

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  • DOI: https://doi.org/10.1134/S0020168512140142

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